OREGON OSHA Batch ID: 428 Employer/Loo: 5701115 ?010 Seq: 004 Employer Name: POLK COUNTY File Type/No: INSPECTION 317718091 No.0fPages: Comments: . ?1 1 1 01317718091004 Oregon Department of Consumers and Business Services Oregon Occupational Safety and Health Division (OR-OSHA) Inspection Report Tue Nov 28, 2017 02:02 PM 1054193 317713091(93) Polk County 820 SW Ash St Dallas, OR 97338 850 Main St Dallas, OR 97338 (503)623-9287 B. LOCAL GOVERNMENT LOCAL GOVERNMENT 5701115?010 30 4 350 237990 Referral Partial Inspection Health Manufacturing Health Yes 57770 08/22/2017 203001781 10/25/2017 1 01? 12 Todd Whittaker 22 S-22 PARC - 6 FIXED Inspection Report Page 1 of2 RECEIVED NOV 2 8' 2017 7/02) Oregon Department of Consumers and Business Services Oregon Occupational Safety and Health Division (OR-OSHA) Inspection Report Tue Nov 28, 2017 02:02 PM CSHOSIgnature WW 3' Inspection Report Page 2 of 2 OSHA- 1 (Rev. 7/02) Ii} IDEPARTMENT OF I?g?v??g OREGON OSHA INSPECTION SUPPLEMENT 1. IMIS no.2a 2. Opt no.2 \IlgaIgOlZ'qu 3. Emp. no.: 570! . Date: ?7 Time on site: 92 LI I Time out: #5770 Travel time: 92 z: $112 5. Total Inspecti time. Legal entity: Corporation Partnership l3 Sole 7. Legal name. 8. DBA: - E-mail: 9. Phone: (635%Z54983i Cell/fax: 10. Site address: 8?30 SUJ Iii?bl?) SI-DCLUQS Q7338 11. Mailing address: 965 Mm Employed in ., Covered by Employed Statewide 12. establishment: 521) inspection. in Oregon. i 13. average DART: 14. OSHA 300 Logs: year year year . 1 Hours worked each year: DART rate: Formula: 200,000 hours worked DART rate 15. Type of 16. SIC: 17. NAICS: 93,197 0 18. yan?a em nt re resentatives: . T'.tle . Opening Insp. Closing ind/II Dill". quIijm/IL 57 ma Hawk/ms ,4 II. Semi. Dame a! $0 :1 El El El 19. Employee representatives: Title El El 20. Photos taken: No Video: Yes. Audio: oftapes) 21. Workers? comp. insurance carrier: Number: 22. Union name/address: 23. Does employer lease any. employees? Yes Leasing co. name: 24. Citation copies: macaw: (S: 003% COMPLIANCE OFFICER: DATE: [Er Print name 440-1254 Department of Consumer and Business Services Oregon Occupational Safety and Health Division Referral Report Wed Aug 16, 2017 01:59 PM Reporting ID 1054193 Previous Activity Referral Number 203001781 Establishment Establishment Polk County Employer ID 5701115-010 Information Name Site Address 820 Ash St City County Dallas, Code Code Site Phone in Site Fax -- Mail Address 850 Main St Dallas, OR 97338 Mail Phone Fax . Industry Type of Business COUNTY GOVERNMENT Primary 237990 No. of 0 Ownership NAICS Employees Ownership Local Government Source Referred By State/Local Government ?Date Received 08/15/2017 Source of Contact (Name, Location, Affiliation, Telephone Number, Email) Tracie Fitzpatrick, PO Box 14360, Salem, OR, 97309, OERS, 5033786377 Referral Health-Serious Classification Hazard Description: Public Works crew was at Brateng Rd/Elkins Road to work on a culvert when they encountered a pink powdered substance covering an area approximately 12 feet by 3 feet. The material was sampled. Laboratory results showed insecticides Chlorpyrifos and Sulfotepp. Four employees sought medical care. Referral Action Send Letter Date Letter Sent Date Response Due Satisfactory) Response Received (Satisfactory or Not Supervisor Assigned V1883 Inspection Planned? Yes llers, Priority: If No, Reason: Transfer To (Name): lTransfer Date [Vac/2017 Transfer To Category: Strategic Initiatives National Emphasis Local Emphasis Optional Information Type Optional Information Value Close Referral Comments Ure 0? Department of Consumer and Business Services Oregon Occupational Safety Health Division (OR-OSHA) Kate Brown, Governor 350 Winter Street NE, Room 430 PO Box 14480 Salem, OR 97309-0405 - Phone: 503-378-3272 Toll Free: 1?800-922-2689 Fax: 503?947-7461 Polk County 850 Main St Dallas, OR 97338 InSpection Number: 31771809l(93) Optional Report Number: Y6318-012-l7 Employer Number: 5701115-010 Inspection Date(s): 08/22/2017-10/25/2017 The Oregon Occupational Safety and Health Division (OR-OSHA) conducted an inspection of your workplace located at 820 SW Ash St, Dallas, OR 97338. The inspection Was to determine if safety or health hazards were present which could cause injury or illness to your employees. 7 In the course ofthe inspection, the OR-OSHA representative noted certain conditions which are listed in the following page which could cause injuries and/or illnesses Although it is not mandatory to correct them at this time, ifthe work process, operation exposure etc. changes, these conditions could be cited as violations during future inspections. By initiating corrective measures you could reduce the high cost of human suffering associated with work-related injuries and illnesses. There may be other hazards present which were not apparent at the time of the inspection. lfyou need assistance in identifying and/or eliminating health or safety hazards consultative and training services are available to you at no cost through OR- OSHA by calling (503) 378- 3272. Your continuing effort to identify and eliminate work-related hazards is appreciated. Ronald Haverkost OR-OSHA Salem Field Of?ce 1340 Tandem Ave NE, Suite 160 PO Box 14513 Salem, OR 97303 Page i of 2 NOTICE Employer Name: Polk County Employer ID No: 5701115-010 Inspection Number: 317718091(93) Optional Num: Y63.18-012-17 THE FOLLOWING IS A LIST OF CONDITIONS WHICH COULD CAUSE WORK- RELATED INJURIES OR ILLNESSES TO EMPLOYEES. ALTHOUGH NOT MANDATORY AT THIS TIME THE OREGON OCCUPATIONAL SAFETY AND HEALTH DIVISION ENCOURAGES YOU TO INITIATE CORRECTIVE MEASURES FOR THESE PROBLEM AREAS IN THE INTEREST OF REDUCING THE HIGH COST AND HUMAN SUFFERING ASSOCIATED WITH INJURIES AND ILLNESSES. Item 01 Employees going home in their personal vehicles in contaminated clothing Providing coveralls for use in an emergency Page 2 OD Tn- ms. 1. . For delivery information visit our website at 'u?sps cam? it? i? i is Ln We. Certi?ed Maii Fee i$ Extra Services Fees (check box. add fee as appropriate) Return Receipt (hardcopyi Return Receipt (electronic) . Postmark cj Mali Restricted Delivery 3 Here Signature Required 3 Signature Restricted Delivery Postage Ln Ell Total Postage and Fees Sent To 2 'StreetandApr? Na. arPO Hoi'iifo. .--. 'biiyj?Siare, COMPLETE THIS SECTION CN DELIVERY - suaav mamas EiHl- do - 3 .. A. Signature 3? 7 7/307/ 2442 Z)?r 4. Restricted Dehvery?br?ExtraF '9d011waxousaomd . item 4 if Restricted Delivery' is eSired. 33 Agent a Print your name and address. on the reverse CI Addressee 3 scathat we can return the card to you. :1 by inted Na e) ate of Delivery 3 I Attach this card to the back of the mailpiece, [@231th \7 3 organ the front if space permits. - I as}; D. is delivery address different from item 1? 3:3 Yes/ i 1' '?yd?g Addressed to. if YES, enter delivery address below: No i .. sir; #?mh'mw 53:31? i p345: var-r, 3 1" . In.? 5 i: w" POLK COUNTY 3 850 MAIN ST DALLAS OR 97338 1? 3. Serv' Type 3 a Hw?? Certified Mail Express Mail . -. - E3 Registered Return ReCeipt for Merchandis '3 El insured Maii Warm usan aw P's Form 381 ?3 February 2004 Domestic Return Receiptf'i?i? 1: 1 1 02595-02-M-1 5405 Ol HAZARD (non code related) WORKSHEET Employer Name: Polk County Public Works Report No: Y6318-012?l7 An inspection occurred at Polk County Public Works to investigate the Pesticide Analytical Response Center Case #18-0038 of employee exposure to pesticides following a culvert cleaning operation. An evaluation of the incident, and subsequent response identi?ed an area of concern. After the employees were contacted by the pesticide contaminated mist from the clog concealed within the culvert, the employees returned to the shop for further decontamination prior to going home in their personal vehicles. They went home wearing contaminated clothing. It is recommended that you have on hand in your shop area, coveralls that could be used in an event where an employees workwear is contaminated. This prevents the spread of contamination to the employees? personal vehicles to their homes. While the provision of emergency use coveralls is not required, it is highly recommended. If you have any additional questions, please contact Oregon consultative services section. Polk County Public Works Y6318-012-17 PARC Case 18-0038 A partial health inspection was conducted at Polk County Public Works by Garnet Cooke as a result of a PARC referral. An anticipatory warrant was obtained, as per the Polk County policy to require one, and was served to both Todd Whittaker, Director and Matt Hawkins, Administrative Services Director. The opening conference was then conducted with both as per the opening conference checklist. The Public Works Department has 30 staff with 350 employees total within the county. There were 4 staff affected by the pesticide exposure. OERS received the following on August 15, 2017: Polk County Public Works (PCPW) reported the discovery of a pesticide spill. PCPW crews were at the listed location (Brateng Rd near Elkins Road in Monmouth) to work on a culvert and were exposed to an apparent dumping of pesticides. lt?s unknown exactly how much was dumped, or when it occurred, but it covered an area approximately 12? by The material was sampled and sent to a lab in Tigard and the substances were chlorpyrifos and sulfotep. Since the discovery at least 3 employees needed medical attention after being exposed to the material. 