Chamours— TheChemoursCompany 910- 483- 46810 Fluoroproducts chemours com 22828 NC Highway 87 W Fayetteville, NC 28306- 7332 CERTIFIED MAIL ARTICLE NUMBER 7002 0860 0006 9104 7828 RETURN RECEIPT REQUESTED April 27, 2016 Ms. Wren Thedford NCDEQ Division of Water Resources NPDES Unit 1617 Mail Service Center Raleigh, North Carolina RECEIVED/ NCDEQ/ DWR 27699- 1617 MAY O' S 1016 SUBJECT: NPDES Permit Renewal Application Water Quality Permitting Section NPDES Permit No. NC0003573 Dear Ms. Thedford: The Chemours Company — Fayetteville Works is requesting renewal of NPDES Wastewater Discharge Permit No. NC0003573. Since the issuance of the last permit, the ownership of this facility changed from the DuPont Company to The Chemours Company FC, LLC. Also, two separate companies, Kuraray America Inc. and the DuPont Company, are operating manufacturing units and are treating and discharging their wastewaters under the Chemours' NPDES Permit. Enclosed are the original and two copies of the General Information Form 1 ( Form 3510- 1), Wastewater Discharge Information Form 2C ( Form 3510- 2C), and additional required supporting documentation for renewal of the subject permit by the NC Division of Water Resources. Included in the permit application are the following supplemental information documents: Sludge Management Plan, Current Facility Wastewater Management, Current Facility Operating Conditions, Alternate Application Schedule for § 316( b) of the Clean Water Act, Elimination of Monitoring Requirement for PFOA, and the non-reporting of bis(chloromethyl) ether. If you have any questions or need additional information, please contact me at ( 910) 678- 1155. Sincerely, a E. Johnson, PE nvironmental Manager Enclosures r Form Approved v pleAe print or type in the unshaded areas only U S. ENVIRONMENTAL PROTECTION AGENCY FORM E/ EPA 1 I EPA I D GENERAL INFORMATION 5 Consolidated Permits Program F TrA NCD Read the" General instructions" before starang) GENERAL OMB No 2040- 0086 NUMBER 047 368 642 D 3 2 5 14 GENERAL INSTRUCTIONS LABEL ITEMS If a prepnnted label has been provided, affix it in the designated space Review the information carefully, if any of it I. EPA I D III. FACILITY NAME is incorrect, cross through it and enter the correct data in the NUMBER appropriate fill- in area below Also, if any of the preprinted data is absent ( the area to the left of the label space lists the information that should appear), please provide it in the proper fill- in area( s) below If the label is complete and correct, you PLEASE PLACE LABEL IN THIS SPACE need not complete Items I, FACILITY MAILING V. III, V, and VI ( except VI-B which must be completed regardless) Complete all items if no label ADDRESS has been provided Refer to the instructions for detailed item for the legal authorizations under which this FACILITY LOCATION VI data ncollected is ollected II POLLUTANT CHARACTERISTICS INSTRUCTIONS Complete A through J to determine whether,you need to submit any permit application forms to the EPA If you answer" yes" to any questions, you must submit this form and the supplemental form listed in the parenthesis following the question Mark" X" in the box in the third column if the supplemental form is attached If you answer" no" to each question, you need not submit any of these forms. You may answer" no" if your activity is excluded from permit requirements, see Section C of the Instructions See also, Section D of the instructions for definitions of bold-faced terms Mark" X" Mark* X* YES NO SPECIFIC QUESTIONS FORM results in a discharge to waters of the U. S?( C Is this a facility which currently results in discharges to / waters of the U. S. other than those described in A or B above?( FORM 2C) X X zz E Does or will this facility treat, store, or dispose brought to the surface 34 below the lowermost X stratum 31 32 33 X fuel, or recovery of geothermal energy?( FORM 4) 31 36 35 J 1 36 39 Is this facility a proposed stationary source which is NOT one of the X 28 industrial categories listed in the X instructions and which will potentially emit 250 tons per year of any air pollutant regulated under the Clean Air Act 40 or be located in an attainment area?( FORM 5) effluent solution mining of minerals, in situ combustion of fossil Is this facility a proposed stationary source which is one which will potentially emit 100 tons per year of any air pollutant regulated under the Clean Air Act and may affect 27 processes such as mining of sulfur by the Frasch process, X inject fluids used for enhanced recovery of oil or natural gas, or inject fluids for storage of liquid hydrocarbons? of the 28 industrial categories listed in the instructions and / 26 Do you or will you inject at this facility industrial or municipal in FORM 4) X 25 containing, within one quarter mile of the well bore, underground sources of drinking water?( FORM 4) N 21 H Do you or will you inject at this facility fluids for special connection with conventional oil or natural gas production, 1 20 19 the U. S. 9( FORM 2D) X G Do you or will you inject at this facility any produced water are FORM 2B) or B above) which will result in a discharge to waters of F 26 ATTACHED D Is this a proposed facility( other than those described in A 2. 23 of hazardous wastes?( FORM 3) which discharge to waters of the U. S?( 1e r , FORM NO B Does or will this facility ( either existing or proposed) include a concentrated animal feeding operation or aquatic animal production facility which results in a X FORM 2A) 16 or other fluids SPECIFIC QUESTIONS ATTACHED A Is this facility a publicly owned treatment works which YES 42 91 43 and may affect or be located in an attainment area? 44 u FORM 5) III NAME OF FACILITY T,KIEE& 15 IV 18- 29 mours Company - Fayetteville FACILITY CONTACT A NAME& TITLE( last, first,& 2 15 Works 70 Johnson, Michael, Environmenta B ade) PHONE( area code& 6 1 ) Manager 45 16 48 46 8- 1 no) 5 51 1 52- l9 55 V. FACILTY MAILING ADDRESS A STREET OR P O BOX c22828 NC Highway 87 WW 3 5 45 16 4 Fayetteville, 15 VI. D ZIP CODE C STATE B CITY OR TOWN 2 C 40 16 41 42 3 6 47 51 FACILITY LOCATION A STREET, ROUTE NO OR OTHER SPECIFIC IDENTIFIER c 5 2 8 8 NC 5 ighway 8 45 16 B COUNTY NAME Bladen to D STATE C CITY OR TOWN E ZIP CODE F COUNTY CODE( if known) c F y t evi 15 C 1 16 41 40 42 23 47 3 6 51 52 017 - SC CONTINUE ON REVERSE EPA Form 3510- 1( 8- 90) c COt?TINUED FROM THE FRONT VII SIC CODES( 4- digit, to order of rion A Jt 7 2869 15 B FIRST 1peC) specfy) INDUSTRIAL ORGANIC CHEMICALS 19 16 C 6pec) 43'08'Al UNSUPPORTED process 3083 15 16 SECOND LAMINATED PLASTICS PLATE, D t FILM AND SHEET units SHEET, AND PROFILE SHAPES 19 THIRD PLASTICS Kuraray Butacite HutaciteO and SentryGlasO sheeting NOTE 7 7 2 821 FOURTH sped) PLASTIC MATERIALS AND RESINS DuPont NOTE: PVF resin process units 15 VIII OPERATOR INFORMATION B. Is the name listed In Item A NAME VIII- A also the owner? Jc LLC s The Chemours Company FC, 5 FEDERAL M= S= STATE P= B6 D PHONE( area code& C. STATUS OF OPERATOR( Enter the appropriate letter into the answer box if" Other," specify) F= NO G3 YES 55 16 no) specify) PUBLIC( otherthanfederal orstate) p ( 302) A ( 773- 1000 0= OTHER( specfy) PRIVATE 18 1516 19 21 22 26 E STREET OR P o BOX 1 0 treet t 55 26 F JB 15 X G STATE CITY OR TOWN DE Wilmington H ZIP CODE IX INDIAN LAND Is the facility located on Indian lands? L19898 13 NO YES 52 0 16 t1 t2 47 51 - EXISTING ENVIRONMENTAL PERMITS A C T 9 N 15 16 C T NPDES C NC0003573 1] 30 18 B UIC 9 D PSD AirFnmvons from Pro osedSources D, schar es toSurface Water 91P NC 151 18 1 1] Title V Permit E I W6003 C T R 15 1 16 XI tp eC1h) Land App l kation Penult 9 18 E OTHER( specify) C I NCD047368642 1] OTHER s ect ) 431 C RCRA Hazardous Wastes 9 03735 19 Under roundlnecuanjFlutds N/ A U T T specify) 9 39 1 15 1 18 117 118 18 MAP Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must show the outline of the facility, the location of each of Its existing and proposed Intake and discharge structures, each of Its hazardous waste treatment, storage, or disposal facilities, and each well where it Injects fluids underground Include all springs, rivers, and other surface water bodies In the map area. See instructions for precise requirements XII. NATURE OF BUSINESS( provide a bnefdescnphon) Fayetteville Works) Fayetteville Works ( formerly the DuPont Company Chemours Company chemicals manufacturer situated on" a 2, 200- acre property in northwestern Bladen County, NC. The The Chemours, located at operates the SentryGlasO a fluorinated products produced at the facility include fluorinated monomers and fluorinated vinyl ethers, Nafion" membranes and dispersion, oil- fired boilers, which provides Also is this ionoplast manufacturing Chemours operates two natural gas / fuel Kuraray Kuraray America Inc. and the DuPont Company. companies: thermoplastic sheet and resin manufacturing unit and the resin DuPont operates two polyvinyl fluoride ( PVF) interlayer manufacturing unit. facility are Butacite° and fluoropolymer processing aids. steam for the entire facility. two tenant polyvinyl butyral ( PVB) units. Chemours receives and treats all of the Kuraray and DuPont process wastewater, sanitary wastewater, and contact stormwater in the Chemours' owned and operated wastewater treatment plant, and discharges that treated wastewater through Outfall 001 under the Chemours' NPDES Wastewater Discharge Permit ( Permit No. N00003573) . The Kuraray and DuPont non- contact cooling waters and stormwaters are discharged through Outfall 002 under the Chemours' NPDES Wastewater Discharge Permit. XIII CERTIFICATION( see instructions) I certify under penalty of law that I have personally examined and am familiar with the information submitted in this application and all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information contained to the appltcatro I believe that the information is true, accurate, and complete I am aware that there are significant penalties for submitting false information, including the possibility of fi B SI A. NAME 8 OFFICIAL TITLE( type orprint) Ellis H. MCGaughy - Plant and imprisonment C DATE SIGNED ATURE/// Z' 7/ 2'01 Manager V COMMENTS FOR OFFICIAL USE ONLY JC s, 6 EPA Form 3510- 1( 8- 90) 55 yoAs RALEIGH, N. C. 5E14 SAIN'P PAULS 15' QUADRANGLE G hal. TO l.N7PRSTATF 9v 30° AND COMMUNITY DEVELOPMENT 7. 