Date of Issue: 05/07/2014 04:11:41 DEP Bureau of Laboratories - Harrisburg P.O. Box 1467 2575 Interstate Drive Harrisburg, PA 17105-1467 Contact Phone Number: (717) 346-7200 Analytical Report For Mining And Reclamation Date Collected: 04/10/2014 11:20:00 AM Sample ID: 0523 092 Lab Sample ID: I2014009874 Status: Completed Name of Sample Collector: Gregory Prentice Date Received: County: Greene State: PA Municipality: Jefferson Boro Sample Medium: Water Sample Medium Type: Water Location: Outfall of Clyde Mine AMD Plant (final discharge) Reason: Complaint Project: NOT INDICATED Standard Anlysis: 755 Matrix: Water Stream Condition: Sample Standard Comment: Time Limit For Test Exceeded Test Codes / CAS # - Description Reported Results Date And Time Analyzed Analyst Test Method 00410M ALKALINITY REPORTED @ pH 3.9 216.0 MG/L 04/11/2014 06:02 PM SSPUHLER SM 2320B 01105A ALUMINUM, TOTAL (WATER & WASTE) BY ICP <200 UG/L 04/16/2014 10:09 AM MOBERCASH EPA 200.7 71870 4.340 MG/L 04/16/2014 08:19 AM FVODOPIVEC EPA 300.0 772.000 UG/L 04/16/2014 10:09 AM MOBERCASH EPA 200.7 BROMIDE BY ION CHROMATOGRAPHY 01045A IRON, TOTAL (WATER & WASTE) BY ICP 1 of 2 Analytical Report For Mining And Reclamation Sample ID: 0523 092 Date Collected: 04/10/2014 11:20:00 AM Lab Sample ID: I2014009874 Status: Completed Test Codes / CAS # - Description Reported Results Date And Time Analyzed Analyst Test Method 01055A MANGANESE, TOTAL (WATER & WASTE) BY ICP 217.000 UG/L 04/16/2014 10:09 AM MOBERCASH EPA 200.7 82550 126 MOSM 04/11/2014 12:45 PM KMCMULLEN BOL BOL 8.5 pH units 04/11/2014 06:02 PM SSPUHLER SM 4500H-B 01147H SELENIUM, TOTAL (WATER & WASTE) BY ICPMS 9.800 UG/L 04/16/2014 03:33 PM DSOLENBERG EPA 200.8 00929A SODIUM, TOTAL (WATER & WASTE) BY ICP 1910.000 MG/L 04/16/2014 10:09 AM MOBERCASH EPA 200.7 01082A STRONTIUM, TOTAL (WATER & WASTE) BY ICP * 3639.000 UG/L 04/16/2014 10:09 AM MOBERCASH EPA 200.7 70508 -124.80 MG/L 04/14/2014 03:17 PM TVOROBEYCH SM 2310B 00940A Total Chloride-Colorimetric 736.0 MG/L 04/30/2014 01:01 PM CRADEK SM 4500-CL E 70300U TOTAL DISSOLVED SOLIDS @ 180C BY USGS-I-1750 6938 MG/L 04/11/2014 12:00 AM LWILKINSON USGS I-1750 00945A Total Sulfate-Colorimetric 4050.4 MG/L 04/24/2014 01:51 PM LHREHA EPA 375.2 00530 64 MG/L 04/11/2014 12:00 AM LWILKINSON USGS I-3765 OSMOTIC PRESSURE, MOS/KG 00403M pH Reported with 3.9 alk ** Comment ** Time Limit For Test Exceeded Total Acidity ** Comment ** Aliquot of sample used for analysis yielded > 200 mg dried TOTAL SUSPENDED SOLIDS The results of the analyses provided in this laboratory report relate only to the sample(s) identified in the report. Unless otherwise noted, the results presented on this laboratory report meet all the requirements of the 2009 TNI standards. Sample was in acceptable condition when received by the Laboratory. Any exceptions are noted in the report. Tests noted with an "*" are not included in our NJ NELAP Annual Certified Parameter List. Taru Upadhyay, Technical Director, Bureau of Laboratories 2 of 2