0138 plan is to refer the scene to the local fire dept. Polk 1 PD, Neil Olson. The exact location is the 1300 ft west ofthe east end intersection of Brateng Rd and Elkins Rd. It is an inlet to a culvert that leads to a field tile about 1 mile from ?owing water. Unknown if waterways are threatened. N0 Cleanup measures have been taken. Due to the remote location and low usage, the FD did not cone, or tape off the area. Caller advised to report this to the NRC also. Oregon OSHA received the referral from PARC on August 16th, The warrant process began on the 16th and was signed by the Judge on the 22nd of August. The inspection was opened that day. Site visits to Brateng Road occurred on August 22?, 23rd with PARC coordinator Ted Bunch, and on August 24th with Geoffrey Brown, State On-Scene Coordinator, Emergency Response Program. The investigation revealed a varied description. On August 7th, a crew of two were working on cleaning culverts using a ?jet rod.? This devise has a cone that is propelled forward by water shooting in the opposite direction. When it was deployed in the culvert it met an obstruction. The employee on the controls pulled it back, returned to the controls and restarted the device. As it shot forward it sprayed out a pink colored, chemical smelling cloud that hit the bank, and was swirled toward the controller. He received substantial frontal contact. The second employee directly above the culvert received minor contact. They extracted the jet rod and pulled forward up the road where they washed with water and called in to their supervisor to report the incident and returned to the yard. There they washed their face and hands with soap and water, did not change clothes and went home. The employee with the most contact threw away his clothes, shoes and took 3 showers. He experienced almost immediate that increased in severity. The second employee had minor PCPW contacted the sheriff who noti?ed Polk County Fire District l,who, due to the remote location opted not to restrict the area. The following day, the Director and tea/r0724 1" supervisor of the two employees went to the site and tried to look into the culvert to see what was in there and both immediately experienced Upon returning to the yard all four went to the Emurgent Medical Care office in Dallas. There they were informed there was nothing they could do for them because they had no idea what to test for, nor what body ?uid to take. Northwest Fire Fighters Environmental, Emergency Spill Response were dispatched to collect soil samples at the site on August 81}] and submitted them for analysis on August 9th. On August the results were obtained and showed two toxic organophosphate insecticides and high levels. Chlorpyrifos levels at 207,000 Sulfotepp levels at 678 Todd Whittaker then contacted the Oregon Emergency Response System at 1514 hours, and the National Response Center at 1830 hours. The employee with the greatest exposure sought additional medical care at the Corvallis Occupational Clinic with biological samples taken for organophosphate exposure. At 0800 on August 16th, DEQ issued the cleanup contract with work commencing later that day of scraping surface soils around the culvert. No containers were found.? Site visits on August 22nd and 23rd still revealed heavy strong odors with subsequent noti?cation made to Geoffrey Brown, at DEQ. A second cleanup took place on August 24?h which consisted of the culvert being jet rodded with water at either end being collected. The soil was retested at four points. at 11 o?clock (NW ofthe culvert), SS-2 to the right of 12 o?clock (North ofthe culvert), 88?3 at 6 o?clock (S of the culvert) and at the top where greenish material had been observed along a separation where the culvert sections had separated. This was termed a ?rat hole.? These results revealed: - at 28.9 ug/kg Chlorpyrifos at 101,000 ug/kg Chlorpyrifos at 370 ug/kg SS-3: 4, at 9.9 ug/kg Chlorpyrifos at 17,600 rig/kg ss?4: 2,4 at 320,000 ug/kg DEQ was planning no further action after a cost of approximately $10000 with no responsible party identified. The farm immediately south of the location was notified. The closing conference was conducted by phone with Todd Whittaker on October 2017 as per the closing conference checklist. A hazard letter issued in regards to providing the availability of coveralls for use in an emergency so affected employees would not return home in their personal vehicles in contaminated clothing. County Public Worksdocx OREGON OSHA CONFERENCQ EMPWER PW [Wit/6% {Malta WM (5 Opt No OPENING CONFERENCE Full 3 5* *Abbreviated Date full Opening conducted 9/22?? 7? *lntroduction/cryentials *Employer rep lad/A CV I Employee rep 3. *Explain purpose, vnature, and scope Of inspection (include expansion Of serious) 4. Loc under Oregon OSHA consultation (7 days prior to 60/30 days after)? Yes No 5. Loc NAICS code? Scheduled NAICS code :T/S?pc MOD rate 5 0.50 or less (must have written proof): Yes/rate 7.. Sampling Photos Video Audio Trade secrets? Employee interviews (in private) discrimination prohibited _1 . Violations Reductions (size, history, good faith, immediate) 11. Closing conference at end Of inspection 12. Records review (min. OSHA 8015) 7/13. PPE required by employer for inspection Indicates minimum requirement for an abbreviated Opening CLOSING lift Via phone Letter Closing date 1 Employer rep. Employee rep. 1. Employer right to present pertinent information re: violations (included in the report) 2. Describe alleged violations (identify probability and severity) Penalties assessed Repeat violations (2X, 5X, 10X, 15X, 20X) Abatement time for each violation (immediate; 7, 14, 21, or 28 days) Hazard letters Citations issued from Salem via certified mail. Abatement time starts upon receipt Letter of Corrective Action. Due date. Follow-up inspection Failure to abate violations may result in daily penalties Employer must post citation (3 days or until abated) where employees Can view it 10. Employer can appeal violation/penalty/abatement time. Employees can appeal abatement time 11. Citation becomes final order if not appealed within 30'days Of receipt 12. Appeal in writing (appealed items stayed if serious must be abated) 13. Informal conference at field Office or by phone. Formal hearing 14. Abatement assistance is available through CO 15. Abatement extension available 16. Referrals? To whom? 17. Variance A 18. Employees protected from discrimination (BOLI) 19. Oregon OSHA consultation available and their workers? comp. carrier required to provide 20. Work-related in-patient hospitalization, loss Of an eye, and amputation or avulsion that results in bone or cartilage loss requires notification within 24 hours an 21. Work-related fatality or catastrophe requires notification within 8 hours 440-2318 Polk County Public Works Y6318-012-17 FILE POLK COUH I 1 0R (3 2 TRIAL COUR 3 ENTERED 4 IN THE CIRCUIT COURT OF THE STATE OF OREGON 5 FOR THE COUNTY OF POLK 6 STATE OF OREGON, ex rel Case No. - I7 [q I) 0/2 (556 OREGON OCCUPATIONAL SAFETY 7 HEALTH DIVISION of the DEPARTMENT 8 OF CONSUMER BUSINESS SERVICES, 9 Petitioner, V. MOTION AND APPLICATION FOR 10 INSPECTION WARRANT UNDER 11 POLK COUNTY PUBLIC WORKS, ORS CHAPTER 654 Em lo er. 12 13 The Oregon Occupational Safety and Health Division of theDepartment of 14 Consumer and Business Services, by and through its attorney, Kyle J. Martin, Senior Assistant 15 Attorney General, hereby moves and makes application to the court for the issuance of an 16 inspection warrant, pursuant to ORS 654.067(3) and 654.202 to 654.216. This motion is 17? supported by the Af?davit of Garnet Cooke, .OR-OSHA Compliance Of?cer. . 4i? 18 DATED this )4 day of August 2017. 19 Respect?illy submitted, 20 .. ELLEN F. ROSENBLUM Attorney General 21 22 . . 23 NI?artln, OSB 913723 Senior Assistant Attorney General 24 Department of Justice . 1 162 Court Street NE 25 Salem, OR 97301-4096 76 Email: Kyle.j.martin@state.or.us Page I - MOTION AND APPLICATION FOR INSPECTION WARRANT UNDER ORS CHAPTER 654 Department ofJustice 1162 Court Street NE Salem, OR 97301-4096 (503) 947?4520 Fax: (503) 378-3784 h?l HapPolk Count Y63I8- 012 7Ublic Works C3 FILED . POLK CDUHI person 17 AUG 22 PM 2121+ COURI ENTERED In the Circuit Court ofthe State of Oregon for the County of Polk In the Matter of the Inspection of: Polk County Public Works Case No. 17H i AFFIDAVIT OF GARNET COOKE The Oregon Occupational Safety and Health Division of the Department of Consumer and Business Services for the State of Oregon makes application for an administrative inspection warrant pursuant to ORS 654.202 through 654.216, to permit inspection of the workplace of Polk County Public Works, at 820 Ash St, Dallas, OR 97338, . as well as the insecticide spill site of 1300 ft. west of the east end intersection of Branteng Rd and Elkins Rd, Dallas, OR. I, Garnet Cooke, first being duly sworn, state as follows: Per ORS 654.003, the purpose of the Oregon Safe Employment Act is to. assure safe and healthful working conditions for every working man and woman in Oregon. The Director of the Department of Consumer and Business Services is charged with the administration of the pursuant to ORS 654.025. is authorized by ORS 654.035(4) to establish a program'of inspection for places of employment for the purpose of determining whether an employer is furnishing a safe and healthful place of employment in accordance with the its standards, rules, and regulations. OR-OSHA is responsible for developing and implementing the OR-OSHA inspection program. Per OAR 437?001?0055, inspections are based on reports of imminent danger, Page 1 POIK County ublic Y6318-012-i7 works 0) fatalities, catastrophes or accidents, complaints, referrals, programmed inspections and follow?up inspections. I am a health compliance officer for In my capacity as a health compliance officer, I am required to make inspections of places of employment throughout the state of Oregon to verify compliance with safety and health regulations. I am authorized by ORS 654.025, 654.062, and 654.067 to enter, inspect, and