5 MINUTE SERIES ( TOPOGRAPHIC) GEOLOGICAL SURVEY 78° 5?' 34° 52' 30'' - DEPARTMENT OF NATURAL RESOURCE NORTH CAROLINA DEPARTMENT OF THE INTERIOR z STATE OF NORTH CAROLINA DUART QUADRANGLE UNITED STATES 6950 0- E 697 cabs C,- EEK G AN. 5253/ V NE 5 CEDAR CREEK) 699 < i C m BM 144 140 737 x l i_- l b I B 140 . w i \\ 7 I 1 S v o 3860000- N l 731 " VV V, Cem Ci e 7" L 1 i L 1. J.' a 1 hWo'pd en o ake f C 3859 i ek Mill ' Cam 1, a 1 4"— pin Wil s k r eki oze 3858° C F13 glA 7& Tanks i r ' it S p V 6e 158 0 1 Tanks nd Waste r o onds Sbstatro 3857 o _ r agin FACILITY LEGAL l + ' I 117 I BOUNDARY rr{; Huske Dam No 3 1 0 Daniel SM 14s 50' 1 3856 o 66 o 7C g. ° 758 O- i75 Ap 7 3855 a erBo pQ9e• em r O y aros Hal y s Lock M 145 i i o ARadio Tower Boat ogre W mP SCALE 1: 24 000 cz z 5 D MILES 1000 0 1000 5 l000 2000 3000 0 40005000 KILOMETERS 0METERS o 6000 7000 8000 9000 10 000 1 1000 2000 k CONTOUR INTERVAL 5 FEET NATIONAL GEODETIC VERTICAL DATUM OF 1929 Boone_ cam Duact Roadside' 3852 THIS MAP COMPLIES WITH NATIONAL MAP ACCURACY STANDARDS 47' 30° FOR SALE ABYFOLDER U. S. DESCRIBING GEOLOGICALTOPOGRAPHIC SURVEY, DENVER, COLORADO 80225, OR RESTON, VIRGINIA 22092 MAPS AND SYMBOLS IS AVAILABLE ON REQUEST BM 136 CHEMOURS COMPANY - FAYETTEVILLE WORKS LOCATIONS OF INTAKE AND DISCHARGE STRUCTURES NORTH dP RIVER WATER INTAKE AND PUMPS t SAW r i, i - ' OUTFALL 002 EFFLUENT OUTFALL 001 DISCHARGE POINT USACE LOCK& DAMW. CHEMOURS COMPANY - FAYETTEVILLE WORKS s LOCATIONS OF HAZARDOUS WASTE MANAGEMENT FACILITIES NORTH Two( 2) Waste Fluorocarbon Tanks corrosive, reactive, toxic) Waste DMSO Storage Tank corrosive) ti Hazardous Waste Storage Area Y Waste '. corrosive, toxic) Fluorocarbon Tank corrosive, reactive, toxic) dk Ignitable Waste l ' Container USACE LOCK& DAAS= h Fir. - *• v * k * '' r. i 1 t .- 1\ _.. *•* r ri r I yam,.: . 1. v 1, 4. YAl r I A 1 Properly! 1 t t 1000 All welts are shown1. Photograph 0 11 000 2, 000 Form Approved. EPA 1. D. NUMBER(, opi 1rwn ltrnr I r)/ hirrnr I) OMB No. 2040- 0086. IVCD Please print or type in the unshaded areas only. 047 368 FORM 642 Approval expires 3- 31- 98. U. S. ENVIRONMENTAL PROTECTION AGENCY ZC FOR PERMIT TO DISCHARGE WASTEWATER EPA \-/ ACTURING, EXISTING MANUFACTURING, COMMERCIAL, MINING AND SILVICULTURE OPERATIONS Consolidated Permits Program NPDES I. OUTFALL LOCATION For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water. C. LONGITUDE B. LATITUDE A. OUTFALL NUMBER h, i) 1 2, MIN. DEG 001 34. 002 34. 00 1 2. MIN. DEG D. RECEIVING WATER( mune) 3 SEC. 00 22. 93 - 78. 00 50. 00 11. 47 Cape Fear River 50. 00 21. 58 - 78. 00 49. 00 25. 70 Cape Fear River 50. 00 3 SEC II. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES A Attach a line drawing showing the water flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent, and treatment units labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average flows between intakes, operations, treatment units, and outfalls. If a water balance cannot be determined( e. g.. for certain mining activities). provide a pictorial description of the nature and amount of any sources of water and any collection or treatment measures. B. For each outfall, provide a description of: ( 1) All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water, and storm water runoff; ( 2) The average flow contributed by each operation: and ( 3) The treatment received by the wastewater. Continue on additional sheets if necessary. 1 3. TREATMENT 2. OPERATION( S) CONTRIBUTING FLOW OUTFALL b. LIST CODES FROM b. AVERAGE FLOW NO.( lot) 51OL•OCICAL Che,— urs Man,:`. a--. wring P= xess:+ ura- a' Demin 1) Eutacite Mfg Process 5 Mfg water Process Areas INFLUENT S--. Evaporation from Sludge Drying water Content OLITTAL- Outfall 0^ Treated Effluen- 002 NonCantact river ware- Near— tacr. Eilte_ed water Stormwater sediment and O aeration gal; day 1, 205, aaa gal/ day emergency Retention Tank E e- Digester 1- C Tank 3- 5) Activated Sludge 6) Clarrficatron ( 3 Aeration E Tank A clarifiers in ca—_ 1-'_ L--- EIOLOGICAL S-' 2DGE ._? LIPS-i 50, 000gal/ riay I1) 19, 943ga 1/ 2, 493 gal/ daY 1, 133, 452 gal/ day 1, 1s3, 552 — 1! Dissolved Air Flotation da y 2) Rotary Filter 3) Sludge Filter f4I Sludge Steam- Hca-- Fri. 5) L`isr— 1— Off-: I ...;: I I. day 23, 057, 345 gal! day 1, 9_ a, 3. a a. 1/ day 50, 000 gal/ day Elow'down TOTAL 002 - OFFICIAL USE ONLY( with mr>: ina 214, 509 gal/ tiny Removal 9oiler Condensate O; ITFALL gal/ day Operations EFF', JEN' f gal/ day 10, 000 of TOTAL 1 001 WWTP gal/ day 75, 000 3- 1, 215 water from 211, 655 4! -_ R-egene_'atc Evawra: i: n S1- 3) TOWWTP Influent Equalizac.ioa gal/ day Processes Neutralized PLANT gal/ day eZ) Sanitary Sewer TOTAL 5, 55": Sentr Y'= - las Mfg Process DuPont _ VF WASTEWATER. TREATMENT 7. 59, 361 gal/ day 0 01 xcraray TABLE 2C- 1 a. DESCRIPTION u), fmIe unu) a. OPERATION( hvr) EF' FL; IEN' r 3.'. 4, 000 gal/ day Discharge 6, 013, 13.3 gal/ day to surface water ( Cape Fear R--).. r. fllurnrsrur(.lina cuh- arra;knri,,) EPA Form 3510- 2C( 8- 90) PAGE 1 of 4 CONTINUE ON REVERSE CONTINUED FROM THE FRONT C. Except for storm runoff, leaks, or spills. are any of the discharges described in Items II- A or B intermittent or seasonal? W1 NO Cvn ru. S i lnnr 1/ 1) YES( complete the fill,-, g!able) 3 4 FLOW FREQUENCY B TOTAL VOLUME a DAYS PER 1 MONTHS PER YEAR prr(1i CONTRIBUTING FLOW OUTFALL b WEEK 2 OPERATION( s) NUMBER( h, t) a. FLOW RATE( nrG, Q prn) r wluuun) 1 LONGTERM 2 MAXIMUM 1 LONG TERM AVERAGE DAILY AVERAGE 2 MAXIMUM C DURATION DAILY III. PRODUCTION A. Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility? W] YES( omtpletn Item 111- 1i) NO Cpo to Semon 11) B. Are the limitations in the applicable effluent guideline expressed in terms of production( or other measure of operation)? W] NO( ea to. Secuan 11) YES( complete Nem 1/ 1-() C- If you answered" yes" to Item III- B, list the quantity which represents an actual measurement of your level of production, expressed in the terms and units used in the applicable effluent guideline, and indicate the affected outfalls. 1. AVERAGE DAILY PRODUCTION 2. AFFECTED OUTFALLS c. OPERATION, PRODUCT, MATERIAL, ETC. a. QUANTITY PER DAY b. UNITS OF MEASURE h, lomlitll muahen) sperrh) IV. IMPROVEMENTS A Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater treatment equipment or practices or any other environmental programs which may affect the discharges described in this application? This includes, but is not limited to, permit conditions, administrative or enforcement orders, enforcement compliance schedule letters, stipulations, court orders, and grant or loan conditions. NO( iu w Nem II'- R) YES( romplew the fid/m, my tahk) 1. IDENTIFICATION OF CONDITION, 2. AFFECTED OUTFALLS 3. BRIEF DESCRIPTION OF PROJECT 4. FINAL COMPLIANCE DATE AGREEMENT. ETC. a NO. b SOURCE OF DISCHARGE a REQUIRED b. PROJECTED B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs ( or other environmental projects which may affect your discharges) you now have underway or which you plan. Indicate whether each program is now underway or planned, and indicate your actual or planned schedules for construction. MARK" X" IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED EPA Form 3510- 2C( 8- 90) PAGE 2 of 4 CONTINUE ON PAGE 3 i EPA I. D. NUMBER( ru/„/ rum lien,/ NCD 047 368 q// , nn l) 642 CONTINUED FROM PAGE 2 V INTAKE AND EFFLUENT CHARACTERISTICS A. B, 8 C See instructions before proceeding— Complete one set of tables for each outfall— Annotate the outfall number in the space provided. NOTE: Tables V- A. V- B. and V- C are included on separate sheets numbered V- 1 through V- 9. D. Use the space below to list any of the pollutants listed in Table 2c- 3 of the instructions, which you know or have reason to believe is discharged or may be discharged from any outfall. For every pollutant you list, briefly describe the reasons you believe it to be present and report any analytical data in your possession. None in of the Table pollutants 2C- 3 Inc. present discharge in from POLLUTANT 2. SOURCE listed are believed the wastewater thi 1. 