investigate in a reasonable manner any establishment or workplace where an employee is performing work. When consent for an inspection cannot be'obtained from an employer, OR-OSHA is authorized to obtain an inspection warrant for the purposes of entry and. inspection pursuant to ORS 654.202 to 654.216. Under ORS an inspection warrant is issued upon a showing of cause. Under ORS cause exists if there is probable cause. to believe that a workplace condition does not conform with a safety or health statute, ordinance, regulation, rule, standard, or order. Probable cause can be established through the referral of a safety or health violation in the workplace. OAR 437-001-0055(4) states an inspection may be initiated if safety or health violations are observed by an Oregon OSHA employee or other federal, state, or local governmental representative. and the nature of the information received indicates the probable validity of the referral. On August 15, 2017, received a referral about a hazardous condition located at 1300 ft west of the east end intersection of Branteng Rd and Elkins Rd, Dallas, OR from a source that appears to be reliable because of a report received by the National Response Center stating that employees from the Polk County Public Works of?ce reported Page 2 pPolk County Public Works Y6318-012-17 respiratory ailments due to an insecticide spill and were being tested and observed at a1 medical facility. The referral alleges the following: Unknown pink powder substances were found along a road during maintenance work. The substances were later identified as Chlorpyrifos (insecticide) and Sculfotep (insecticide). Individuals reported respiratoryrailments due to exposure to these substances. On August 15, 2017, this inspection was assigned to me. I will inspect the spill site noted above as well as the main of?ce of Polk County Public Works, located at 820 Ash Street, Dallas, Oregon, because the exposed employees are based out of this location and records are maintained in this location. Per ORS 654.206, an inspection warrant will be issued if entry into the workplace has been sought and refused, or the facts or circumstances reasOnably indicate the inspection- will be frustrated if entry is sought without a warrant. Representatives of Polk County informed at the last OR-OSHA inspection in 2016 that future inspections would require a warrant, which indicates this inspection will likely be frustrated if entry is sought without a warrant. Due to the size and location of Polk County Public Works, a maximum 10 days will be required to complete the inspection. Therefore, I, Garnet Cooke, a representative of OR-OSHA, request the court issue an inspection warrant pursuant to ORS 654.202 to inspect the workplace of Polk County Public Works located at 820 Ash St, Dallas, OR 97338, and the spill site located at 1300 ft. west of the east end intersection of Branteng Rd and Elkins Rd, Dalls, OR, to determine if this Page 3 14 15 16 17? 18 Polk County Public Works Y6318-012-l7 employer has complied with the Oregon Safe Employment Act, its standards, rules and regulations. 1 haveread this affidavit and swear the contents are true to the best of my knowledge, information, and belief. Garnet Cooke, Health Compliance Of?cer Date Subscribed and sworn to before me FEATHER NICOLE CHASE on 101.1% 97317 NOTARY PUBLIC-OREGON COMMISSION NO 92633OA WW EXHRES MARCH19.2018 (Mow/cot, vim . Notary Public My commission expires on: L'Mmu?; '61 901 93? Page 4 Polk County Public Works Y6318-Ol2-l7 - In the Circuit C0urt of the State of Oregon for the County of Polk In the Matter of the Inspection of: CaseNo. quD 08 854 Polk County Public Works INSPECTION WARRANT To: Garnet Cooke, Compliance Officer of the Oregon Occupational Safety and Health Division of the Department of Consumer and Business Services An application has been made by the Oregon Occupational Safety Health Division (OR- OSHA) of the Department of Consumer Business Services of the State of Oregon, for an inspection warrant pursuant to ORS 654.202 for the purpose of conducting an inspection - authorized by OAR 437-001?0055. The applicant, Garnet Cooke, provided under oath or affirmation a signed affidavit, which is attached and includes factual information and the legal basis for issuance of an inspection warrant. The Court has verified the accUracy of the affidavit by examining Garnet Cooke under oath or affirmation, and has determined that cause exists to inspect the workplace described as the work area(s), site(s), premises, building(s), and/or facilities of: Page 1 - INSPECTION WARRANT '24 Polk County Public Works Y6318-012-17 Cd Polk County Public Works 1300 ft west of the east end intersection of Branteng Rd and Elkins Rd, Dallas, Oregon, and the main office located at 820 SW Ash St, Dallas, OR 97338. based upon a referral received by OR-OSHA that supports a belief that a condition of non? conformity with safety or health standards exists at this place of employment. The rules established by Oregon Occupational Safety and Health Division?in OAR Chapter 437, Division 1, are being applied on a valid and neutral basis to this particular workplace. The facts or circumstances reasonably indicate the inspection will be frustrated if entry is sought without a warrant. It is hereby ordered that Garnet Cooke and/or other designated representatives enter and inspect the work site located at 1300 ft west of the east end intersection of Branteng Rd and Elkins Rd, and the main office located at 820 SW Ash St, Dallas, OR, on any day of the week between the hours of 8:00 am and 6:00 pm, and inspect and investigate in a reasonable manner and to a reasonable extent. Per OAR 437-001-0090, this includes, but is not limited to, inspecting all required records, conditions, structures, machines, materials and methods for compliance with statutes, regulations, rules, standards and orders; use of photography, videotape, audiotape, or other devices to record conditions; privately interviewing employees about safety and health conditions; use of interpreters; taking environmental and personal exposure samples; or other activities which may determine whether the employer is furnishing to its employees a safe and healthful work environment. Page 2 WARRANT Polk County Public Works Y6318-012-l7 This inspectionjwill be conducted without unreasonably disrupting operations at this work - site. Any information obtained or observed which contains or might reveal a trade secret referred to in section 1905, title 18, United States Code, shall be considered confidential per ORS Representatives of the Oregon Occupational Safety Health Division are hereby commanded to make an inspection for a maximum of 10 day(s). Before entry, Garnet Co'oke, will present her credentials to an agent of the employer, explain the purpose of the inspection and will present the warrant. A peace officer will assist, if requested, in the execution of this inspection warrant. This inspection warrant must be executed and returned to this court within ten (10) days from its date of issuance, unless this court before the expiration of such time extends the time for five (5) days. After the expiration of the time prescribed, the warrant, unless executed, is void. DATED this 23 day of ,2017 ?x Page 3 - INSPECTION WARRANT Polk County Public Works Y63l8-012?l7 IN THE CIRCUIT COURT OF THE STATE OF OREGON FOR THE COUNTY OF Polk CASE NO. 17AD02859 In the Matter of the Inspection of: Polk County Public Works 820 Ash St Dallas, OR 97338 RETURN OF INSPECTION WARRANT STATE OF OREGON County ofPolk I, Garnet Cooke, Safety/Health Compliance Of?cer for the Oregon Occupational Safety and Health Division of the Department of Consumer and Business Services for the State of Oregon, certify that I received a copy of the above Inspection Warrant on the 16th day of August, 2017. I served the Inspection Warrant on the 22nd day of August, on Polk County Public Works located at 820 Ash St, Dallas, OR 97338 DATED this 29th day of August, 2017. Garnet Cooke Safety/Health Compliance Of?cer Page 1 - RETURN OF INSPECTION WARRANT DocumentZ 10 ll 12 Polk County Public Works Y6318-012-17 ?0033 Flt- CONN I Gd:- htbOH 17/111822 PH 2:21; TRIAL count ENTERED or IN THE CIRCUIT COURT OF THE STATE OF OREGON FOR THE COUNTY OF POLK STATE OF OREGON, ex rel OREGON OCCUPATIONAL SAFETY HEALTH DIVISION of the DEPARTMENT OF CONSUMER BUSINESS SERVICES, Petitioner, v. POLK COUNTY PUBLIC WORKS, Employer. l7 0 17? 