2. SOURCE 1. POLLUTANT to site. VI. POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final product or byproduct? W1YES( 6ct all nah Pollutant, hrGn, NO(,, u tr, Item 17- 8) Antimony Benzene 1, 2- dichloroethane Methylene chloride Toluene EPA Form 3510- 2C( 8- 90) PAGE 3 of 4 CONTINUE ON REVERSE CONTINUED FROM THE FRONT VII. BIOLOGICAL TOXICITY TESTING DATA Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in relation to your discharge within the last 3 years? YES( nlomlt the teuly/ uud de rnhc their pure—,, The " North with the Carolina requirement Ceriodaphnia of Chronic condition A( 4) of NO(¢ o ro Sewwr I' lll) h. luo) Effluent Bioassay Procedure" the facility' s NPDES Permit. is performed each quarter The NCDEQ Division of in accordance Water Resources has copies of the Form AT- 1 test results that were submitted with the Discharge Monitoring Reports during the period from February 2012 through February 2016. The quarterly chronic test performed during February 2012, failed for the ceriodaphnia dubia No other The required monthly chronic tests performed in March and April 2012 both passed. reproduction. toxicity test failures occurred during the five- year term of the current permit. VIII. CONTRACT ANALYSIS INFORMATION Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm? YES( ler thr n. nnr a, hire,. NO(, 4o ro Semon A) and idep{wne number of and pollrnunte analrcrd{, r. rorh w, h hrhoranory or firer hchnr) D. POLLUTANTS ANALYZED C. TELEPHONE A B ADDRESS NAME 2401 TBL West Lumberton, 5th Street NC 28358 list) area rude X no.) Chemical 910- 738- 6190 Oxygen Total COD); Carbon ( Fecal Total TOC); Susoended Ammonia ( Demand Organic Solids ( TSS); as N); Color; Fluoride; Coliform; Nitrate- Nitrite ( as Nitrogen; as Oil N); Total Total and SO4) Surfactants; Total Cyanide, C Part and GC/ Metals, Phenols; Volatile Part Compounds; MS - Total C Total GC/ MS - Compounds; P); Iron; Magnesium; Manganese; Acid as 1 Total Total Aluminum; Fart Grease; Phosphorus ( Sulfate ( as N); Organic C GC/ MS - Part C Base/ Neutral Compounds; Fraction - Part C GC/ M5 Pesticides IX. CERTIFICATION I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true. accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. B PHONE NO.( arra rodr& no.) A. NAME& OFFICIAL TITLE( npr orpron) Ellis C. SIGN H. McGaughy URE - Plant Man 910) er 678- 1224 D DATE SIGNED Q Z- 7 EPA Form 3510- 2C( 8- 90) PAGE 4 of 4 FORM 2C ITEM II- A: NPDES PERMIT RENEWAL APPLICATION LINE DRAWING Chemours Company- Fayetteville Works NPDES Permit No. NC0003573 WATER BALANCE ( Revised 04- 21- 2016) Flow Units: Gallons per Day Basis: ( 1) All Manufacturing Units operating 2) Maximum 30- day average of measured flows( 2013- 2015) Cape Fear River 26, 567, 845 NaOCI 3, 500, 000 Sediment Filtered Water FILTERED 50, 000 2, 400, 000 WATER SYSTEM NON- CONTACT RIVER WATER 1, 050, 000 to/ from each unit200, 000 Demineralized COOLING WATER 1, 800, 000 Water DEMINERALIZED 975, 000 WATER SYSTEM 100, 000 23, 067, 845 150, 000 150, 000 Neutralized Regenerate 578, 000 72, 000 325, 000 Atmosphere PURCHASED CHEMOURS 10, 000 POTABLE KURARAY AMERICAS DUPONT DUPONT BUTACITEtRt SENTRYGLASIRI POLYVINYL POLYVINYL FLUORIDE FLUORIDE FLUOROPRODUCT 1, 000 WATER KURARAY AMERICAS MANUFACTURING PROCESSES SANITARY FACILITIES POLYVINYL BUTYRAL LAMINATE MANUFACTURING MANUFACTURING PROCESS PROCESS i RESINPROCESS# 1 RESIN PROCESS# 2 BOILERS, STORM- 10, 000 Stormwa ^—— 100, 000 44, 173 1, 722, 343 112, 639 75, 000 105, 827 105, 827 655, 657 159, 361_ j WATER 44, 173 I r from I ProcessProcess Alas 94, 216 I I Condensate/ 1 1 Blowdown I Non- Contact Cooling Water 26, 813, 133 1 I 214 509 1, 205, 888 Non- process I Stormwater Evaporation OUTFALL I ACTIVATED H I SLUDGE 50, 000 19 I EI WWTP 324 000 CLARIFI- OUTFALL CATION' 001 I ml 19, 943 BIOSOLIDS DEWATER/ 1 I Biosohds Moisture 2, 493 -- DRYING 0 0 c U U o 1, 133, 452 3 cc U Evaporation I o 3 Z o o Z Z 002 OUTFALL 001 PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information FEPA LD NUMBER( copyfrom Item I ofForm 1) on separate sheets( use the same format) instead of completing these pages NCD SEE INSTRUCTIONS. 047 3 68 642 OUTFA LL NO. 0 V. INTAKE AND EFFLUENT CHARACTERISTICS( continued from page 3 ofForm 2- C) ooi PART A- You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details. 3. UNITS 2. EFFLUENT b. MAXIMUM 30 DAY VALUE a MAXIMUM DAILY VALUE 1. POLLUTANT CONCENTRATION ( CONCENTRATION 26. 8 ( 2) MASS 4. INTAKE blank) opnona( c. LONG TERM AVRG. VALUE fmwdable) ifavatfable) 2) MASS specrfv( ( 1) CONCENTRATION ( a. LONG TERM AVERAGE VALUE 2) MASS d. NO. OF ANALYSES 37. 8 465 m g/ L lb. n a. CONCEN- TRATION b. NO. OF b. MASS CONCENTRATION ( 2) MASS ANALYSES a. Biochemical Oxygen Demand( BOD) 71. 0 675. 9 b. Chemical Oxygen Demand( COD) 32. 1 313. 2 1 m g/ L lb. n/ a n/ a n/ a 84. 9 828. 4 1 mg/ L lb. n/ a n/ a n/ a 44. 0 387. 8 465 m L mg L lb. n/ a n/ a n/ a 0. 414 4. 0 1 mg/ L lb. n/ a n/ a n/ a 1095 MGD MGD c. Total Organic Carbon TOC) d. Total Suspended Solids( TS.S VALUE f. Flow MINIMUM 6. 37 22. 2 VALUE MINIMUM n/ a a n a n a VALUE 907 n/ a n/ a n/ a n/ a n/ a n/ a VALUE 18. 4 118 C 29. 0 118 C VALUE 30. 6 MAXIMUM 8. 47 54. 6 VALUE 32. 0 summer) 8 0. VALUE VALUE i• PH 9. 1. 133 26. 0 h. Temperature 177. 0 VALUE 627 VALUE hinter) PART B- 22. 0 5. 8 VALUE 1. g Temperature 207. 1 VALUE MAXIMUM n/ a STANDARD UNITS 374 Mark" X" in column 2- a for each pollutant you know or have reason to believe is present. Mark" X" in column 2- b for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements. 2. MARK" X" 3. EFFLUENT b b. MAXIMUM 30 DAY VALUE a. MAXIMUM DAILY VALUErf available 1. POLLUTANT AND a CAS NO. BELIEVED BELIEVED favadable) PRESENT ABSENT 1) 1) CONCENTRATION ( 2) MASS CONCENTRATION 4. UNITS 1) ( 2) MASS 5. INTAKE( opuonal) c LONG TERM AVRG. VALUE fm,minble) CONCENTRATION ( 2) MASS a. LONG TERM AVERAGE VALUE d. NO. OF ANALYSES a. CONCENTRATION b. MASS b NO. OF CONCENTRATION ( 2) MASS ANALYSES a. Bromide 24959-67- 9) b Chlorine, Total Residual c. Color X 0. 03 0. 3 1 mg/ L lb. n/ a n/ a n/ a X 10 n/ a 1 PCU n/ a n/ a n/ a n/ a n/ 1 col/ dL n/ a n/ a n/ a n/ a 1659 1 mg/ L lb. n/ a n/ a n/ a 0. 6 1 mg/ L lb. n/ a n/ a n/ a d. Fecal Coliform X est. 2 a e. Fluoride 170 16964 4& 8) to Nitrite X 88- EPA Form 3510- 2C(( 990) 0. 065 PAGE V- 1 CONTINUE ON REVERSE OUTFALL 001 ITEM V- B CONTINUED FROM FRONT POLLUTANT b. MAXIMUM 30 DAY VALUE AND a b CAS NO. BELIEVED BELIEVED javadable) PRESENT ABSENT 4. UNITS 3. EFFLUENT 2. MARK" X" 1. a. MAXIMUM DAILY VALUE ijavadable) AVERAGE VALUE ifavadable) 1 CONCENTRATION ( 2) MASS CONCENTRATION ( 5. INTAKE( optronan a. LONG TERM c. LONGTERM AVRG. VALUE 2) MASS CONCENTRATION ( 2) MASS d. NO. OF a. CONCEN- ANALYSES TRATION b. MASS 1 mg/ L lb. 36 mg/ L b. NO. OF 1 CONCENTRATION ( 2) MASS ANALYSES n/ a n/ a n/ a lb. n/ a n/ a n/ a g. Nitrogen, Total Organic( M 1. asX h. Oil and 5. Grease i Phosphorus 9. 9 016 50. 6 0 5. 2 42. 5 0. 26 1. 87 ` as P), Total X 7723- 14- 0) 12. 4 121. 0 1 mg/ L lb. n/ a n/ a n/ 1083 10568 1 mg/ L lb. n/ a n/ a n/ a 1 mg/ L lb. n/ a n/ a n/ a a I. Radioactivity X 1) Alpha, Total 2) Beta, Total X 3) Radium, Total 4) Radium 226, x Total k. Sulfate assn,) 14808- 79- 8) I. Sulfide x( as S) m. Sulfite as S03) y 14265- 45- 3) X 3. 07 TotalX 7429- 90- 5) 0. 19 1. 9 1 mg/ L lb. n/ a n/ a n/ a 0. 28 2. 1 mg/ L lb. n/ a n/ a n/ a 22. 1 1 mg/ L lb. n/ a n/ a n/ a 0. 1 mg/ L lb. n/ a n/ a n/ a n. Surfactants 30. 0 o. Aluminum, p. Barium, Total 7440- 39- 3) q. Boron, Total 7440. 42- 8) r. Cobalt, Total x( 7440- 48- 4) s. Iron, Total 7439- 89- 6) \/ \ 7 I. Magnesium, Total 2. 26 7439- 95-4) u. Molybdenum, Total 7439- 98- 7) X v. Manganese, Total 0. 005 < 049 7439- 96- 5) w. Tin, Total 7440- 31- 5) x. Titanium, Total u 7440-32- 6) EPA Form 3510- 2C( 8- 90) PAGE V- 2 CONTINUE ON PAGE V- 3 OUTFALL 001 EPA I. D. NUMBER( copyfromltem I ofForm 1) NCD CONTINUED FROM PAGE 3 OF FORM 2- C 047 368 642 OUTFALL NUMBER 001 PART C- If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/ MS fractions you must test for. Mark" X" in column 2- a for all such GC/ MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2- a( secondary industries, nonprocess wastewater outfalls, and nonrequired GC/MS fractions), mark" X" in column 2- b for each pollutant you know or have reason to believe is present. Mark" X" in column 2- c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolem, acrylonitrile, 2, 4 dinitrophenol, or 2- methyl- 4, 6 dmitrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part, please review each carefully Complete one table( all 7 pages) for each outfall See instructions for additional details and requirements. POLLUTANT b AND a b C. CAS NUMBER TESTING BELIEVED BELIEVED REQUIRED PRESENT ABSENT ifavailable) MAXIMUM 30 DAY VALUE a. MAXIMUM DAILY VALUE ( 2) MASS CONCENTRATION 1) ( AVERAGE VALUE VALUE( ifavaifable) 1) CONCENTRATION ( a. LONG TERM c. LONG TERM AVRG. rfavadable) 1) 5. INTAKE( opuona( 4. UNITS 3. EFFLUENT 2. MARK" X" 1. 2) MASS CONCENTRATION ( 2) MASS d. NO. OF a. CONCEN- ANALYSES TRATION b MASS b NO. OF 1) CONCENTRATION ( 2) MASS ANALYSES METALS, CYANIDE, AND TOTAL PHENOLS 1 M. Antimony, Total 7440- 36- 0) 2M. Arsenic, Total 7440- 38- 2) 3M Beryllium, Total 7440- 41- 7) 4M. Cadmium, Total 7440- 43- 9) X 5M. Chromium, Total( 7440- 47- 3) 6M. Copper, Total 7440- 50- 8) 7M. Lead, Total 7439- 92- 1) 8M Mercury, Total 7439- 97- 6) 9M. Nickel, Total 7440- 02- 0) 10M. Selenium, Total( 7782- 49- 2) 11 M Silver, Total 7440- 22- 4) 12M Thallium, Total( 7440- 28- 0) 13M. Zinc, Total 7440- 66- 6) 0. 002 < 0. 020 1 mg/ L lb. n/ a n/ a n/ a 0. 005 < 0. 049 1 mg/ L lb. n/ a n/ a n/ a 0. 001 < 0. 010 1 mg/ L lb. n/ a n/ a n/ a ' 0. 002 < 0. 