02 35?? Case No. MOTION AND APPLICATION FOR INSPECTION WARRANT UNDER ORS CHAPTER 654 The Oregon Occupational Safety and Health Division of the Department of Consumer and Business Services, by and through its attorney, Kyle J. Martin, Senior Assistant Attorney General, hereby moves and makes application to the court for the issuance of an inspection warrant, pursuant to ORS 654.067(3) and 654.202 to 654.216. This motion is supported by the Af?davit of Garnet Cooke, OR-OSHA Compliance Of?cer. . DATED this )4 day of August 2017. Respectfully submitted, ELLEN F. ROSENBLUM Attorney General Martin, OSB 913723 Senior Assistant Attorney General Department of Justice 1162 Court Street NE Salem, OR 97301-4096 Email: Kyle.j.martin@state.or.us Page 1 MOTION AND APPLICATION FOR INSPECTION WARRANT UNDER ORS CHAPTER 654 Department of Justice 1 162 Court Street NE Salem, OR 97301-4096 (503) 9474520 Fax: (503) 378-3784 4s. 25 26 27 28 29 Polk County Y63 8-Ol2-l In the Circuit Court of the State of Oregon for the County of Polk Public Works 7 In the Matter of the Inspection of: CaseNo. IVHD 03- 854 Polk County Public Works INSPECTION WARRANT To: Garnet Cooke, Compliance Officer of the Oregon Occupational Safety and Health Division of'the Department of Consumer and Business Services An application has been made by the Oregon Occupational Safety Health Division (OR- OSHA) of the Department of Consumer Business Services of the State of Oregon, for an inspection warrant pursuant to ORS 654.202 for the purpose of conducting an inspection authorized by OAR 437-001-0055. The applicant, Garnet Cooke, provided under oath or affirmation a signed affidavit, which is attached and includes factual information and the legal basis for issuance of'an inspection warrant. The Court has verified the accuracy of the affidavit by examining Garnet Cooke under oath or affirmation, and has determined that cause exists to inspect the workplace described as the work area(s), site(s), premises, building(s), and/or facilities of: Page 1 - INSPECTION WARRANT ?24 Polk County Public Works Y63l8-Ol2-l7 Polk County Public Works 1300 ft west of the east end intersection of Branteng Rd and Elkins Rd, Dallas, Oregon, and the main office located at 820 SW Ash St, Dallas, OR 97338. based upon a referral received by OR-OSHA that supports a belief that a condition of non- conformity with safety or health standards exists at this place of employment. The rules established by Oregon Occupational Safety and Health Division in OAR Chapter 437, Division 1, are being applied on a valid and neutral basis to this particular workplace. The facts or circumstances reasonably indicate the inspection will be frustrated if entry is sought without a warrant. It is hereby ordered that Garnet Cooke and/or other designated representatives enter and inspect the work site located at 1300 ft west of the east end intersection of Branteng Rd and Elkins Rd, and the main office located at 820 SW Ash St, Dallas, OR, on any day of the week between the hours of 8:00 am and 6:00 pm, and inspect and investigate in a reasonable manner and to areasonable extent. Per OAR 437-001-0090, this includes, but is not limited to, inspecting all required records, conditions, structures, machines, materials and methods for compliance with statutes, regulations, rules, standards and orders; use of photography, videotape, audiotape, or other devices to record conditions; privately interviewing employees about safety and health conditions; use of interpreters; taking environmental and personal exposure samples; or other activities which may I determine whether the employer is furnishing to its employees a safe and healthful work environment. Page 2 - WARRANT Polk County Public Works Y6318-Ol2-l7 [p This inspection will be conducted without unreasonably disrupting operations at this work site. Any information obtained or observed which contains or might reveal a trade secret referred to in section 1905, title 18, United States Code, shall be considered confidential per ORS Representatives of the Oregon Occupational Safety Health Division are hereby commanded to make an inspection for a maximum of 10 day(s). Before entry, Garnet Cooke, will present her credentials to an agent of the employer, explain the purpose of the inspection and will present the warrant. A peace officer will assist, if requested, in the execution of this inspection warrant. This inspection warrant must be executed and returned to this court within ten. (10) days from its date of issuance, unless this court before the expiration'of such time extends the time for five (5) days. After the expiration of the time prescribed, the warrant, unless executed, is void. DATED this gg day of 2017 Page 3 - INSPECTION WARRANT y(:0th . ?5318-0123/17? he Works Certified Tiiu\2'4 TRla?xi. ENTERED in the Circuit Court 0 the State of Oregon for the County of Polk In the Matter of the Inspection of: Polk County Public Works Case No. ?7 A 00,285? AFFIDAVIT 0F GARNET COOKE The Oregon Occupational Safety and Health Division (OR-OSHA) of the Department of Consumer and Business Services for the State of Oregon makes application for an administrative inspection warrant pursuant to ORS 654.202 through 654.216, to permit inspection of the workplace of Polk County Public Works, at 820 Ash St, Dallas, OR 97338, as well as the insecticide spill site of 1300 ft. west of the east end intersection of Branteng Rd and Elkins Rd, Dallas, OR. I, Garnet Cooke, first being duly sworn, state as follows: Per ORS 654.003, the purpose of the Oregon Safe Employment Act is to assure safe and healthful working conditionsfor every working man and woman in Oregon. The Director of the Department of Consumer and Business Services is charged with the administration of the pursuant to ORS 654.025. OR-OSHA is authorized by ORS 654.035(4) to establish a program of inspection for places of employment for the purpose of determining whether an employer is furnishing a safe and healthful place of employment in accordance with the its standards, rules, and regulations. OR-OSHA is responsible for developing and implementing the OR-OSHA inspection program. Per OAR 437-001-0055, inspections are based on reports of imminent danger, Page 1 Polk County Public Works Y63l8-012?17 fatalities, catastrophes or-accidents, complaints, referrals, programmed inspections and follow-up inspections. I am a health compliance officerfor In my capacity as a health compliance officer, I am required to make inspections of places of employment throughout the state of Oregon to verify compliance with safety and health regulations. I am authorized by ORS 654.025, 654.062, and 654.067 to enter, inspect, and investigate in a reasonable manner any establishment or workplace where an employee is performing work. When consent for an inspection cannot be obtained from an employer, is authorized to obtain an inspection warrant for the purposes of entry and inspection pursuant to ORS 654.202 to 654.216. 1 Under ORS an inspection warrant is issued upon a showing of cause. Under ORS cause exists if there is probable cause to believe that a workplace condition does not conform with a safety or health statute, ordinance, regulation, rule, standard, or order. Probable cause can be established-through the referral of a safety or health violation in the workplace. OAR 437-001-0055(4) states an inspection may be initiated if safety or health violations are observed by an Oregon OSHA employee or other federal, state, or local governmental representative and the nature of the information received indicates the probable validity of the referral. On August 15, 2017, received a referral about a hazardoUs condition located at 1300 ft West of the east and intersection of Branteng Rd and Elkins Rd, Dallas, OR from a source that appears to be reliable because of a report received by the National Response Center stating that employees from the Polk County Public Works office reported Page 2 py63I8_012:y17ub1lC Works 15? respiratory ailments due toan insecticide Spill and were being tested and observed at a medical facility. The referral alleges the following: Unknown pink powder substances were found along a road during maintenance work. The substances were later identified as Chlorpyrifos (insecticide) and Sulfotep (insecticide). Individuals reported respiratory ailments due to exposure to these substances. 7 On August 15, 2017, this inspection was assigned to me. lwill inspect the spill site noted above as well as the main of?ce of Polk County Public Works, located at 820 Ash Street, Dallas, Oregon, because the exposed employees are based out of this location and records are maintained in this location. Per ORS 654.206, an inspection warrant will be issued if entry into the workplace has been sought and refused, or the facts or circumstances reasonably indicate the inspection will be frustrated if entry is sought without a warrant. Representatives of Polk County informed OR-OSHA at the last OR-OSHA inspection in 2016 that future inspections would require a warrant, which indicates this inspection will likely be frustrated if entry is sought without a warrant. Due to the size and location of Polk County Public Works, a maximum 10 days will be required to complete the inspection. Therefore, I, Garnet Cooke, a representative of OR-OSHA, request the court issue an inspection warrant pursuant to ORS 654.202 to inspect the workplace of Polk County Public Works located at 820 Ash St, Dallas, OR 97338, and the spill site located at 1300 ft. west of the east end intersection of Branteng Rd and Elkins Rd, Dalls, OR, to determine if this Page 3 13 14 15 16 17 18 Polk County Public Works Y63 i8-012-l7 employer has complied with the Oregon Safe Employment Act, its standards, rules and regulations. have read this affidavit and swear the contents are true to the best of my knowledge, information, and belief. . JwUzwcL/t? 5L Garnet Cooke, Health Compliance Of?cer Ra?s?90%? Date Subscribed and sworn to before me on Hug/15% L99, 9131'? ul/L, . Notary Public My commission expires on: ell/Latch ?01 90195 SEAL FEATHER NICOLE CHASE NOTARY PUBUC - OREGON COMMISSION NO 926330A MARCH19.201B Page 4 51050017 ?r 1 Polk County Public Works COOKE Garnet DCBS Wig-012:? From: Theodore Bunch Jr Sent: Wednesday, August 16, 2017 10:16 AM To: COOKE Garnet DCBS Subject: Fwd: Begin forwarded message: From: Theodore Bunch Jr Subject: Fwd: Date: August 16, 2017 at 8:25:42 AM PDT To: Parc Begin forwarded message: From: VAN-PATTEN Kimberlee Subject: FW: Date: August 15, 2017 at 4:29:41 PM PDT To: BUNCH Theodore Here is the corresponding NRC report. Kimberlee Van Patten Duty Of?cer Emergency Response Program Oregon Dept. of Environmental Quality 503-229-5256 office 971-563-8034 cell 700 NE Multnomah St., Suite #1400 Portland, OR 97232 Original Message~-~~? From: Sent: Tuesday, August 15, 2017 3:47 PM To: DO Spills DEQ Subject: NATIONAL RESPONSE CENTER 1-800?424-8802 USE USE 1 Information released to a third party shall comply with any Polk County Pubiic Works applicable federal and/or state Freedom of Information and Privacy Laws Y53 8012-? Incident Report 1 187340 INCIDENT DESCRIPTION *Report taken by: DO ALEXANDER DOMINGO ARANA at 18:30 on 7 Incident Type: FIXED Incident Cause: DUMPING Affected Area: Incident was discovered [on 07-AUG-17 at 15:10 local incident time. Affected Medium: LAND COUNTY DITCH REPORTING PARTY Name: TODD WHITAKER Organization: POLK COUNTY PUBLIC WORKS Address: 820 SW ASH ST DALLAS, OR 97338 Email Address: PRIMARY Phone: (503)6239287 Type of Organization: LOCAL GOVERNMENT SUSPECTED RESPONSIBLE PARTY Name: UNKNOWN Type of Organization: UNKNOWN INCIDENT LOCATION 10630 ELKINS RD County: POLK City: DALLAS State: OR ON BRATENG APPX 1300 FT FROM THE INTERSECTION WITH ELKINS RD RELEASED CHRIS Code: NCC Of?cial Material Name: NO CHRIS CODE Also Known As: CHLORPYRIFOS (INSECTICIDE) Qty Released: 207000 PER MILLION CHRIS Code: NCC Of?cial Material Name: NO CHRIS CODE Also Known As: SULFOTEP (INSECTICIDE) Qty Released: 673 PER MILLION DESCRIPTION OF INCIDENT CALLER REPORTED AN UNKNOWN PINK POWDER SUBSTANCES WERE DISCOVERED ALONG A ROAD DITCH DURING MAINTENANCE WORK. IT WAS LATER IDENTIFIED TO BE CHLORPYRIFOS (INSECTICIDE) AT 207,000 PPM AND SULFOTEP (INSECTICIDE) AT 673 PPM. 04 INDIVIDUALS REPORTED RESPIRATORY AILMENTS DUE TO THESE SUBSTANCES AND ARE BEING TESTED AND OBSERVED 2 AT A MEDICAL FACILITY. Polk County Public Works Y6318-012?l7 SENSITIVE INFORMATION INCIDENT DETAILS Package: Building ID: Type of Fixed Object: OTHER Power Generating Facility: NO Generating Capacity: Type of Fuel: NPDES: NPDES Compliance: UNKNOWN IMPACT Fire Involved: NO Fire Extinguished: UNKNOWN INJURIES: YES 4 Hospitalized: 4 Empl/Crew: Passenger: Empl/Crew: Passenger: Occupant: Who Evacuated: Radius/Area: Damages: NO Hours Direction of Closure Type Description ofClosure Closed Closure Air: Major Road: ArteryzN Waterway: Track: Environmental Impact: UNKNOWN Media Interest: UNKNOWN Community Impact due to Material: REMEDIAL ACTIONS TURNED OVER TO LOCAL FIRE DEPARTMENT Release Secured: YES Release Rate: Estimated Release Duration: WEATHER Weather: CLEAR, ADDITIONAL AGENCIES NOTIFIED Polk County Public Works Federal: Y6318-012-17 State/Local: OR ERS (7/9 I State/Local On Scene: LOCAL FD, State Agency Number: EMR: 2017-2436 NOTIFICATIONS BY NRC CENTERS FOR DISEASE CONTROL (GRASP) 18:46 (770)4887100 DHS DEFENSE THREAT REDUCTION AGENCY (CHEMICAL AND BIOLOGICAL TECHNOLOGI 18:46 (703)7673477 NTNL PROGRAMS AND DIR (OFC OF INFRASTRUCTURE PROTECTION RGN 15-AUG-17 18:46 (202)3097911 DOT CRISIS MANAGEMENT CENTER (MAIN OFFICE) 15-AUG-17 18:46 (202)3661863 EPA CRIMINAL INVESTIGATION DIVISION (EPA CRIMINAL INVESTIGATION DIV REG 15-AUG-17 18:46 (206)5538306 EPA HQ EMERGENCY OPERATIONS CENTER (MAIN OFFICE) 15-AUG-17 18:46 (202)5643850 EPA EMERGENCY OPERATIONS CENTER (AFTER HOURS SECONDARY) (202)5643850 US. EPA SEATTLE (MAIN OFFICE) (206)5531263 US. EPA SEATTLE (CID OREGON) 15-AUG-17 18:46 (206)5531263 FEMA REGION 10 (MAIN OFFICE) 15-AUG-I7 18:46 (425)4874704 NATIONAL INFRASTRUCTURE COORD CTR (MAIN OFFICE) 15-AUG-I7 18:46 (202)2829201 NOAA RPTS FOR OR (MAIN OFFICE) 15-AUG-17 18:46 (206)5264911 NATIONAL RESPONSE CENTER HQ (MAIN OFFICE) 18:46 NATIONAL RESPONSE CENTER HQ (AUTOMATIC REPORTS) 18:46 (202)2671136 OREGON DEQ (EMERGENCY RESPONSE PROGRAM) 18:46 (503)2296391 OREGON TITAN FUSION CENTER (FUSION COMMAND CENTER) 15-AUG-17 18:46 (877)6204702 OREGON PUBLIC HEALTH (ENVIRON OCCUPATIONAL EPIDEMIOLOGY) 18:46 (503)7314025 OCCUPATIONAL SAFETY HEALTH ADMIN (MAIN OFFICE) (801)9180995 REPORTING PARTY (RP SUBMITTER) OREGON EMERGENCY MANAGEMENT (MAIN OFFICE) 15-AUG-17 18:46 (800)4520311 USCG DISTRICT 13 (DISTRICT THIRTEEN (DRAT 15-AUG-17 18:46 (206)2207221 ADDITIONAL INFORMATION .. 7 . Polk County Public Works Y6318 0_12 _1_7 I -. - . 777:7 A?um? . .494420999/5 00%? 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I. - WWL 6W1 10:18:16 17 W6 MW WW: p164 D4CL ,5 3 him/L Jam/163M M1ww8w V7: 5 . Mij 57': m1: MPH [Mac/L65: m9 Mam UM 0:161:7wa 7/ WW WW 11631801717 (331D ?111 W5 1W1W WV 0,11ch - 61111sz 8% 113me 726111654411 WW1 =13 D0121) Ag Poi County Public Works 18-012-17 MWW Way/m (19 98/375443 ~fK/M/l7 WW wife 79 @4777) 77747177759 i . Polk County Public Works ey??i?lz'?ee Cm TODD WHITAKER, PE Director POLK COUNTY WARLTMERSTS 503?623-9287 820 SW. ASH STREET Fax 503-623-0897 DALLAS, OREGON 97338-2151 Oregon - - ZDEPARTMENT OF Geomey Brow? ENVIRONMENTAL QUALITY State On- Scene Coordinator. 7 Emergency Response Program "g Western Reglon- Eugene Office (541) 686 7819 165 East 7th Avenue, Suite 100 Cell. (541) 501- 2145 Eugene, OR 97401- 3049 . Fax: (541) 686- -7551 .- 111 (800) 844-8467.- browh.geoff@deqetatebpus La - ., k) (W Polk County Public Works A Polk County Publi 17 Works Polk County Public Works Y6318-012-l7 ?12- ., onqnd Kjunog >110d mo? 00:50. 35:0 E018 123555-: Polk County Public Works 3?qu Klunog >110d .18?012-1 7 11C Works we? moss? 36:0 ?016 <3Hm-o_w-3 3E imam awn 4 Polk County Public Works Y63l8-012-17 Polk County EOP Incident Annex IA 4. Hazardous Materials (Accidental Release) Hazardous Materials Incident Checklist Supplemental Action Items Information PRE-INCIDENT PHASE El Have personnel participate in necessary training and exercises, as determined by Polk County Emergency Management and the ESF 10 Hazardous Materials Lead, including the Salem Of?ce of State Fire Marshal Regional Hazardous Materials Response Team HazMat 13. El Participate in the County?s preparedness activities, seeking understanding of interactions with agencies that would participate in a hazardous materials scenario. Cl Ensure that emergency contacts lists are updated and establish a pre? event duty roster allowing for 24/7 operational support for the County EOC. CI Inform Emergency Management of any major developments that could adversely affect response operations personnel shortages, loss of equipment, etc.). RESPONSE PHASE El In most incidents, the local ?re districts will initially respond, assume ESF 10 Annex 0f the initial Incident Commander responsibilities, and request County EOP activation/deployment of the Hazardous Materials Team. El Determine the type, scope, and extent of the hazardous materials Form 209: Incident incident (recurring). Verify that reports and obtain estimates of the area Status Summary that may be affected. I Notify 911 dispatch, support agencies, adjacent jurisdictions, ESF coordinators, and liaisons of the situation. Assess the type, severity, and size of the incident. If possible, characterize the hazardous material(s) of concern and determine appropriate personal protection equipment requirements. Ensure that a health and safety plan is developed by the designated Safety Of?cer, including monitoring ?rst responders in accordance with all applicable guidance. Cl Provide support for implementation of applicable Geographic Response Northwest Area Plans established by the Oregon Department of Environmental Quality Contingency Plan to guide activities throughout the duration of the incident. Cl Ensure that proper containment methods have been implemented by the ?rst responders until hazardous materials response teams arrive. El Establish access control to the incident site through local law enforcement agencies. If the situation warrants, request activation of the County EOC Via the Section 5 of the County Incident Commander through the County Emergency Manager. EOP IA 4?1 Public Works 2 Polk Count -17 Y63 I 8-01 Oregon Emergency Response System (OERS) Oregon Emergency Response System Mailing Address: PO Box 14360 Salem, OR Nationwide Local: 503- 97309?6074 800-452-0311 378-6377 Page 1 of2 POW County Pu vests-01247 E?mail: oers.staff@state.or.us Fax: (503) 588-1378 OERS Incident Number: 2017-2436 Incident Type: CBT Received: 08/15/2017 at 1514 Taken Fitz atrick Tracie Occurred: 08/07/2017 at 1510 By: Location: Brateng Rd. near Elkins Rd. Coordination Time: City: Monmouth 15 County: Polk Contact Type: Paged: Answered: Contact Name Organization: Phone Caller Todd Whitaker Polk Co. PW 503-623-9287 Comments Email 1538 [pm I Comments Pager 1538 IDEQ Comments Email 1538 Comments Pager 1538 I Comments Pager 1538 IOSHA Comments Email 1539 Comments Pager 1539 Comments Notification 1539 IPCC Comments Incident Desc?tion: Polk Co. PW reported the discovery of a pesticide spill. Polk Co. PW crews were at the listed location to work on a culvert and were exposed to an apparent dumping of pesticides. It's unknown exactly how much was dumped, or when it occurred, but it covered an area approximately 12ft 3ft. The material was sampled and sent to a lab in Tigard and the substances were "chlorpyrifos" and "sulfotep". Since the discovery at least 3 employees needed medical attention after being exposed to the material. PW's ops plan is to refer the scene to the local fire dept. (Polk 1 FD, Neil Olson, 503-838- 1510.) The exact location is the 1300 ft west of the east end intersection of Brateng Rd and Elkins Rd. It is an inlet to a culvert that leads to a field tile about 1 mile from flowing water. Unknown if waterways are threatened. No cleanup measures have been taken. Due to the remote location and low usage, the FD did not cone, or tape, off the area. Caller advised to report this to the NRC also. Material: Pesticides Unit Of Measure: UNK Quantity Released: unknown Release Source: Potential for further spillage: None known Site secured for safety: None Threat to public waterways: Possibly ://oregonem Inc?b .aspx 8/15/2017 Oregon Emergency Response System (OERS) Threat to public safety: Yes, inhalation may cause Page 2 of2 Polk County Public Works Y6318?012?i7 Threat to property: Unknown Containment steps taken: Refered to fire dept './/oregonem ERSInc-b.aspx 8/15/20] 7 COOKE Garnet DCBS From: Theodore Bunch Jr Sent: Wednesday, August 16, 2017 10:16 AM To: COOKE Garnet DCBS Subject: Fwd: Begin forwarded message: From: Theodore Bunch Jr Subject: Fwd: Date: August 16, 2017 at 8:25:42 AM PDT To: Parc Begin forwarded message: From: Kimberlee Subject: FW: Date: August 15, 2017 at 4:29:41 PM PDT To: BUNCH Theodore Here is the corresponding NRC report. Kimberlee Van Patten Duty Of?cer Emergency Response Program Oregon Dept. of Environmental Quality 503?229-5256 of?ce 971?563?8034 cell 700 NE Multnomah St., Suite #1400 Portland, OR 97232 Original Message-??