020 1 mg/ L lb. n/ a n/ a n/ a 0. 010 0. 070 0. 010 0. 070 0. 007 0. 050 0. 007 0. 050 0. 003 0. 0002 15M. Phenols, Total 0. 004 0. 034 4 mg/ L lb. n/ a n/ a n/ a 0055 0. 047 4 mg/ L lb. n/ a n/ a n/ a < 0. 029 1 mg/ L lb. n/ a n/ a n/ a < 0. 002 1 mg/ L lb. n/ a n/ a n/ 4 mg/ L lb. n/ a n/ a n/ a 0. 0. 012 090 0. 012 0. 090 0. 0083 0. 065 a 0. 005 < 0. 049 1 mg/ L lb. n/ a n/ a n/ a 0. 002 < 0. 020 1 mg/ L lb. n/ a n/ a n/ a 0. 005 < 0. 049 1 mg/ L lb. n/ a n/ a n/ a 4 mg/ L lb. n/ a n/ a n/ a n/ a 0. 0. 390 042 14M. Cyanide, Total( 57- 12- 5) 0. 0. 0. 0. 042 0. 390 0. 0343 0. 286 005 < 0. 049 1 mg/ L lb. n/ a n/ a 0400 < 0. 390 1 mg/ L lb. n/ a n/ a I n/ a DIOXIN 2, 3, 7, 8- Tetra- DESCRIBE RESULTS Not applicable chlorodibenzo- P- Dioxin( 1764- 01- 6) EPA Form 3510- 2C( 8- 90) PAGE V- 3 CONTINUE ON REVERSE OUTFALL 001 CONTINUED FROM THE FRONT POLLUTANT AND a. b CAS NUMBER TESTING BELIEVED BELIEVED REQUIRED PRESENT ABSENT favadable) GC/ MS FRACTION- c C. LONG TERM AVRG. ( favailable) VALUE( rfavadable) d. NO. OF a. CONCEN- ANALYSES TRATION b. MASS 1 mg/ L lb. 098 1 mg/ L 10 1 1) 1) 1) CONCENTRATION ( a. LONG TERM AVERAGE VALUE 2) MASS CONCENTRATION ( 2) MASS CONCENTRATION ( 2) MASS b. NO OF 1) 2) MASS ANALYSES n/ a n/ a n/ a lb. n/ a n/ a n/ a mg/ L lb. n/ a n/ a n/ CONCENTRATION ( VOLATILE COMPOUNDS 1V. Accrolein 0. 0500 107- 02- 8) 2V. Acrylonitrile b. MAXIMUM 30 DAY VALUE a. MAXIMUM DAILY VALUE 5. INTAKE( ophnna 4. UNITS 3 EFFLUENT 2. MARK" X" 1. / 0. 0100 107- 13- 1) < 0. 488 < 0. 3V. Benzene 0. 00100 < 0. a 4V. Bis( Chloro- medrv() Ether X 542- 88- 1) 5V. Bromoform 75- 25- 2) ired Not Req per NCDWR NPDES Permitt' g Unit 0. 00100 < 0. 10 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 10 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 10 1 mg/ L lb. n/ a n/ a n/ a 0. 10 1 mg/ L lb. n/ a n/ a n/ a 049 1 mg/ L lb. n/ a n/ a n/ a 0. 488 1 mg/ L lb. n/ a n/ a n/ a 0. 049 1 mg/ L lb. n/ a n/ a n/ a 10 1 mg/ L lb. n/ a n/ a n/ a 049 1 mg/ L lb. n/ a n/ a n/ a Carbon TetrachlorideX Te 56- 23- 5) 7V. Chlorobenzene 108- 90- 7) 8V. Chlorodi- bromomethane x 0. 00100 0. 00500 < 124- 48- 1) 9V. Chloroethane / 75- 00- 3) < 0. 10V. 2- Chloroethylvinyl Ether 0. 0500 < 110- 75- 8) 11 V. Chloroform \ 67- 66- 3) 0. 00500 < 0. 00100 0. 00500 0. 00100 < 0. 10 1 mg/ L lb. n/ a n/ a n/ o. 00100 < 0. 10 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 0. 10 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 10 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 10 1 mg/ L lb. n/ a n/ a n/ 0. 00100 < 0. 10 1 mg/ L lb. n/ a n/ a n/ a 0. 00500 < 0. 049 1 mg/ L lb. n/ a n/ a n/ a 0. 00250 < 0. 024 1 mg/ L lb. n/ a n/ a n/ a 12V. Dichloro- bromomethaneX 75- 27- 4) < 0. 13V. Dichlorodifluoromethane X 75- 71- 8) 14V. 1, 1- Dichloroethane( 75- 34- 3) 15V. 1, 2- Dichloroethane( 107- 06- 2) 16V. 1, 1- Dichloro- ethylene( 75- 35- 4) 17V. 1, 2- Dichloro- / propane( 78- 87- 5) ^ < < 0. a 18V. 1, 3- Dichloropropylene X a 542-75- 6) 19V Ethylbenzene 100-41- 4) 20V Methyl Bromide( 74- 83- 9) 21V. Methyl Chlonde( 74- 87- 3) EPA Form 3510- 2C( 8- 90) PAGE V-4 CONTINUE ON PAGE V- 5 OUTFALL 001 CONTINUED FROM PAGE V- 4 POLLUTANT AND a. CAS NUMBERTESTING REQUIRED ifavailable) GC/ MS FRACTION- b e BELIEVED BELIEVED PRESENT 4. UNITS 3. EFFLUENT 2. MARK" X" 1 ABSENT a MAXIMUM DAILY VALUE ( b. MAXIMUM 30 DAY VALUE javailoble) CONCENTRATION ( 2) MASS CONCENTRATION ( 1) 2) MASS AVERAGE VALUE VALUE( javadable) 1) 1) 5. INTAKE( opaonan a. LONG TERM c. LONG TERM AVRG. d. NO. OF CONCENTRATION ( 2) MASS ANALYSES a CONCEN- b. NO. OF 1) TRATION b MASS CONCENTRATION ( 2) MASS ANALYSES VOLATILE COMPOUNDS( conunuern 22V. Methylene Chloride( 75. 09- 2) 0. 00500 < 0. 049 1 mg/ L lb. n/ a n/ a n/ 0. 00100 < 0. 010 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 010 1 mg/ L lb. n/ a n/ a n/ a 0. 00500 < 0. 049 1 mg/ L lb. n/ a n/ a n/ 0. 00100 < 0. 010 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 010 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 010 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 010 1 mg/ L lb. n/ a n/ a n/ a 0. 00500 < 0. 049 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 010 1 mg/ L lb. n/ a n/ a n/ a 0. 098 1 mg/ L lb. n/ a n/ a n/ a a 23V. 1' 1' 2' 2- X Tetraclrethane 79- 34- 5 24V. Tetrachloroethylene( 127- 18- 4) 25V Toluene Xx 108- 88- 3) a 26V. 1, 2- Trans- DichloroethyleneX 156 60- 5 27V. 1, 1, 1- Trichloroethane( 71- 55- 6) 28V / / 1, 1, 2- Trichloro- ethane( 79- 00- 5) 29VTrichloro- ethylene( 79- 01- 6) 30V. Trichloro- fluoromethaneX 75- 9- 4 31V. Vinyl Chloride 75- 01- 4) GC/ MS FRACTION- ACID COMPOUNDS 1A. 2- Chlorophenol 95- 57- 8) 2A. 2, 4- Dichlorophenol( 120- 83-2) 3A. 2, 4- Dimethylphenol( 105- 67- 9) 4A. 4, 6- Dinitro- 0Cresol( 534-52- 1) 5A. 2, 4- Dinitro- phenol( 51- 28- 5) 6A. 2- Nitrophenol 88- 75- 5) 7A. 4- Nilrophenol 100- 02- 7) BA. P- Chloro- MCresol( 59- 50. 7) 9A Pentachlorophenol( 87- 86- 5) 10A. Phenol 108- 95- 2) 1IA. 2, 4, 6- Trichlorophenol( 88- 05- 2) X EPA Form 3510- 2C( 8- 90) 0. 0100 < 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 098 1_ mg/ L lb. PAGE V- 5 n/ a n/ a n/ a CONTINUE ON REVERSE r OUTFALL 001 CONTINUED FROM THE FRONT POLLUTANT AND CAS NUMBER TESTING BELIEVED BELIEVED favailable) REQUIRED PRESENT ABSENT a. GC/ MS FRACTION- b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. fm•ailable) VALUE( favarlable) a MAXIMUM DAILY VALUE C. ( 1) 1) CONCENTRATION ( 2) MASS CONCENTRATION 1) ( 2) MASS CONCENTRATION ( 2) MASS a. LONG TERM AVERAGE VALUE d. NO. OF a. CONCEN- ANALYSES TRATION b. MASS b NO. OF 1) CONCENTRATION ( 2) MASS ANALYSES BASE/ NEUTRAL COMPOUNDS 1 B. Acenaphthene 8332- 9) 2B. Acenaphtylene 208- 96- 8) 3B. Anthracene b 5. INTAKE( opaonal 4. UNITS 3. EFFLUENT 2. MARK" X" 1 / 120- 12- 7) Benzidine X 92- 87- 5) 92 0. 00100 < 0. 01 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 01 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 01 1 mg/ L lb. n/ a n/ a n/ a 098 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 5B. Benzo( a) Anthracene X 56- 55- 3) 6B Ben( 32- 8) Pyrene( 50- 3X 0. 00100 < 0. 01 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 01 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 01 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 01 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 01 1 mg/ L lb. n/ a n/ a n/ a 7B. 3, 4- Benzofluoranthene 205- 99- 2) 8B. Benzo( glu) / Perylene( 191- 24- 2) 9B ^ Benzo( k) FluorantheneX 207- 08- 9) 10B. Bis( 2- Chlnm- erhnxv) Methane / 111- 91- 1) x 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 00300 < 0. 029 1 mg/ L lb. n/ a n/ a n/ a < 0. 098 1 mg/ L lb. n/ a n/ a n/ a < 0. 029 1 mg/ L lb. n/ n/ a n/ a 01 1 mg/ L lb. n/ a n/ a n/ a 09B 1 mg/ L lb. n/ a n/ a n/ a 11 B. Bis( 2- ChlamedryoEther 111- 44- 4) 12B. Bis( 2Chlororsopropyf Ether( 102- 80- 1) 13B. Bis( 2- Edtr1- heron Phthalate 0. 117- 81- 7) 14B 4- Bromophenyl Phenyl Ether 0. 0100 101- 55- 3) 15BButyl Benzyl Phthalate( 85- 68- 7) x 0. X 0. 00100 00300 a 16B. 2- Chloronaphthalene 91- 58- 7) < 0. 17B. 4- Chlorophenyl Phenyl Ether 0. 0100 7005-72- 3) 18B Chrysene 218- 01- 9) < 0. 0. 00100 < 0. 01 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 01 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 01 1 mg/ L lb. n/ a n/ a n/ a 0.0. 00100<00100 < 0. 01 1 mg/ L lb. n/ n/ a n/ a 19B Dibenzo( a,h) Anthracene 5370-3) X 20B. 1, 2- Dichlorobenzene( 95- 50- 1) 21 B. 1, 3- Di- chlorobenzene( 541- 731) x EPA Form 3510- 2C( 8- 90) PAGE V- 6 a CONTINUE ON PAGE V-7 OUTFALL 001 CONTINUED FROM PAGE V-6 b. MAXIMUM 30 DAY VALUE AND CAS NUMBER favarlable) a. b. c TESTING BELIEVED BELIEVED REQUIRED PRESENT ABSENT GC/ MS FRACTION- ( CONCENTRATION ( x 246. Diethyl 2) MASS CONCENTRATION 1) ( 2) MASS CONCENTRATION ( 2) MASS AVERAGE VALUE d. NO. OF a. CONCEN- ANALYSES TRATION b. MASS b. NO. OF 1) CONCENTRATION ( 2) MASS ANALYSES 00100 < 0. 001 1 mg/ L lb. n/ a n/ a n/ a 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 0. 00300 < 0. 029 1 mg/ L lb. n/ a n/ a n/ a 0. 00300 < 0. 029 1 mg/ L lb. n/ a n/ a n/ a 0. 00300 < 0. 029 1 mg/ L lb. n/ a n/ a n/ a 0. benzene( 106-46- 7) / 1) 1) a. LONG TERM c. LONG TERM AVRG. VALUE( favarlable) BASE/ NEUTRAL COMPOUNDS( co» unuee 22B. 1, 4- Dichloro- 236. 3, 3- Dichlorobenzidine( 91- 94- 1) favarlable) a. MAXIMUM DAILY VALUE 5 INTAKE( opnonan 4. UNITS 3 EFFLUENT 2. MARK" X" 1. POLLUTANT v Phthalate( 84- 66- 2) 0. 25B. Dimethyl Phthalate 131- 11- 3) 26B. Di- N- Butyl Phthalate( 84- 74- 2) 276. 2, 4- Dinitrotoluene( 121- 14- 2) 288. 2, 6- Dinitrotoluene( 606- 20- 2) 29B. Di- N- Octyl 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 0. 029 1 mg/ L lb. n/ a n/ a n/ a 0. 098 1 mg/ L lb. n/ a n/ a n/ a 0. Phthalate( 117- 84- 0) 00300 < 308. 1, 2- Diphenylhydrazine( as Azo- 0. benzene)( 1 22- 66- 7) 31B Fluoranthene 206- 44- 0) \/ x 32B. Fluorene 86- 73- 7) 33B. Hexachlorobenzene( 118- 74- 1) 34B. Hexachlorobutadiene( 87- 68- 3) 0100 < 0. 00100 < 0. 001 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 001 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 001 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 09B 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ < 0. 001 1 mg/ L lb. n/ a n/ a n/ a 0. 098 1 mg/ L lb. n/ a n/ a n/ a < 0. 001 1 mg/ L lb. n/ a n/ a n/ a < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 35B. Hexachlorocyclopentadiene 77- 47- 4) 36BHexachloro- ethane( 67- 72- 1) a 37B. Indeno 1, 2, 3- cd) Pyrene 0. 