-? From: Sent: Tuesday, August 15, 2017 3:47 PM To: DO Spills DEQ Subject: NATIONAL RESPONSE CENTER 1?800?424?8802 USE USE 1 Information released to a third party shall comply with any applicable federal and/or state Freedom of Information and Privacy Laws Polk County Public Works Incident Report 1 187340 . INCIDENT DESCRIPTION *Report taken by: DO ALEXANDER DOMINGO ARANA at 18:30 on 15-AUG-17 Incident Type: FIXED Incident Cause: DUMPING Affected Area: . Incident was discovered on 07-AUG-17 at 15:10 local incident time. Affected Medium: LAND COUNTY DITCH REPORTING PARTY Name: TODD WHITAKER Organization: POLK COUNTY PUBLIC WORKS Address: 820 SW ASH ST DALLAS, OR 97338 Email Address: whitaker.todd@c0.polkorus PRIMARY Phone: (503)6239287 Type of Organization: LOCAL GOVERNMENT SUSPECTED RESPONSIB LE PARTY Name: UNKNOWN Type of Organization: UNKNOWN INCIDENT LOCATION 10630 ELKINS RD County: POLK City: DALLAS State: OR ON BRATENG APPX 1300 FT FROM THE INTERSECTION WITH ELKINS RD RELEASED CHRIS Code: NCC Of?cial Material Name: NO CHRIS CODE Also Known As: CHLORPYRIFOS (INSECTICIDE) Qty Released: 207000 PER MILLION CHRIS Code: NCC Of?cial Material Name: NO CHRIS CODE Also Known As: SULFOTEP (INSECTICIDE) Qty Released: 673 PER MILLION DESCRIPTION OF INCIDENT CALLER REPORTED AN UNKNOWN PINK POWDER SUBSTANCES WERE DISCOVERED ALONG A ROAD DITCH DURING MAINTENANCE WORK. IT WAS LATER IDENTIFIED TO BE CHLORPYRIFOS (INSECTICIDE) AT 207,000 PPM AND SULFOTEP (INSECTICIDE) AT 673 PPM. 04 INDIVIDUALS REPORTED RESPIRATORY AILMENTS DUE TO THESE SUBSTANCES AND ARE BEING TESTED AND OBSERVED 2 AT A MEDICAL FACILITY. Polk County Public Works Y63t8-Oll-l7@ SENSITIVE INFORMATION INCIDENT DETAILS Package: Building ID: Type of Fixed Object: OTHER Power Generating Facility: NO Generating Capacity: Type of Fuel: NPDES: NPDES Compliance: UNKNOWN IMPACT Fire Involved: NO Fire Extinguished: UNKNOWN INJURIES: YES4 Hospitalized: 4 EmpI/Crew: Passenger: ATALITIES: NO Empl/Crew: Passenger: Occupant: EVACUATIONSNO Who Evacuated: Radius/Area: Damages: NO Hours Direction of Closure Type Description of Closure Closed Closure Air: Major Road: Artery2N Waterway: Track: Environmental Impact: UNKNOWN Media Interest: UNKNOWN Community Impact due to Material: REMEDIAL ACTIONS TURNED OVER TO LOCAL FIRE DEPARTMENT Release Secured: YES Release Rate: Estimated Release Duration: Weather: CLEAR, ADDITIONAL AGENCIES NOTIFIED Federal: Polk County Public Works State/Local: OR ERS State/Local On Scene: LOCAL FD, State Agency Number: EMR: 2017-2436 NOTIFICATIONS BY NRC CENTERS FOR DISEASE CONTROL (GRASP) 15-AUG-17 18:46 (770)4887100 DHS DEFENSE THREAT REDUCTION AGENCY (CHEMICAL AND BIOLOGICAL TECHNOLOGI 18:46 (703)7673477 NTNL PROGRAMS AND PROTECTION DIR (OFC OF INFRASTRUCTURE PROTECTION RGN 18:46 (202)3097911 DOT CRISIS MANAGEMENT CENTER (MAIN OFFICE) 15-AUG-17 18:46 (202)3661863 EPA CRIMINAL INVESTIGATION DIVISION (EPA CRIMINAL INVESTIGATION DIV REG 15-AUG-17 18:46 (206)5538306 EPA HQ EMERGENCY OPERATIONS CENTER (MAIN OFFICE) 15 AUG 17 18 46 (202)5643850 EPA HQ EMERGENCY OPERATIONS CENTER (AFTER HOURS SECONDARY) (202)5643850 US. EPA SEATTLE (MAIN OFFICE) (206)5531263 US. EPA SEATTLE (CID OREGON) 18:46 (206)5531263 FEMA REGION 10 (MAIN OFFICE) 18:46 (425)4874704 NATIONAL INFRASTRUCTURE COORD CTR (MAIN OFFICE) 18:46 (202)2829201 NOAA RPTS FOR OR (MAIN OFFICE) 18:46 (206)5264911 NATIONAL RESPONSE CENTER HQ (MAIN OFFICE) 18:46 NATIONAL RESPONSE CENTER HQ (AUTOMATIC REPORTS) 15-AUG-17 18:46 (202)2671136 OREGON DEQ (EMERGENCY RESPONSE PROGRAM) 15 AUG 17 18 46 (503)2296391 OREGON TI TAN FUSION CENTER (FUSION COMMAND CENTER) 15 AUG 17 18 46 (877)6204702 OREGON PUBLIC HEALTH (ENVIRON OCCUPATIONAL EPIDEMIOLOGY) 15-AUG-17 18:46 (503)7314025 OCCUPATIONAL SAFETY HEALTH ADMIN (MAIN OFFICE) (801)9180995 REPORTING PARTY (RP SUBMITTER) 18:46 OREGON EMERGENCY MANAGEMENT (MAIN OFFICE) 18:46 (800)4520311 USCG DISTRICT 13 (DISTRICT THIRTEEN (DRAT - 18:46 (206)2207221 ADDITIONAL INFORMATION END INCIDENT REPORT #1187340 REport any problems by calling 1-800-424-8802 Polk County PUbliC Works PLEASE VISIT OUR WEB SITE AT Polk County Public Works 0 - OREGON DEPARTMENT OF ENVIRONMENTAL QUALITY 6" ?8 0?3" 7 rx EMERGENCY CRITICAL REMOVAL INCIDENT ORDER DEQ INCIDENT ORDER NUMBER ?-06 (Project Number) For OITICIHI Use Oniy CONTRACTOR NRC Services INCIDENT CHANGE ORDER NUMBER 5858 OERS NUMBER ATTENTION Bob Ransdelt EPA GENERATOR NUMBER PHONE NUMBER (800) 337-7455 DEQ AUTHORIZED PROJECT MANAGER David Mastros FAX NUMBER (503) 239-6568 NOIS) 501229-67? CONTACT PERSON Bob FAX NUMBER DEQ ON-SCENE COORDINATOR: Geoi?I?BrOxI/n PHONE NUMBER: 54 DEQ Western Region MOBILE NUMBER: YES NO AUTHORIZED TO MAKE FIELD CHANGES WHICH CHANGE THE SCOPE OF THE LO. WORK. YES NO TO MAKE FIELD CHANGES WHICH EXCEED THE TOTAL AMOUNT. SITE INFORMATION SITE NAME: Pesticide Dump - Brateng Rd ADDRESS: About 1300 from Intersection of Elltins RII. CITY: Monmouth COUNTY: Polk STATE: Oregon CHECK ALI. WHICH APPLY: SUBSTANCES): EMERGENCY RESPONSE ACTION Chlorpyrifbs (207k ppm), Sulfotcp (6731mm) TIME CRITICAL REMOVAL ACTION ESTIMATED QUANTITY: DRUG LAB 3-5 t't ot'contaminated ditch HIGHWAY RELATED SPILL ON-SCENE CONTACT PERSO NIAGENCY: ABANDONED WASTE MATERIAL tt/H LEAKING MANIFEST TO BE SIGNED BY: CONTAINED NRC Petsonncl OTHER WASTE DISPOSITION: WAIVE ONE-HOUR MOBILIZATION Based on rccommemtntimi of contractor SCOPE OF WORK: Assess extent at pesticide contamtnatton Remove pesticide and remediate a??ected soil Dispose ofpestieide and contaminated soil in accordance with appiicahle Iawsv Contact BBQ ifcteamtp costs wiII exceed $3,000.00 Hm ISSUE 3II0I2017 0300 SCHEDULE: 8/16/2017 0300 LO. AMOUNT CHANGE ORDER FUND: HSSR SPLF DCRF TO DATE AMOUNT TOTAL TYPE: SPILL DRUG IIPHASE: RA EST HOURS: 2 2 RESPONSIBLE PARTY: ?Ia COST: 53.500 5 3,500.00 This incident order, or change order, authorizes the above described work only. In the event ofeiny uncertainty regarding the scope Ofeleannp requested under this incident order, as amended, or problems in cieztning up hazardous materials consistent with state law, the CONTRACTOR shall immediately contact the DEQ Authorized Project Manager or DEQ Coordinator. .4. ans/2m? AUTHORIZED PROJECT MANAGER SIGNATURE DATE ?7 W4) 7 AUTHORIZED CLEAN UP CONTRACTOR SIGNATURE DATE ENIAIL OR FAX TO: I) CONTRACTOR 2) DEQ ON-SCENE COORDINATOR 3) DEQ BUSINESS OFFICE BELINDA SAUTAO d) DEQ COST RECOVERY COORDINATOR (503) 229-0977 12232 SW. Garden Place Apex Labs Tigard,OR 97223 503?718-2323 Phone 503-718-0333 Fax Polk County Public Works Y6318-012-l7 Saturday, August 12, 2017' Ross lVchakin NWFF PO Box 188 Philomath, OR 97370 RE: 095/095 Enclosed are the results of analyses for work order A7H0255, which was received by the laboratory on 8/9/2017 at Thank you for using Apex Labs. We appreciate your business and strive to provide the highest quality services to the environmental industry. If you have any questions concerning this report or the services we offer, please feel free to contact me by email at: or by phone at 503-718?2323. DRAFT REPORI 77m rem/M pmw'tlutr' rim i'dpnr/ arc and are ,i'rrbfucl change buxcc/ rm unulwr'x, QC nr/irm/ dam rcw'cw. l?iurue me Jlmxu r'cxullx with 1th understanding ?rm they may have ma! licmn?mr/izcd by the i'crharumry DRAFT REPORT, DATA SUBJECT To CHANGE Page 1 ?"22 Apex Labs Po1k Countv Public . mus?012117 12232 SW. Garden Place Tigard, OR 97223 503?718?2323 Phone 503-718?0333 Fax PO Box 188 PhitomatiLOR 97370 Project: (195 Project Number: 095 Project Manager: Ross McMakin Reported: 08/12/17 06:23 ANALYTICAL REPORT FOR SAMPLES Sample ID SAMPLE INFORMATION Laboratory ID Matrix Date Sampled Soil 08/08/17 11:50 Date Received 08/09/17 08:42 DRAFT REPORT The ram/Ix provided in {his 11.77an are and are rub/cc! to Change ham! on .vu/uequml (mu/His. QC vul/t/ulirm (Ir/inn] dam rev/cu: me than: mam/ix wirh (/10 r/my may how not bccn_/iuulizez/ by the laboratory DRAFT REPORT, DATA SUBJECT TO CHANGE Page 2 01'22 Polk County Public Works Y6318?Ol2-l7 12232 S.W. Garden Place Apex Labs Tigard. OR 97223 b3 503-718?2323 Phone 503-718-0333 Fax NWFF Project: 095 PO Box 188 Project Number: 095 Reported: Philomath, OR 97370 Projccl Manager: ROSS MCMakin 08/12/17 06:23 ANALYTICAL SAMPLE RESULTS Organochlorine Pesticides by EPA 80818 I Analyle Result MDL Limit Units Dilution Date Analyzed Method Notes US-1 (ATH0255-01RE1) . Matrix: Soil Batch: 7080569 0-05. R434 Aldrin ND 64.8 130 mg/kg dry 10000 08.0 1/1 7 13.42 EPA 8081B alpha-BHC ND 64.8 130 .. .. hem-Bl-lC ND 64.8 130 .. della~BHC ND 64.8 130 gamma?BHC (Lindanc) ND 648 130 .. .. cis~Chlordanc ND 64.8 I30 .. trans?Chlordane ND 64.8 130 .. ND 64.8 130 .. ND 6464.8 130 .. Endosull?an ND 64.8 130 .. .. .. lEndosulf'zm ll ND 64.8 130 Endosull?zm sulfate ND 64.8 130 .. l. Endrin ND 64.8 130 .. l. Endrin Aldehyde ND 64.8 130 .. Endrin kelonc ND 64.8 130 l. Hcplachlor ND 64.8 130 Heptachlor epoxide ND 64Chlordane (Technical) ND 1940 3390 .. .. Toxaphenc (Total) ND 1940 3890 .. .. r. Surrogate: Rec-ovum!" Limm: 4.1/29 5-0! (Xurr) Umim.? 65?l5l 5-0] DRAFT REPORT The rem/?M provided in {Inlr report are Ill? and are .mly?ccl to change fumed on QC validation ur?na/ dam review. l?lcasc my rhm'r: rem/1.x- u-irh [he H'mi they may have not by the laboratory DRAFT REPORT, DATA SUBJECT TO CHANGE Page} Polk County Public Works Y6318-012-l7 12232 S.W. Garden Place Apex Labs Tigard,OR 97223 . 503-718-2323 Phone 503?713?0333 Fax NWFF Project: 095 PO Box l88 Project Number: 095 Reported: Philomath, OR 97370 Project Manager: Ross McMakin 08/12/17 06:23 ANALYTICAL SAMPLE RESULTS I Organophosphorous Pesticides (OPPs) by EPA 8270!) (GCIMS) - I Reporting Analyte RCSUH MDL Limit Units Dilution Date Analyzed Method Notes US-1 (A7H0255-01) Matrix: Soil Batch: 7080573 Azinphos methyl (Guthion) ND 35.9 71.7 mg/kg dry IOO 08/10/17 16: I2 8270B OPP Coumaphos ND 359 71_7 -- .. .. Demeton Diazinon ND 2290 2290 .. R-OZ Dichlorvos ND 35.9 7! .7 Dimcthoate ND 359 717 .. .. .. Disulf?oton . ND 4-3.0 86.1 .. EPN ND 35lilhoprophos (ProphosFensulf?othion 2440 2440 .. .. R-OZ Malathion ND 359 717 .. .. ND 93.2 93.2 .. -- .. R-02 Methyl parathion ND 359 7l.7 .. .. Mevinphos (Phosdrin) ND 359 71.7 .. .. Monocrotophos ND 717 71_7 .. .. .. Naled (Dibrom) ND 359 71_7 .. .. Phorate ND 35.9 71.7 .. Ronnel (FenchlorphosSulfuten 673 35.9 71.7 .. .. .. Sulprotos (Bolstar'l'ctt'achlorvinphos (Rabon) ND 71.7 71.7 .. Tokuthion (Prothiol'os) ND 719 .. .i 'l?richloronate ND I43 143 .. R-OZ .S'irr?l'uguic, (243 mex.? 50?14] 3-05 Nip/Wt [vim-mimic (Sm-r) 420 UmfrxREPORT The run/Ix pruviducl in ilu?x report an: I l? and cw .mly'ucl to change based on (mall's-ix, QC Wilt/mini: ur?nai dam review. Home use these m.t'ufl.r with my I/ml [hey may have mil bccn?nulizctl by the laboramry DRAFT DATA SUBJECT TO CHANGE P3246 4 OFZZ Polk County Public Works Y6318-012-17 12232 S.W. Garden Place Ap 6X Lab - Tigurd, OR 97223 503-718-2323 Phone 503-718-0333 Fax Project: 095 PO Box 188 Project Number: 095 Reported: Ph110ma1h, OR 97370 Project Manager: Ross McMakin 08/12/17 06:23 ANALYTICAL SAMPLE RESULTS I Organophosphorous Pesticides (OPPs) by EPA 82700 I Reporting Analyte Result L1mit Units Dilution Date Analyzed Method US-1 (A7H0255-01RE1) Matrix: 3011 Batch: 7080573 Chlurpyrifos 207000 3590 7170 mg/kg dry 10000 08/10/17 16:49 8270B OPP 13-02 Parathiom ethyl ND 3590 7170 .. .. DRAFT REPORT The mum prrwiu'ud I?d/mm are Sub/cw change: huxcd rm .mbxeqwnl (Ina/147A: QC vultdun?un ur?mn? dart.- mv/cw, Plume uxc lime ram/M xvii/1 1/78 um/crxlum/ing r/ml H'rcry may have not by [/10 DRAFT REPORT, DATA SUBJECT To CHANGE . - Page 5 0f 22 Polk County Public Works Y6318-012-l7 12232 S.W. Garden Place Apex Labs Tigard,0R 97223 503-718?2323 Phone 503-718-0333 Fax Project; 095 PO Box 188 - Project Number: 095 Reported: Philomalli. OR 97370 Project Manager: Ross McMakin 08/12/17 06:23 ANALYTICAL SAMPLE RESULTS 1 Total Metals by EPA 6020 (ICPMS) I Reporting Analyle Result MDL Limil Units Dilution Date Analyzed Method Notes US-1 (ATHozss-on Matrix: Soil Batch: 7080565 Antimony ND 0824 1.65 mg/kg dry 10 08/11/17 20:01 EPA 6020A Arsenic 2.12 0.824 1.65 53.0 0.824 1.65 .. Beryllium 0.240 0.165 0.330 1 Cadmium ND 0.165 0.330 .. .. Chromium 5,22 (1324 1.65 .. .. Cobalt 5.19 0.105 0.330 .. .. .. Conner 12.2 0.824 1.65 i .. .. .. Lead 3.98 0.165 0.330 Mercury ND 0.0059 0.132 ., .. .. ND 0324 1.65 .. .. .. .. Nickel 3.43 0 824 1 05 .. Selenium ND 0.824 1.65 Silver . ND 0.165 0.330 Thallium ND 0.165 0.330 Vanadium 17.1 0.824 1.65 Zinc 14.5 3.30 6.59 DRAFT REPO R911 Thu rem/Li- in rcpurl are change lim'ccl (1H .s'uh,i'cqim1t QC i?a/iz/rtliun or?nu/ clam review. Please me {have ram/Ix with {he Ilia! Ihqv may have nu: [acct/?nalized by the DRAFT REPORT, DATA SUBJECT TO CHANGE Page 6 of 23 1 County - . ubl . 1C Works 12232 s.w. Garden Place Apex Labs - Tigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax NWFF Project: 095 PO Box 138 Project Number: 095 Reported: Ph110malh, OR 97370 Projed Manager: Ross McMakin 08/12/17 06:23 ANALYTICAL SAMPLE RESULTS I Percent Dry Weight Reporting Analyle Result MDL Limit Unus Dilution Date Analyzed Method Notes US-1 (A7H0255-01) Matrix: 5011 Batch: 7080529 Solids 61.2 100 1.00 by Weight 1 08/10/17 07:39 EPA 8000C DRAFT REPORT The pruvm?cd mm rcpuri are am! are Tub/Lac: to Change hmc?d rm .s'n/M'cquem analyv?. QC validation ur?mn? dam rcvimr. Please uxc 1116.31? raw/M with 1th r/ml may have no! bcr'n?mtlizcd by {he DRAFT REPORT, DATA SUBJECT To CHANGE P386 7 0122 Apex Labs Polk County Public Works Y6318-012-l7 12232 SW. Garden Place Tigard, OR 97223 503-718-2323 Phone 503~718-0333 Fax PO Box 188 Philornmn. OR 97370 Project: 095 Project Number: 095 Projccl Manager: Ross McMakin Reporled: 08/12/17 06:23 QUALITY CONTROL (QC) SAMPLE RESULTS Organochlorine Pesticides by EPA 8081B Reporting Spike Source RPD Analyte Result MDL Limit Units Dil. Amount Result Limits RPD Limit Notes Batch 7080569 - EPA (G PC) Soil Blank (7080569-BLK1) Prcparcd: 08/09/17 13:35 Analyzed: 08/11/17 12:14 00: 8118111 Aldrin ND 0.000909 0.00182 mg/kg wet I w- alpha-811C ND 0.000909 0.00182 beta-BHC ND 0.000909 0.00182 delta-1311C ND 0.000909 0.00182 gamma-BHC (Lindane) ND 0.000909 0.00182 ciS-Chlordanc ND 0.000909 0.00182 trans-Chlordane ND 0.000909 0.00182 ND 0.000909 0.00182 ND 0.000909 0.00182 ND 0.000909 0.00 82 Dieldi?in ND 0.000909 0.00182 Endosull?an 1 ND 0.000909 0.00182 Endosull?an 11 ND 0.000909 0.00182 Endosulfan snll'ale ND 0.000909 0.00182 Endrin ND 0.000909 0.00182 Endrin Aldehyde ND 0.000909 0.00182 Endrin ketonc ND 0.000909 0.00182 l-leplachlor ND 0.000909 0.00182 l'lcplaChlor cpoxide ND 0.000909 0.00182 ND 0.00273 0.00545 Chlordane (Technical) ND 002 73 0.0545 (Total) ND 002 73 0.0545 Sm?r: 1456-71 YMX (Si/Hf) 57 Urn/m: 42?129 Wu [Jr/minus Ix 113 "0 LCS (70805694381) Prepared: 08/09/17 l3135 Analyzed: 08/11/17 12:31 005 EPA 811818 Aldrin 0.0416 0.00100 0.00200 wet 1 0.0500 83 45-13(3% alpha-1311C 0.0478 0.00100 0.00200 96 45-137% Q41 0.0473 0.00100 0.00200 95 50-136% delta-1311C 0.0488 0.00100 0.00200 97 Q-41 gamma-1311C (Lindanc) 0.0519 0.00100 0.00200 104 49-135% cis~Chlordanc 0.0508 0.00100 0 00200 102 54-133% trans-Chlordane 0.0502 0.00100 0.00200 100 53?135% 0.0595 0.00100 0.00200 119 56-139% Q-41 DRAFT REPORT The are 1' and are .ruhjcci to change 11mm! (in .m/mequwri anu/yxiax QC i'a/ft/crliwi (Jr/inn! dam review. ['lmxe me Ilium rem/Ix Hit/7 {/10 that they rircrr' have 1701' bec'Ir/ina/r'mr/ by [/16 [allow/my DRAFT REPORT, DATA SUBJECT TO CHANGE Page 8 of 22 Apex Labs Polk County Public Works Y6318-012-l7 12232 S.W. Garden Place [Qq Tigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax NWFF PO Box 188 Phllomath.OR 97370 095 Project Number: 095 Project: Project Manager: Ross McMakin Reported: 08/12/17 06.23 QUALITY CONTROL (QC) SAMPLE RESULTS Organochlorine Pesticides by EPA 8081B Reporting Spike Source RPD Analytc Result Limit Units D11. Amount Result Limits RPD Limit Notes Batch 7080569 - EPA (GPC) Soil LCS (70805694351) Prepared: 08/09/17 13:35 Analyzed: 08/11/17 12:31 005 EPA 8118113 0.0478 0.00100 0.00200 tug/kg wel 96 56-134% 0.0638 0.00100 0.00200 128 50v141% 0.0572 0.00100 0.00200 114 56?136% Endosull?anl 0.0562 0.00100 0.00200 112 52?132%' Endosullhn 11 0.0615 0.00100 0.00200 123 53~l34% Q'4l Endosullhn sulfate 0.0565 0.00100 0.00200 113 55-136"n 0'41 0.0634 0.00100 0.00200 127 Endrin Aldehyde 0.0518 0.00100 0.00200 104 35?137% Endrin kctonc 0.0641 0.00100 0.00200 123 55'136% Q41 Heptachlot? 0.0530 0.00100 0.00200 106 47-136% -..- Q-?ll HCptachlor CpUdeC 0.0502 0.00100 0.00200 100 52?136% 0.0649 0.00300 0.00600 130 52-143"u Surr: Recovery: 80% Urn/M: 112-I29 "a Ui/mfun: IX I'Jccash/nrub/plmuv/ 65?15/ LCS Dup (708056943801) Prepared: 08/09/17 13:42 Analyzed: 08/11/17 12:49 C-OS, Q-19 EPA 8081 Aldrin 0.0420 0.00100 0.00200 mg/kg wet 1 0.0500' 84 45-136% 1 30% alpha-811C 0.0448 0.00100 0.00200 90 45-137?u 6 30% (2-41 bcIa?Bl-IC 0.0444 0.00100 0.00200 1' 89 50-13601: 6 30% deltaaBl-{C 0.0463 0.00100 0.00200 93 47-139% 5 30% 0'41 gamma-BHC (Lindanc) 0 0500 0.00100 0.00200 100 49-135% 4 30% CiS-Chlordanc 0.0475 0 00100 0.00200 95 54-133% 7 30% truns~Chlordane 0.0484 0.00100 0.00200 97 53?135% 4 30% 0.0558 0.00100 0.00200 112 56-139"n 6 30% 0.0468 0.00100 0.00200 94 56?134% 2 30% 0.0596 0.00100 0.00200 1' 119 50-141?u 7 30% 0.0530 0.00100 0.00200 106 56-136% 8 30% Endmull?anl 0.0530 0.00100 0.00200 106 52-132% 6 30% Endosull?an 11 0.0570 0.00100 0.00200 114 53-134% 8 30% Q41 Endosull?an sulfate 0.0542 0.00100 0.00200 108 55-136% 4 30% Q41 0.0590 0.00100 0.00200 118 56-140% 7 30% Aldehyde 0.0494 0.00100 0.00200 99 35?137% 5 30% Endl?in ketonc 0.0584 0.00100 0.00200 117 55-136% 9 30% (2'41 l?lcptachlot' 0.0520 0.00100 0.00200 104 47~136% 2 30% DRAFT REPORT The rm'Il/M? pmwc/cr/ in mm rupurt at? 1? and are tub/cc; to change hmer/ rm (malty/x. QC unlit/alum (lam rev/ctr. Hume rm: theme rem/Lt: I/vc I/m/ r/rcy may [mm Iman?nal/Zcr/ by the lahururrmy Page 9 of22 DRAFT REPORT, DATA SUBJECT TO CHANGE Polk Count PUblic - ?5318-01247 Works 12232 SW. Garden Place Apex Labs Tigard, OR 97223 503-718-2323 Phone 503?713-0333 Fax NWFF Pro?jcul: 1195 PO Box 188 Project Number: 095 Reported: l?hilomalh. OR 97370 Project Manager: ROSS MCMakin 08/12/17 06:23 QUALITY CONTROL (QC) SAMPLE RESULTS Organochlorine Pesticides by EPA 80818 I . Reporting Spike Source RPD Analylc Result MDL Limit Units Dil. Amount Result Limits RPD Limit Notes Batch 7080569 - EPA (GPC) Soil LCS Dup (7080569-BSD1) Prepared: 08/09/17 13:42 Analyzed: 08/11/17 12:49 C-OS. Q?l9 PA 80813 Heptachlor CpOdeC 0.0482 0.00100 000200 mg/kg wet 96 52?136% 4 3000 0.0709 0.00300 0.00600 142 52-14 9 30% .N'url': Rccm'r'ry: 75 Li'mirx.? 42?129 Diirtrimi: [Moduli/umhiphuuyl (Surr) 65?]51' DRAFT REPORT Tin: raw/ixpmw?dud in I/i/x rcpm?r are l?leL/rW/NA Rl? and are .i'uhjcci in change hatred (m andwiv. QC MHz/mm: (It/inn! dam rel-ricii?. Flame me More with My that they may have nor llemil?lth-ZL?U, by {he laboratory DRAFT REPORT, DATA SUBJECT TO CHANGE Page ?0 Apex Labs Polk County Public W0 Y6318-012-l7 12232 S.W. Garden Place Tigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax PO Box l88 Philomath, OR 97370 Protect Number. 