00100 193- 39- 5) 38B Isophorone 0. 78- 59- 1) 39B. NaphthaleneV 91- 20 3) x 40B. Nitrobenzene 98- 95- 3) 0. 0100 00100 c0. 0100 < 41B. N- Nitrosodimethylammeu 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 62- 75- 9) 42B. N- Nitrosodi- N- Propylamineu 621- 64- 7) EPA Form 3510- 2C( 8- 90) PAGE V- 7 CONTINUE ON REVERSE OUTFALL 001 CONTINUED FROM THE FRONT 2 1. 3 MARK" X" POLLUTANT AND CAS NUMBER favailable) a b TESTING BELIEVED BELIEVED REQUIRED PRESENT ABSENT GC/ MS FRACTION- c 4. UNITS EFFLUENT b MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. favmlable) VALUE( favailable) a. MAXIMUM DAILY VALUE 1 1 1 CONCENTRATION ( 2) MASS CONCENTRATION ( 2) MASS CONCENTRATION ( 2) MASS 5 INTAKE( opaonan a. LONG TERM AVERAGE VALUE d. NO. OF a. CONCEN- ANALYSES TRATION b. MASS b. NO. OF 1 CONCENTRATION ( 2) MASS ANALYSES BASEINEUTRAL COMPOUNDS( continuer!) 43B. N- Nitrosodiphenylamine 0. 0100 < 0. 098 1 mg/ L lb. n/ a n/ a n/ a 86- 30- 6) 44B Phenanthrene 8501- 8) 4 X 129s- 00-oo- 0)o> 0. 00100 < 0. 001 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 001 1 mg/ L lb. n/ a n/ a n/ 098 1TMg/ L lb. n/ a n/ a n/ a a 4(6B. 1, 2, 4- Trichlorobenzene 120- 82- 1) X GC/ MS FRACTION- PESTICIDES 1P. Aldrin 309- 00- 2) 2P. cc- BHC 319- 84- 6) 3P. p- BHC 319- 85- 7) 4Py-BHC 58- 89- 9) 5P. 5- BHC 319- 86- 8) 6P. Chlordane 57- 74- 9) 7P. 4,4'- DDT 50- 29- 3) 8P. 4,4'- DDE 72- 55- 9) 9P. 4,4'- DDD 72- 54- 8) 0. 0100 < 0. 0. 000050 < 5e- 4 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 5e- 4 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 5e- 4 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 5e- 4 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 5e- 4 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 0. 005 1 mg/ L lb. n/ a n/ a n/ 0. 000050 < 5e- 4 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 5e- 4 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 5e- 4 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 5e- 4 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 5e- 4 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 5e- 4 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 5e- 4 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 5e- 4 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 5e- 4 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 5e- 4 1 mg/ L lb. n/ a n/ a n/ 10P. Dieldrin 60- 57- 1) v 11 P. a- Enosulfan 11529-7) 12P.( 3- Endosulfan 11529- 7) 13P Endosulfan Sulfate 1031- 07- 8) 14P a Endrin 72- 20- 8) 15P. Endrin Aldehyde 7421- 93- 4) 16P. Heptachlor / 76-44- 8) EPA Form 3510- 2C( 8- 90) PAGE V- 8 a CONTINUE ON PAGE V- 9 OUTFALL 001 EPA I D. NUMBER( convfroin hem I ofPorm 1) NCD 047 368 OUTFALL NUMBER 642 001 CONTINUED FROM PAGE V- 8 AND CAS NUMBER favarlable) GC/ MS FRACTION- 4 3. EFFLUENT 2. MARK" X" 1. POLLUTANT a p TESTING BELIEVED BELIEVED REQUIRED PRESENT ABSENT e a. MAXIMUM DAILY VALUE ( 2) MASS 1) ( a. LONG TERM AVERAGE VALUE VALUE( favailable) i/ available) CONCENTRATION 5. INTAKE( opnonan UNITS c. LONG TERM AVRG. 1) 1) CONCENTRATION ( I b MAXIMUM 30 DAY VALUE 2) MASS CONCENTRATION ( 2) MASS d. NO. OF a. CONCEN- ANALYSES TRATION b. MASS 1 mg/ L lb. b. NO. OF 1) 2) MASS ANALYSES n/ a n/ a n/ a CONCENTRATION ( PESTICIDES( conHnueeI 17P. Heptachlor Epoxide 0. 000050 < 5e- 4 1024- 57- 3) 18P. PCB- 1242 53469-21- 9) 19P. PCB- 1254 11097- 69- 1) 20P. PCB- 1221 11104- 28- 2) 21P. PCB- 1232 11141- 16- 5) 0. 000500 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0. 000500 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0. 000500 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0.0. 000500<000500 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0.0. 000500<000500 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0. 000500 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0. 000500 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0. 000500 < 0. 1 mg/ L lb. n/ a n/ a n/ a 22P. PCB- 1248 12672- 29- 6) 23P. PCB- 1260 11096- 82- 5) 24P. PCB- 1016 12674- 11- 2) x X 25P. Toxaphene 8001- 352) EPA Form 3510-2C( 8- 90) 005 PAGE V- 9 r OUTFALL 002 PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information FEPA I. D. NUMBER( copvfrom/ fern/ ofForm/) on separate sheets( use the same format) instead of completing these pages. SEE INSTRUCTIONS. NCD 047 0 V. INTAKE AND EFFLUENT CHARACTERISTICS( continued from page 3 of Form 2- C) 368 642 OUTFALL NO. M 002 PART A- You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details. 4. INTAKE 3. UNITS 2. EFFLUENT a. MAXIMUM DAILY VALUE CONCENTRATION a. Biochemical Oxygen 3. Demand( BOD) b. Chemical Oxygen Demand( COD) c. Total Organic Carbon TOCK AVERAGE VALUE ifavadable) ijavadable) ( CONCENTRATION 2) MASS 762. 1 9 3. ( 2) MASS 9 1) CONCENTRATION ( 1. 4 762. 1 33. 7 ( 4. 37 a. CONCEN- 2) MASS TRATION b. MASS CONCENTRATION 185. 7 12 mg/ L lb. n/ a n/ a n/ a 458. 6 12 mg/ L lb. n/ a n/ a n/ a e. Ammonia( as N) 1135 1 mg/ L lb. n/ a n/ a n/ a 10. 6 939. 7 1 mg/ L lb. n/ a n/ a n/ a 0. 410 36. 3 1 mg/ L lb. n/ n/ a n/ a 1095 MGD MGD 4898 18. 22. 0 14. 8 33. MINIMUM 6. 11 MAXIMUM 8. 16 MINIMUM n/ a C 188 1 30. 0 31. 1 0 n/ a n/ a n/ a n/ a n/ a VALUEVALUE VALUE VALUE swnmer) a n/ VALUEVALUE VALUE VALUE pH 14. 556 26. 813 791 a VALUE VALUE VALUE 34. hinter) i. ANALYSES 12. 8 VALUE h Temperature 2) MASS ( 4898 f. Flow g. Temperature 1 33. 7 d. Total Suspended Solids( 7-SS) S b. NO. OF d. NO OF ANALYSES 1 t POLLUTANT a. LONG TERM c LONGTERM AVRG. VALUE b. MAXIMUM 30 DAY VALUE 1. opuanaO specffvffblank) 190 C 647 STANDARD UNITS MAXIMUM n/ a Mark" X" in column 2- a for each pollutant you know or have reason to believe is present Mark" X" In column 2- b for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either PART B- directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements. b. MAXIMUM 30 DAY VALUE AND b a CAS NO. BELIEVED BELIEVED favadable) PRESENT ABSENT fmadable) 1) 1) 1) CONCENTRATION ( 2) MASS CONCENTRATION ( a. LONG TERM AVERAGE VALUE c. LONG TERM AVRG VALUE favadable) a. MAXIMUM DAILY VALUE 5. INTAKE( opuonal) 4. UNITS 3. EFFLUENT 2 MARK" X" 1. POLLUTANT 2) MASS CONCENTRATION ( 2) MASS d. NO. OF a. CONCEN- ANALYSES TRATION b MASS b. NO. OF 1) CONCENTRATION ( 2) MASS ANALYSES a. Bromide 24959-67- 9) b. Chlorine, Total Residual C. Color d Fecal Coliform / X X X 0. 14 12. 4 1 mg/ L lb. n/ a n/ a n/ a 27 n/ a 1 PCU n/ a n/ a n/ a n/ a n/ a 1 col/ dL n/ a n/ a n/ a n/ a 1783 12 mg/ L lb. n/ a n/ a n/ a 127. 5 36 mg/ L lb. n/ a n/ a n/ a 2 est. I e. Fluoride 16984- 48- 8) \ f. Nrtrate- Nitnte as N) EPA Form 3510- 2C( 8- 90) 35. 1 2. 4 4110 35. 1 442. 9 2. 4 4110 442. 9 17. 3 1. 04 PAGE V- 1 CONTINUE ON REVERSE OUTFALL 002 ITEM V- B CONTINUED FROM FRONT b. MAXIMUM 30 DAY VALUE AND a b. CAS NO. BELIEVED BELIEVED favndable) PRESENT ABSENT g. Nitrogen, 4. UNITS 3. EFFLUENT 2. MARK" X" 1. POLLUTANT AVERAGE VALUE fnrndable) favadable) a. MAXIMUM DAILY VALUE b. NO. OF d NO. OF a. CONCEN- ANALYSES TRATION b. MASS 32. 1 1 mg/ L lb. 422 1 mg/ L 36 1 1 CONCENTRATION ( 5. INTAKE( optionao a. LONG TERM c. LONGTERM AVRG. VALUE 2) MASS CONCENTRATION ( 2) MASS CONCENTRATION ( 2) MASS 2) MASS ANALYSES n/ a n/ a n/ a lb. n/ a n/ a n/ a mg/ L lb. n/ a n/ a n/ a CONCENTRATION ( \/ X Total Organic( as 0. 362 M h. Oil and Grease i. Phosphorus as P), Total 4. 76 1. 2 \/ X 154 1. 2 154 0. 8 85. 8 7723- 14- 0) 1. Radioactivity X 1) Alpha, Total 2) Beta, Total X 3) Radium, Total 4) Radium 226, Total k. Sulfate also,) 14808- 79- 8) X 105 9309 1 mg/ L lb. n/ a n/ a n/ a 0. 552 48. 9 1 mg/ L lb. n/ n/ a n/ a I. Sulfide ar m. Sulfite X SN 14265- 45- 3) n. Surfactants X a o. Aluminum, 1. 27 112. 6 1 mg/ L lb. n/ a n/ a n/ a 1. 15 102. 0 1 mg/ L lb. n/ a n/ a n/ a Total2. 26 200. 4 1 mg/ L lb. n/ a n/ a n/ a 6. 12 1 mg/ L lb. n/ a n/ a n/ TotalX 7429- 90- 5) p. Barium, Total 7440.39- 3) n q Boron, Total 7440-42- 8) r. Cobalt, Total 7440-48- 4) x( s Iron, Total 7439-89- 6) L Magnesium, 7439-95-4) u. Molybdenum, Total 7439- 98- 7) v. Manganese, Total0. 069 7439- 96- 5) w. Tin, Total a v 7440- 31- 5) x. Titanium, Total 7440-32- 6) EPA Form 3510- 2C( 8- 90) X PAGE V- 2 CONTINUE ON PAGE V-3 OUTFALL 002 EPA LD. NUMBER( copy from lrem l ofh-onn 1) NCD CONTINUED FROM PAGE 3 OF FORM 2- C 047 368 642 OUTFALL NUMBER 002 PART C- If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/ MS fractions you must test for. Mark" X" in column 2- a for all such GC/ MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a( secondary industries, nonprocess wastewater outfalls, and nonrequued GC/MS fractions), mark" X" in column 2- b for each pollutant you know or have reason to believe is present. Mark" X" in column 2- c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater If you mark column 2b for acrolein, acrylonitrile, 2, 4 dinitrophenol, or 2- methyl4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to be discharged Note that there are 7 pages to this part, please review each carefully Complete one table( all 7 pages) for each outfall. See instructions for additional details and requirements. POLLUTANT b. MAXIMUM 30 DAY VALUE AND b c TESTING BELIEVED BELIEVED REQUIRED PRESENT ABSENT a CAS NUMBER ifavadable) CONCENTRATION ( 2) MASS CONCENTRATION ( a. LONG TERM AVERAGE VALUE c. LONG TERM AVRG. VALUE( Ijarmlable) favadablc) a. MAXIMUM DAILY VALUE 5. INTAKE( opnonan 4. UNITS 3. EFFLUENT 2. MARK" X" 1. 2) MASS CONCENTRATION ( 2) MASS b NO OF d. NO. OF a. CONCEN- ANALYSES TRATION b MASS CONCENTRATION ( 2) MASS ANALYSES METALS, CYANIDE, AND TOTAL PHENOLS 1M. Antimony, Total 7440- 36- 0) 2M Arsenic, Total 7440- 38- 2) / X 3M. Beryllium, Total 7440- 41- 7) 4M Cadmium, Total 7440-43- 9) 5M. Chromium, Total( 7440- 47- 3) X X 6M. Copper, Total 7440- 50- 8) 7M. Lead, Total 7439- 92- 1) 8M Mercury, Total 7439-97- 6) 0. 002 < 0. 177 1 mg/ L lb. n/ a n/ a n/ a 0. 005 < 0. 443 1 mg/ L lb. n/ a n/ a n/ a 0. 001 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 002 < 0. 177 1 mg/ L lb. n/ a n/ a n/ a 0. 005 < 0. 433 1 mg/ L lb. n/ a n/ a n/ a 1 mg/ L lb. n/ a n/ a n/ a 0. 0. 7440-02- 0) 10M. Selenium, Total( 7782- 49- 2) 11 M. Silver, Total 7440- 22- 4) 12M. Thallium, Total( 7440- 28- 0) 13M. Zinc, Total 7440- 66- 6) 14M. Cyanide, 15M. Phenols, < 0. 266 1 mg/ L lb. n/ a n/ a n/ a 0. 018 1 mg/ L lb. n/ a n/ a n/ a 005 < 0. 433 1 mg/ L lb. n/ a n/ a n/ a 0. 005 < 0. 433 1 mg/ L lb. n/ a n/ a n/ a 0. 002 < 0. 177 1 mg/ L lb. n/ a n/ a n/ a 0. 005 < 0. 433 1 mg/ L lb. n/ a n/ a n/ a 1 mg/ L lb. n/ a n/ a n/ 0. 0. < 0. 0. Total( 57- 12- 5) Total 003 0. 0002 9M. Nickel, Total 0. 443 005 0. 008 005 0433 < 709 a 0. 433 1 mg/ L lb. n/ a n/ a n/ a 3. 84 1 mg/ L lb. n/ a n/ a n/ a DIOXIN 2, 3, 7, 8- Tetra- DESCRIBE RESULTS Not applicable chlorodibenzo-PDioxin( 1764- 01- 6) EPA Form 3510- 2C( 8- 90) PAGE V- 3 CONTINUE ON REVERSE OUTFALL 002 CONTINUED FROM THE FRONT 2 1 b. MAXIMUM 30 DAY VALUE AND a b TESTING BELIEVED BELIEVED REQUIRED PRESENT ABSENT CAS NUMBER javadable) GC/ MS FRACTION- c a MAXIMUM DAILY VALUE ( 1) CONCENTRATION ( 2) MASS CONCENTRATION ( a. LONG TERM AVERAGE VALUE VALUE( rfavadable) i( avadable) 1) 5. INTAKE( opnana UNITS c. LONG TERM AVRG. 1) 2) MASS CONCENTRATION ( 2) MASS d. NO. OF a. CONCEN- ANALYSES TRATION b. MASS 1 mg/ L lb. 1 mg/ L 1 b NO. OF 1) CONCENTRATION ( 2) MASS ANALYSES n/ a n/ a n/ a lb. n/ a n/ a n/ a mg/ L lb. n/ a n/ a n/ a VOLATILE COMPOUNDS 1V. Accrolein 107- 02- 8) 2V. Acrylonitrile 4 3. EFFLUENT MARK" X" POLLUTANT \/ 107- 13- 1) 3V. Benzenev 0. 0500 0. 0100 0. 71- 432) 00100 < 4. 433 < 0. 887 < 0. 089 4V. Bis( Chlom- merhyl) Ether X 542- 88- 1) 5V Bromoformv 75- 252) ired Not Req per NCDWR NPDES Permitt' g Unit 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a Carbon Tetrachloride 56- 235) 7V. Chlorobenzene \/ 108- 90- 7) x 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a x 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 8V. Chlorodibromomethane 124- 48- 1) 9V. Chloroethane X n/ a lb. n/ a n/ a 1 0. 00500 < 0. 443 mg/ L 7500-3 00- 3) 1OV. 2- ChloroethylwnylEther 0. 0500 < 4. 433 1 mg/ L lb. n/ a n/ a n/ a 110- 758) 11V. Chloroform \ 0. 0248 67- 66- 3) 2. 199 1 mg/ L lb. n/ a n/ a n/ a 0. 374 1 mg/ L lb. n/ a n/ a n/ a 12V. Dichlorobromomethane 0. 00422 7527- 4) 13V. Dichloro- difluoromethaneX 7571- 8) 14V. 1, 1- Dichloroethane( 75- 34- 3) / ^ 15V. 1, 2- Dichloro / ethane( 107- 015- 2) ^ 16V. 1, 1- Dichloroethylene( 7535-4) 17V. 1, 2- Dichloro- / propane( 78- 87- 5) ^ 0. 00500 < 0. 443 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ 0. 00500 < 0. 443 1 mg/ L lb. n/ a n/ a n/ a 0. 00250 < 0. 222 1 mg/ L lb. n/ a n/ a n/ a a a 18V. 1, 3Dichloro- propylenex 542- 756) 19V. Ethylbenzene 100- 41- 4) \/ x 20V Methyl Bromide( 74- 83- 9) 21V. Methylu Chloride( 74- 87- 3) EPA Form 3510- 2C( 8- 90) PAGE V- 4 a CONTINUE ON PAGE V- 5 OUTFALL 002 CONTINUED FROM PAGE V- 4 AND CAS NUMBER ijavadable) GC/ MS FRACTION- b. MAXIMUM 30 DAY VALUE a b, c TESTING BELIEVED BELIEVED REQUIRED PRESENT ABSENT a. MAXIMUM DAILY VALUE CONCENTRATION ( 2) MASS rjava(ab( e) CONCENTRATION ( 2) MASS 5 INTAKE( opaonan 4. UNITS 3. EFFLUENT 2. MARK" X" 1. POLLUTANT a. LONG TERM AVERAGE VALUE C. LONG TERM AVRG. VALUE( javadable) CONCENTRATION ( 2) MASS b. NO OF d. NO. OF a. CONCEN- ANALYSES TRATION b. MASS CONCENTRATION ( 2) MASS ANALYSES VOLATILE COMPOUNDS( conanuec) 22V. Methylene Chloride( 75- 09- 2) 0. 00500 < 0. 443 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00500 < 0. 443 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00500 < 0. 443 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 23V. 1, 1, 2, 2- TetrachloroethaneX 7934-5 24V. Tetrachloroethylene( 127- 18- 4) 25V. Toluene 10& 88- 3) 26V. 1, 2- Trans- DichloroethyleneX 156- 60- 5 27V. 1, 1, 1- Trichloroethane( 71- 55- 6) 28V. 1, 1, 2- Trichloroethane( 79- 00- 5) X X 29VTrichloro- ethylene( 79- 01- 6) 30V. Trichloro- fluoromethaneX 75- 69-4 31V. Vinyl Chloride 75- 01- 4) GC/ MS FRACTION- ACID COMPOUNDS 1A. 2- Chlorophenol 95- 57- 8) 2A 2,4- Dichloro- phenol( 120- 83- 2) 3A. 2, 4- Dimethylphenol( 105- 67- 9) 4A. 4,6- Dinitro- 0Cresol( 534- 52- 1) 5A. 2, 4- Dinitrophenol( 51- 28- 5) 6A. 2- Nitrophenol 88- 75- 5) 7A. 4- Nitrophenol 100- 02- 7) SA. P- Chloro- MCresol( 59- 50- 7) 9A Pentachlorophenol( 87- 86- 5) X 10A. Phenol 10B- 95- 2) 11 A. 2, 4, 6- Trichlorophenol( 88- 05- 2) X EPA Form 3510- 2C( 8- 90) 0. 0100 < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 0. 887 1 mg/ L lb. n/ a n/ a n/ 0. 0100 < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 887' 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 887 1 mg/ L lb. < PAGE V- 5 n/ a n/ a a n/ a CONTINUE ON REVERSE OUTFALL 002 CONTINUED FROM THE FRONT POLLUTANT b. MAXIMUM 30 DAY VALUE AND a. b C. CAS NUMBER TESTING BELIEVED BELIEVED lava! able) REQUIRED PRESENT ABSENT GC/ MS FRACTION- 1 1 1 CONCENTRATION ( 2) MASS CONCENTRATION ( 2) MASS a. LONG TERM c. LONG TERM AVRG. VALUE favai hl") CONCENTRATION ( 2) MASS AVERAGE VALUE d. NO. OF a. CONCEN- ANALYSES TRATION b MASS b NO. OF 1 CONCENTRATION ( 2) MASS ANALYSES BASE/ NEUTRAL COMPOUNDS 1B. Acenaphthene 83- 32- 9) 2B. Acenaphtylene fm adable) a. MAXIMUM DAILY VALUE 5 INTAKE( opuonan 4. UNITS 3. EFFLUENT 2. MARK" X" 1. / 208- 96- 8) 3B. Anthracene 120- 12- 7) 4B. Benzidine 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 92- 87- 5) 5B. Benzo( a) Anthracene 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 56- 55- 3) 6B Benzo( a) Pyrene( 50- 32- 13) 7B. 3,4- Benzofluoranthene 205- 99- 2) 8B. Benzo( ghi) / Perylene( 191- 24- 2) ^ 9B. Benzo( k) Fluoranthene 207- 08- 9) 10B. Bis( 1- Chloro- erhoxy) Methane 111- 91- 1) 11B 0. 0100 < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 0. 887 1 mg/ L lb. n/ a n/ a n/ a Bis( 2- Ch( om- erhi,n Ether 111- 44- 4) 12B. Bis( 1- Chloro,soprowQ < Ether( 102- 80- 1) 13B. Bis( 2- Erhvlhex,0Phthalate 00300 < 0. 266 1 mg/ L lb. n/ a n/ a n/ a 0100 < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. 00300 < 0. 266 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 117- 81- 7) 14B. 4- Bromophenyl Phenyl Ether 101- 55- 3) 15B 0. Butyl Benzyl Phthalate( 85- 68- 7) 16B. 2- Chloro- X naphthalene 91- 58. 7) 17B. 4- Chlorophenyl Phenyl Ether 0100 < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ n/ a 0. 7005- 72- 3) 18B. Chrysene 218- 01- 9) 19B. Dibenzo( a,h) Anthracene 53- 70- 3) 208. 1, 2- Dchlorobenzene( 95- 50- 1) / x 21 B. 1, 3- Di- chlorobenzene( 541- 73- 1) / EPA Form 3510- 2C( 8- 90) PAGE V- 6 a a CONTINUE ON PAGE V-7 r OUTFALL 002 CONTINUED FROM PAGE V- 6 3 2. MARK" X" 1. POLLUTANT AND a b C. CAS NUMBER TESTING BELIEVED BELIEVED favadablc) REQUIRED PRESENT ABSENT GC/ MS FRACTION- CONCENTRATION ( 0. benzene( 106- 46- 7) 23B. 3, 3- Dichloro- 00100 0. benzidine( 91- 94- 1) v Diethyl favailable) I 5 INTAKE( opnonan a. LONG TERM AVERAGE VALUE c. LONG TERM AVRG. VALUE( favarlable) b NO. OF d NO OF a. CONCEN- ANALYSES TRATION b. MASS 089 1 mg/ L lb. n/ 0. 887 1 mg/ L 226 1 2) MASS CONCENTRATION ( 2) MASS CONCENTRATION ( 2) MASS 2) MASS ANALYSES a n/ a n/ a lb. n/ a n/ a n/ a mg/ L lb. n/ a n/ a n/ a CONCENTRATION ( BASE/ NEUTRAL COMPOUNDS( conanuerQ 226. 1, 4- Dichloro- 246 a. MAXIMUM DAILY VALUE 4. UNITS EFFLUENT b. MAXIMUM 30 DAY VALUE Phthalate( 84- 66- 2) 0100 < < 0. 0. 00300 < 0. 0. 00300 < 0. 226 1 mg/ L lb. n/ a n/ a n/ a 0. 00300 < 0. 226 1 mg/ L lb. n/ a n/ a n/ a 256. Dimethyl Phthalate 131- 11- 3) 26B. Di- N- Butyl Phthalate( 84- 74- 2) 27B. 2, 4- Dlnitrotoluene( 121- 14- 2) 28B. 2, 6- Dinitro- toluene( 606- 20- 2) 29B. Di- N- Octyl 0. 0100 < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. < 0. 887 1 mg/ L lb. n/ a n/ a n/ a < 0. 226 1 mg/ L lb. n/ a n/ a n/ a 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. Phthalate( 117- 84- 0) 0100 00300 30B 1, 2- Diphenylhydrazine( as Azo- 0. 0100 < benzene)( 122- 66- 7) 31B. Fluoranthene 206- 44- 0) 32B. Fluorene 86- 73- 7) 33B. Hexachlorobenzene( 118- 74- 1) 34B. Hexachloro- butadiene( 87- 68- 3) 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 0. 887 1 mg/ L lb. n/ a n/ a n/ a 089 1 mg/ L lb. n/ a n/ a n/ a 0. 887 1 mg/ L lb. n/ a n/ a n/ a 35B. Hexachloro- cyclopentadieneX 77- 47- 4) 36BHexachloro- ethane( 67- 72- 1) < 378. Indeno 1, 2,2, 3- cd) Pyrene 193- 39- 5) 0. 38B. Isophorone 0. 78- 59- 1) 39B. Naphthalene 0. 91- 20- 3) 40B. Nitrobenzene 98- 95- 3) \/ x 00100 0100 00100 < 0. < < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. 0100 < 0. 887 1 mg/ L lb. n/ a n/ a n/ a 416 N- Ndrosodimethylamine 62- 75- 9) 42B. N- NitrosodiN- Propylamine 621- 64- 7) EPA Form 3510- 2C( 8- 90) PAGE V- 7 CONTINUE ON REVERSE OUTFALL 002 CONTINUED FROM THE FRONT 3 2. MARK" X" 1. POLLUTANT AND a b. c CAS NUMBER TESTING BELIEVED BELIEVED favadable) REQUIRED PRESENT ABSENT GC/ MS FRACTION- a MAXIMUM DAILY VALUE ( CONCENTRATION ( 2) MASS 1) ( AVERAGE VALUE VALUE( favadable) ifavadable) CONCENTRATION a. LONG TERM c. LONG TERM AVRG. 1) 1) 5. INTAKE( opnona 4. UNITS EFFLUENT b. MAXIMUM 30 DAY VALUE 2) MASS CONCENTRATION ( 2) MASS d. NO OF a CONCEN- ANALYSES TRATION b. MASS b. NO OF 1) CONCENTRATION ( 2) MASS ANALYSES BASE/ NEUTRAL COMPOUNDS( conanuetn 43B. N- Nitro- 0. 887 1 mg/ L lb. n/ a n/ a n/ a 0. 00100 < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. < 0. 089 1 mg/ L lb. n/ a n/ a n/ a 0. 887 1 mg/ L lb. n/ a n/ a n/ a 000050 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 0. 005 1 mg/ L lb. n/' a n/ a n/ a 0. 000050 < 0. 005 1 mg/ L lb. n/ a n/ a n/ 0. 000050 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 0. 044 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0. 000050 < 0. 005 1 mg/ L lb. n/ a n/ a n/ a 0. sodiphenylamineX 86- 30- 6) 44B Phenanthrene 85- 01- 8) 45B. Pyrene x 129- 00- 0) 0100 00100 < 46B. 1, 2, 4- Trichlorobenzene 0. 120- 82- 1) GC/ MS FRACTION- 0. 309- 00- 2) 2P. u.-BHC 319- 84- 6) 3P. p- BHC 319- 85- 7) x 58- 89- 9) 5P. 6- BHC 319- 86- 8) 6P. Chlordane 57- 74- 9) 7P. 4, 4'- DDT 50- 29- 3) 8P. 4,4'- DDE 72- 55-9) 9P. 4,4'- DDD 72- 54- 8) 1OP. Dieldrin 60- 57- 1) 11 P. a- Enosulfanv 115- 29-7) 12P.( 3- Endosulfan < PESTICIDES 1P. Aldrin 4P. y- BHC 0100 \ 115- 29- 7) a 13P. Endosulfan Sulfate 1031- 07- 8) 14P Endrin 72- 20. 8) 15P. Endrin Aldehydeu 7421- 93- 4) 16P. Heptachlor 76- 44- 8) EPA Form 3510- 2C( 8- 90) PAGE V- B CONTINUE ON PAGE V- 9 OUTFALL 002 EPA I. D. NUMBER( eopy,frotn Item I ojl ortn I) NCD 047 368 OUTFALL NUMBER 642 002 CONTINUED FROM PAGE V- 8 3 2. MARK" X" 1. POLLUTANT AND = c TEsaTINGD favailable) VED BELIEVED ENT ABSENT 4. UNITS EFFLUENT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. fmwailable) VALUE( favadable) a. MAXIMUM DAILY VALUE 5. INTAKE( opttonan a. LONG TERM AVERAGE d. NO. OF a. CONCEN- ANALYSES TRATION b. MASS 0. 000050 < 0. 005 1 mg/ L lb. n/ 0. ( CONCENTRATION ( 1) 1) 1) 2) MASS CONCENTRATION ( 2) MASS CONCENTRATION ( 2) MASS b NO. OF V 2) MASS ANALYSES a n/ a n/ a CONCENTRATION ( GC/ MS FRACTION— PESTICIDES( conitnuerl) 172 Heptachlor Epoxide 1024- 57- 3) ` , X 1BP. PCB- 1242 53469- 21- 9) 19P PCB- 1254 11097- 69- 1) 20P PCB- 1221 11104- 28- 2) 21 P. PCB- 1232v 11141- 16-5) 22P. PCB1248 12672- 29- 6) 000500 < 0. 044 1 mg/ L lb- n/ a n/ a n/ a 0. 000500 < 0. 044 1 mg/ L lb. n/ a n/ a n/ a 0. 000500 < 0. 044 1 mg/ L lb. n/ a n/ a n/ 0. 000500 < 0. 044 1 mg/ L lb. n/ a n/ a n/ a 0. 000500 < 0. 044 1 mg/ L lb. n/ a n/ a n/ a 0. 000500 < 0. 044 1 mg/ L lb. n/ a n/ a n/ a 0. 000500 < 0. 044 1 mg/ L lb. n/ a n/ a n/ a 0. 000500 < 0. 044 1 mg/ L lb. n/ a n/ a n/ a 23P. PCB- 1260 11096- 82- 5) 2426 PCB- 1016 1267a- 11_ 1- p)2) x 25P. Toxaphene 8001- 35- 2) EPA Form 3510- 2C( 8- 90) PAGE V- 9 a Chemours Company— Fayetteville NPDES Permit No. NC0003573 Works Supplemental Information — Permit Renewal Application — April 27, 2016 Sludge Management Plan The Chemours Company — Fayetteville Works operates a Class 3 Wastewater Treatment Plant which is comprised of a single- stage activated sludge biological system. Excess sludge is removed from the system by diverting part of the Recycled Activated Sludge ( at approximately 0. 6% solids) from the clarifiers to a Dissolved Air Floatation (" initial thickening. The sludge from the DAF( at approximately 3% solids) agents are added to enhance the dewatering process. DAF") unit for is transferred to a Mix Tank where polymer The semi- thickened sludge is transferred from the Mix Tank to a Rotary Filter for final thickening, whereby the sludge is thickened to 6% solids. The thickened sludge is then transferred to a Screw Press where it is dewatered to a concentration of 9- 20% solids. Following the Screw Press, the sludge is typically dried in steam heated dryers to a concentration of 40- 55% solids. The dried sludge, or on occasion the dewatered sludge, is transported off-site to a commercial This sludge is currently being disposed of at the Waste Industries " Sampson County" Landfill near Roseboro, NC. Subtitle D landfill. In 2015, the average weekly quantity of generated wasted sludge was approximately 35, 000 lb. Michael E. Jo Environme anager y Chemours Company— Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information — Permit Renewal Application — April 27, 2016 Current Facility Wastewater Management Process wastewater and stormwater from the various manufacturing areas are collected in the respective area sumps and ultimately conveyed via a gravity flow underground process sewer pipe to the facility' s central wastewater treatment plant (" WWTP"). Sanitary sewage is conveyed via a separate underground sewer system to the WWTP. The permitted flowrate of the WWTP is 2. 0 MGD, with an actual average flowrate of approximately 1. 2 MGD. This untreated process wastewater is commingled in the WWTP Influent Sump where it is pumped to an 850,000- gallon Equalization Basin. The Equalization Basin is mixed with two floating submerged mixers. Three floating surface aerators in the basin cool and aerate the incoming wastewater. A 175, 000- gallon Emergency Retention Tank is available for temporary storage of untreated wastewater which may need additional treatment or acclimation in the WWTP activated sludge process at a controlled rate that allows for proper biological treatment. Untreated wastewater from the Equalization Basin is normally pumped to a 250, 000- gallon Predigester Tank in which initial biological activity with the WWTP activated sludge begins. The Predigester Tank is aerated. The partially treated wastewater from the Predigester Tank is pumped to a 1, 700, 000- gallon Aeration Tank. The Aeration Tank is the unit where the majority of the biological activity occurs. The Aeration Tank is aerated primarily by a diffused air system located in the bottom of the tank. The tank can have supplemental aeration via one or two floating Biomixers® that injects air through submerged rotors. The biologically treated wastewater is then sent to one of two in-ground clarifiers( 119,000 gallons and 168, 000 gallons respectively) or an above- ground 679, 000- gallon clarifier; with all clarifiers being operated in parallel. The clarified treated effluent is discharged to and through Outfall 001. The wasted activated sludge is sent to a Dissolved Air Floatation ( DAF) unit, then to a 47, 000 gallon Sludge Storage Tank, and finally to a Rotary Filter for thickening. The thickened sludge is dewatered in a Sludge Press, and can be dried in a steam- heated dryer for additional moisture removal. The dewatered sludge or dewatered/ dried sludge is transported off-site to a commercial Subtitle D landfill. Non-contact process cooling water and non-process stormwater are conveyed via surface ditches. In addition, excess riverwater flow and Outfall 001 effluent are discharged directly to a surface ditch. The combined, total flow of water from the site is discharged through and monitored at Outfall 002. The discharged treated wastewater is conveyed via an underground pipe to the Cape Fear River, where it enters the river at a point approximately 1, 500 feet upstream of the William O. Huske Lock & Dam ( a.k.a Lock & Dam No. 3). Chemours Company— Fayetteville NPDES Permit No. NC0003573 Works Supplemental Information — Permit Renewal Application - April 27, 2016 Current Facility Operating Conditions Chemours Fluoromonomers/ Nafion® Membrane Manufacturing Area: The Chemours Company — Fayetteville Works' Fluoromonomers / Nafion® Membrane manufacturing area produces several final products. ChemoursTM Nafion® Membrane is a plastic film used in the chloroalkali industry and in electrochemical fuel cells. ChemoursTM Nafion® Polymer Dispersions are used in the fabrication of thin films and coating formulations for fuel cells membranes, catalyst coatings, The HFPO monomer and the fluorochemical products sensors, and a variety of electrochemical applications. Vinyl Ether monomers such as are ChemoursTM Teflon®. used to Wastewater manufacture various generated from this manufacturing facility is discharged to the Chemours' wastewater treatment plant. Chemours Polymer Processing Aid (" PPA") Manufacturing Area: The Chemours Company — Fayetteville Works' PPA manufacturing area produces a polymer The processing aid produced in this unit is used in the manufacturing of fluoropolymers and fluorinated telomers,, but none of the produced processing aid is used at the processing aid. All process wastewater generated from this manufacturing facility is collected and shipped off-site for disposal. No process wastewater from this manufacturing facility Fayetteville Works site. is discharged to the Chemours' wastewater treatment plant or to the Cape Fear River. Kuraray Butacite® Manufacturing Area: manufacturing area produces two final Interlayer plastic sheeting is the final product used in safety glass The Kuraray America Inc. — Fayetteville products. KurarayTM Butacite® such as automobile windshields. Plant' s Butacite® Polyvinyl butyral resin is shipped off-site as a transfer to other Kuraray locations for final processing. Wastewater generated from this manufacturing facility is discharged to the Chemours' wastewater treatment plant. Kuraray SentryGlas® Manufacturing Area: The Kuraray America Inc. — Fayetteville KurarayTM SentryGlas® Plant' s SentryGlas® manufacturing area produces SentryGlas® interlayer is used for ionoplast interlayer laminate. laminated safety glass in side, rear, and overhead automobile windows. It is also used in architectural applications desiring safety glass. There is no contact process wastewater generated from this manufacturing facility, therefore only sanitary waste from this area is treated in the Chemours' wastewater treatment plant. This manufacturing facility does discharge non- contact cooling water to a surface ditch and ultimately to Outfall 002. DuPont Polyvinyl Fluoride (" PVF") Manufacturing Area: The DuPont Company— Fayetteville Works' PVF manufacturing area produces polyvinyl fluoride resin that is used in the electronics industry as a backing for photovoltaic cells, as well as many other uses. Wastewater generated from this manufacturing facility is discharged to the Chemours' wastewater treatment plant. M Chemours Company— Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information — Permit Renewal Application — April 27, 2016 Alternate Application Schedule for §316( b) of the Clean Water Act Final regulations implementing § 316(b) of the Clean Water Act, which establish requirements for cooling water intake structures at existing facilities, were published in the Federal Register on August 15, 2014 with an effective date of October 14, 2014. The Chemours Company — Fayetteville Works (" Chemours") operates a cooling water intake structure on the Cape Fear River that is subject to this new Federal Cooling Water Intake Structure Rule (" the Rule") as codified in 40 CFR Part 125. The Rule requires' the owner or operator of a facility subject to Subpart J whose currently effective permit expires after July 14, 2018, to submit to the Director the information required in the applicable provisions of 40 CFR 122. 21( r) when applying for a subsequent permit. the owner or operator of a facility subject to Part 125 Subpart J, Requirements Applicable to Cooling Water Intake Structures for Existing Facilities Under Section 316( b) of the Clean Water Act", whose currently effective permit expires prior to July 14, Pursuant to 40 CFR 125. 95( a)( 2), 2018, may request the Director to establish an alternate schedule for the submission of the information required in 40 CFR 122. 21( r) when applying for a subsequent ( renewed) permit. On October 20, 2015, a letter was sent from Michael E. Johnson, Environmental Manager, Chemours Company — Fayetteville Works, to Dr. Sergei Chernikov, NCDEQ Division of Water Resources' NPDES Complex Permitting Unit, requesting an alternate schedule whereby all the materials required by the Rule will be submitted with the 2021 renewal application. On February 26, 2016, a letter was sent from S. Jay Zimmerman, Director, NCDEQ Division of to Michael E. Johnson, Environmental Manager, Chemours Company — Fayetteville Works, wherein the requested alternate schedule for submission of required CWIS information with the next permit renewal in 2021 was approved. A copy of Mr. Zimmerman' s Water Resources, letter is attached to this application package. PAT MCCRORY Gorcrnor DONALD R. VAN DER VAART Secretary Water Resources S. ENVIRONMENTAL QUALITY JAY ZIMMERMAN D, recmr February 26, 2016 Mr. Michael E. Johnson, P. E. Environmental Manager Chemours Company 22828 NC Highway 87 West Fayetteville, North Carolina 28306- 7332 Subject: Alternate CWA 316( b) Application Schedule NPDES Permit NC0003573 Fayetteville Works Bladen County Dear Mr. Johnson: The Clean Water Act Section 316( b) Cooling Water Intake Structure( CWIS) Final Rule outlines regulations and standards for the design and operation of cooling water intake structures under the NPDES program. Your current permit expires October 31, 2016, with renewal application due by May 4, 2016. Since your permit expires prior to July 14, 2018, under 40 CFR 125. 95( a)( 2), you have requested an alternative schedule for submission of CWIS permit application information required in 40 CFR Part 122. 21( r). Based on Division review, an alternate schedule for submission of required CWIS information with the next permit renewal in 2021 is approved. This schedule date will be established in the 2016 permit renewal as well. Please note that facilities should begin to adapt their systems to comply with CWA Section 316( b) requirements. If you have any questions, please contact Tom Belnick with the NPDES Permitting Unit at 919- 807- 6390 or via email: tom. belnick@ncdenr. gov Sing ely, S. Jay Zimmerman, P. G. Director, Division of Water Resources Cc: NPDES File Ec: US EPA Region 4 Central File US FWS NC WRC NC DWR/ Fayetteville Region State of North Carolina I Environmental Quality I Water Resources 1617 Mad Service Center I Raleigh, North Carolina 27699- 1617 919 707 9000 Chemours Company— Fayetteville NPDES Permit No. NC0003573 Works Supplemental Information — Permit Renewal Application — April 27, 2016 Elimination of Monitoring Requirement for PFOA In December 2002, the DuPont Company — Fayetteville perfluorooctanoate (" Works began production of ammonium APFO"), which is the ammonium salt of perfluorooctanoic acid (" PFOA"). The renewed NPDES Permit No. NC0003573 that became effective on July 1, 2007, included a requirement for monthly monitoring of PFOA at Outfall 002. In 2006 the North Carolina Division of Water Quality (" DWQ"), in consultation with the North Carolina Division of Waste Management and the North Carolina Department of Health and Human Services, established an Interim Maximum Allowable Concentration (" IMAC") of 2 gg/ L for PFOA, which was intended for the protection of groundwater as a source of drinking water. Following the issuance of this temporary health-based level, DWQ requested the assistance of the North Carolina Secretary' s Science Advisory Board on Toxic Air Pollutants (" NCSAB") in reviewing the toxicological literature on PFOA and recommending to DWQ an update of the IMAC for PFOA in groundwater. On August 10, 2012, the NCSAB issued their recommendation to DWQ that the IMAC for PFOA in groundwater be reduced to 1 gg/ L. During the 3- year period from 2013 to 2015, the average monthly concentration of the final effluent discharge at Outfall 002 was 0. 027 gg/ L PFOA, with a maximum concentration of 0. 088 gg/ L PFOA. During the same period, the average monthly concentration of the incoming water from the Cape Fear River to the site, which is 99% of the effluent flow at Outfall 002, was 0. 012 gg/ L PFOA, with a maximum concentration of 0.031 gg/ L PFOA. The production of APFO at this facility ceased in April 2013. The Chemours Company — Fayetteville Works ( formerly the DuPont Company — Fayetteville Works) is requesting that the monthly monitoring requirement for PFOA at Outfall 002 be eliminated in the renewed NPDES Permit No. NC0003573 for the following reasons: APFO is no longer manufactured at this facility and has not been produced at the facility since April 2013; APFO is not and has never been used as a process aid or a raw material at this facility; The 3- year average concentration at Outfall 002 was 0. 027 gg/ L PFOA, versus the current NC- DWR IMAC of 2 gg/ L PFOA and the NCSAB recommended 1 gg/ L PFOA; and PFOA is present at low concentrations throughout the Cape Fear River basin, and that background level of PFOA in the Cape Fear River water contributes to the concentration measured at Outfall 002. R J0 Chemours-Company— Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information — Permit Renewal Application — April 27, 2016 Form 2C Permit Application — Bis( chloromethyl) ether Bis( chloromethyl) ether ( CAS No. 542- 88- 1) was not analyzed for, and consequently was not reported on Page V-4 of Form 2C for both Outfall 001 and Outfall 002. On November 28, 2014, the State of Oregon' s Department of Environmental Quality (" ODEQ") issued a memorandum ( Note t) addressing the issue of analyzing for bis( chloromethyl) ether BCME"). In this memorandum, ODEQ states: Based on the chemical' s rapid hydrolysis in water, there are no analytical methods to measure BCME in water samples. Currently, the only analytical techniques available for this compound are for air samples. Region 10 EPA staff queried its Manchester Environmental Lab in Port Orchard, WA about potential, analytical methods for BCME. Staff at the lab confirmed that there is no EPA method for BCME because of its rapid degradation in water." Because of the lack of an' EPA approved analytical method for bis( chloromethyl) ether in a water matrix, ODEQ concluded: Given its rapid hydrolysis in water, there are no recommended analytical methods for BCME in water samples. Because BCME is not quantifiable in wastewater, DEQ will not require permit holders to monitor or conduct reasonable potential analyses for this toxic pollutant." In an April 13, 2106, email from Tom Belnick, Supervisor of the NCDEQ Division of Water Resources' NPDES Complex Permitting Unit, to Michael Johnson, Environmental Manager, Chemours Company— Fayetteville Works, Mr. Belnick stated: I checked with our DWR analytical lab, and they concur with Oregon' s position and are not aware of any labs using even R& D methods for this analyte. Therefore, you can omit this parameter from your application renewal." Note 1: http:// www.deq. state. or.us/ wq/standards/ docs/ toxics/ BisChloromethylMemo. pdf