095 Reported: Project: 095 Project Manager: Ross McMakin 08/12/17 06 :23 QUALITY CONTROL (QC) SAMPLE RESULTS I Organophosphorous Pesticides (OPPs) by EPA 82700 (GCIMS) I Reporting Spike Source RPD Analyte Result MDL Limit Units Dil. Amount Result Limits RPD Limit Notes Batch 7080573 - EPA 3546 Soil Blank Prepared: 08/10/17 l248 Analyzed: l4:20 8270B OPP methyl (Guthion) ND 00250 0 0500 mg/kg wet Chlorpyrilbs 0.0265 0.0250 0.0500 3-0th Coumaphos ND 0,0250 0,0500 2-- Denteton 0 ND 0.0250 0.0500 Dcmeton ND 0.0250 0.0500 Diazinon ND 0.0250 0.0500 chl?tlorvos ND 00250 0.0500 Dlmelhoate ND 0.0250 0.0500 DtSUIioton ND 00300 0.0600 EPN ND 0.0250 0.0500 (Pmphos) ND 0.0250 0.0500 licnmilf?othion ND 00250 0.0500 Ft?nlhlon ND 00250 0.0500 Malathion ND 0.0250 0,0500 ND 0.0250 0.0500 Methyl parathion ND 0.0250 0.0500 -2- Mevmphos (Phosdrin) ND 0.0250 0.0500 Monocrotophos ND 00250 0 0500 Naled (Dibrom) ND 00250 0.0500 Parathion. ethyl ND 00250 0.0500 Phorate ND 00250 0.0500 Ronnel (Fenehlorphos) ND 0.0250 0.0500 Sulf?otep ND 00250 0 0500 Sulprofos (Bolstur) ND 0.0250 0.0500 TEPP ND 0100 0.200 'l?Clrachlorvinphos (Ration) ND 00250 0.0500 'I?Okuthion (Prothiofos) ND 0.0250 0.0500 Trichloronate ND 0.0250 0.0500 'I'I't?hittyl phosphate St?) Lmiitx.? 50?14] Va Dilution: Trtp/wny/ plump/rate (Surr) 83 LCS (7080573-831) Prepared: 08/l0/l7 H148 Analyzed: 08/10/l7 14:57 82700 OPP Azinphos methyl (Guthlon) 0.344. 0.0250 0 0500 mg/kg wet 0.400 86 38-156% Chlorpyrilbs 0.379 0.0250 0 0500 95 47- l40% 3-02 DRAFT REPORT The ram/M tht?x report are and are subject to change braved (m QC validation rtt'?ntt/ ct'utct review. I'lcm?c ttxe (Imxe results with the that they may have not lwen?ttulfzed by the [abut-amt)" DRAFT REPORT, DATA SUBJECT TO CHANGE Page 11 ol?22 Polk County Public Works Y6318-012?l7 12232 S.W. Garden Place Apex Labs ?gamma 97223 503-718-2323 Phone 5113-7184633 Fax NWFF Project: 095 PO Box 188 Project Number: 095 Reported: Philomath, OR 97370 Project Manager: Ross McMakin 08/12/17 06:23 QUALITY CONTROL (QC) SAMPLE RESULTS I Organophosphorous Pesticides (OPPs) by EPA 82700 (GCIMS) Reporting Spike Source RPD Analytc Result MDL Limit Units Dil, Amount Result Limits RPD Limit Notes Batch 7080573 - EPA 3545 Soil LCS (70805734351) Prepared? 08/10/17 11:48 Analyzed: 08/10/17 14:57 82701) OPP Coumaphos 0.393 0.0250 0.0500 mg/kg wet 98 37-160% Dcmemn 0 0.0805 0.0250 0.0500 0.0976 83 43-117% 0237 0.0250 0.0500 0,268 88 Diazinon 0.356 0.0250 0.0500 0.400 89 42-134% Dichlorvos 0.418 00250 0.0500 105 39?142% Dimethoate 0.353 00250 0.0500 . 88 16-139% Disult'oton 0.377 0.0300 0.0600 94 28-144% lil?N 0.404 0.0250 0.0500 101 44-137% Ethoprophos (Proplios) 0.396 0.0250 0.0500 99 47-128% .-- Fenis?tilt'othion 0.419 0.0250 0.0500 105 27-147% Q41 0.366 0.0250 0.0500 91 44-134% Malzithion 0.359 00250 0.0500 90 46-137% 0.395 0.0250 0.0500 99 0-153% Methyl parathion 0.393 0.0250 0.0500 98 49-138"o Mevinphos (Pliosdrin) 0.363 0.0250 0.0500 91 12- 76% Monocrotophos 0.347 00250 0.0500 87 65-135% Nalcd (Dibrom) 0.351 0.0250 0.0500 -.- 88 0-174% Paratliion, ethyl 0.377 0.0250 0.0500 94 50?139% Phorate 0.389 0.0250 0.0500 97 23-142" 0 Ronncl (Fenchlorpl?ios) 0.356 0.0250 0.0500 89 45-138% 0.376 0.0250 0.0500 94 52-126% Sulprol'os (Bolstar) 0.381 0.0250 0.0500 95 48- 1 39% TEPP 0.333 0 100 0,200 83 30-150% 'l?ctrachlorvinphos (Rabon) 0.353 0.0250 0,0500 88 54-129% Toktithion (Protliiol?os) 0.363 0.0250 0.0500 91 45-136% 0.368 0.0250 0.0500 92 37-140% Hilarity!phavp/rule (Sm-r) - 88 [.imilx.? 50-14] Dilution: IX 619430 I LCS Dup (7080573-BSDI) Prepared: 08/10/17 11:48 Analyzed: 08/10/17 15:35 Q-19 82701) OPP Azinphos methyl (Guthion) 0.365 0.0250 0.0500 mg/kg wet 1 0,400 91 3845600 6 20% Chlorpyritbs 0.371 0.0250 0.0500 93 47-14000 2 20% 3-02 Coumapl?ios 0.407 0.0250 0.0500 102 37-160% 3 20% Demcton 0 0.0849 0.0250 0.0500 0.0976 87 43-117% 5 20% DRAFT REPORT The rum/Ix [Jrrii-?idcr/ [hm report are 1? mid are .i'uhjucr to change boxed rm .i'itb.i'cqr.'wu trim/r5115: Qt? validation (Jr/11m! dram rev/cw. I?i'c?m'c: my thew rem/Ix with 1hr rim: they may have not [mm/?nalized by the {aborurm?y DRAFT REPORT, DATA SUBJECT TO CHANGE Page ?2 0m County Public Works Y6318-012-17 12232 73 Ap 6X Labs Tigard, OR 97223 503-718-2323 Phone 503?718-0333 Fax NWFF Project: (195 PO Box 188 Project Ntimbcr: 095 Reported: Philomath, OR 97370 Project Manager: R055 McMaktn 08/12/17 06:23 QUALITY CONTROL (QC) SAMPLE RESULTS I Organophosphorous Pesticides (OPPs) by EPA 82700 (GCIMS) chorting Spike Source RPD Analylc Resuit MDL Limit Units Dil. Amount Result Limits RPD Limit Notes Batch 7080573 - EPA 3546 Soil LCS Dup (7080573-BSDI) Prepared108/10/17 11:48 Analyzed: 08/10/17 15:55 Q-19 82700 OPP 0.225 0.0250 0.0500 tug/kg 0.268 84 5 20% Diazinon 0 358 0.0250 0.0500 0.400 89 42-134?] 0 0.6 20% Dichiorvos 0.401 0.0250 0.0500 100 39-142% 4 20% Dimcthoatc 0.353 0.0250 0,0500 88 16?139% 0.02 20% Disulfoton 0.362 0.0300 0,0600 91 28?144% 4 20% EPN 0,413 0 0250 00500 103 44?137% 2 20% Ethoprophos (Prophos) 0.377 0 0250 0.0500 1 94 47-128% 5 20% Fensulfothion 0.436 0.0250 0.0500 109 27-147% 4 20% Q41 0.363 0.0250 0.0500 91 44-134% 0.7 20% Malathion 0.347 0.0250 0.0500 87 46?137% 3 20% 0.392 0.0250 0.0500 98 0-153% 07 20% parathion 0.388 0.0250 0.0500 97 49-138% 1 20% Mcvinphos (Phosdrin) 0.376 0.0250 0,0500 94 12- 176% 3 20% Monocrotophos .328 0 0250 0.0500 .32 65? 35% 6 20% Nalcd (Dibrom) 0.371 0 0250 00500 93 0-174"o 5 20% Parathion. ethyl 0.375 0.0250 0.0500 94 50-139% 0.5 20% Phoratc 0.394 0.0250 0.0500 99 23-142% 1 20% Ronncl 0.349 0.0250 0.0500 87 45-138% 2 20% Sulfatep 0.380 0.0250 0.0500 95 52-126% 1 20% Sulprofos(13013tat') 0.364 0.0250 0.0500 91 48-139% 4 20% TEPP 0.331 0.100 0.200 83 30-150% 0.8 20% 'l?ctrachlorvinphos (Rabon) 0.354 0.0250 0.0500 89 54-129% 05 . 20% (Prothiofos) 0.356 0.0250 0,0500 89 45-136"o 2 20% Trichloronatc 0.357 0.0250 0.0500 89 37-140% 3 20% Sm?i': 771/71701/plrm'pt'iulc Runway; 81") Limilx.? 50-[4/ Dilution: Ix (Smr) 0?5 60-13!) DRAFT REPORT 7711: rcxiim pruridctl in rcpm?l are RY and are In change boxed rm .s'nbxt'qrmm (nm?itwk, QC ru?jilml dam rcw'eii'. I?lwm?c me Ilium raw/M with the rim! may have heart/?nalized by Ike DRAFT REPORT. SUBJECT TO CHANGE Page ?3 0m . . Polk County Public Works 12232 SW. Garden Place Apex Labs Tigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax NWFF Project; (195 1?0 130x 183 Project Number. 095 Reported: Philomath, OR 97370 Project Manager: Ross McMakin 08/12/17 06:23 QUALITY CONTROL (QC) SAMPLE RESULTS I Total Metals by EPA 6020 (ICPMS) Reporting Spike Source RPD Analyte Result MDL Limit Units Dil. Amount Result Limits RPD Limit Notes Batch 7080565 - EPA 3051A Soil Blank (7080565-BLK1) Prepared: 08/10/17 09:23 Analyzed: 08/11/17 18:41 EPA 6020A Antimony ND 0500 .00 mg/kg wet 10 Arsenic ND 0.500 1.00 Barium ND 0.500 1.00 Beryllium ND 0100 0.200 Cadmium ND 0100 0.200 Chromium I ND 0,500 1,00 Cobalt ND 0100 0,200 Copper ND 0.500 1.00 Lead ND 0100 0.200 Mercury ND 0.0400 0.0800 Molybdenum ND 0.500 1.00 Nickel ND 0.500 1.00 Selenium ND 0. 500 .00 Silver ND 0. 100 0,200 Tliallium ND 0100 0.200 Vanadium ND 0500 1.00 Zinc ND 2.00 4.00 LCS (70805654331) Prepared: 08/10/1709123 Analyzed: 08/11/17 18:45 EPA 6020A Antimony 26.9 0.500 1.00 rug/kg wet 10 25.0 108 30-120% Arsenic 51,4 0.500 1.00 50.0 103 Barium 51.7 0.500 1.00 103 Beryllium 27.0 0.100 0.200 25.0 108 Cadmium 537 0.100 0.200 50.0 107 Chromium 48.8 0.500 1.00 97 Cobalt 52.4 0.100 0.200 105 Copper 52.5 0.500 1.00 105 Lead 55.7 0.100 0.200 111 Mercury 1.12 0.0400 0.0300 1.00 12 Molybdenum 24.9 0.500 1.00 25.0 100 Nickel 52 1 0.500 1.00 50.0 104 Selenium 28.9 0.500 1.00 25,0 116 Silver 259 0.100 0.200 104 Thallium 28.0 0.100 0.200 112 DRAFT REPORT The rum/Ix in Iii/Zr report are l?lt?lfHA/llN/JRY and to change hatred mi .ru/u?eqm?iil (maliwr'x. QC (H?find/ dam review. l?lr'm'u rim rum/1x 11'th 1th 1'11le they may have not [weir/limited by {he labor-army DRAFT REPORT, DATA SUBJECT TO CHANGE Page ?4 ??22 Apex Labs Polk County Public Works 12232 SW. Garden Place Tigard. OR 97223 503-718-2323 Phone 503-718?0333 Fax I .19 PO Box 188 Philomath, OR 97370 Project: 095 Project Number: 095 Project Manager: Ross MeMakin Reported: 08/12/1706i23 QUALITY CONTROL (QC) SAMPLE RESULTS Total Metals by EPA 6020 (ICPMS) Reporting Spike Source RPD Analyte Result MDL Limit Units Di]. Amount Result Limits RPD Limit Notes Batch 7080565 - EPA 3051A Soil LCS (7080565-881) Prepared: 08/10/17 09:23 Analyzed: 08/11/17 18:45 EPA 6020A Vanadium 49.9 0.500 1.00 mg/kg wet 50.0 100 Zine 53.1 2 00 4.00 106 Duplicate (7080565-DUP1) Prepared: 08/10/17 09:23 Analyzed: 08/11/17 20:05 QC Source Sample: (.471111255-01) EPA 61120A Antimony ND 0.795 1.59 mg/kg dry 10 ND --. 40% Arsenic 2.62 0.795 1.59 2.12 21 40% Q-04 Barium 85.7 0.795 1.59 53.0 47 40% Q-04 Beryllium 0.249 0.159 0.318 .-- 0.240 -.- 3 40% Q-OSJ Cadmium ND 0.159 .318 ND 40% Chromium 7.46 0.795 1.59 5,22 35 40% C2434 Cobalt 4.57 0.159 0,318 5,19 13 40% Q-04 Copper 15.9 0.795 1.59 12.2 26 40% Q-04 Lead 3.60 0.159 0.318 3.98 10 40% 0-04 Mercury ND 00636 0.127 ND 40% I Molybdenum ND 0795 1.59 ND 40% Nickel 5.58 0.795 1.59 3.48 46 40% Q-04 Selenium ND 0.795 ND 40% Silver ND 0.159 0.318 ND 40% Thallium ND 0.159 0,318 ND 40% Vanadium 22.3 0.795 1.59 17.1 26 40% Zinc 22.0 3.18 6.36 14.5 41 40% Q-04 Matrix Spike (7080565-MSI) Prepared: 08/10/17 09:23 Analyzed: 08/11/17 20: 10 QC Source Sample: (Mi-10255-0!) EPA 6020A Antimony 41.8 0.853 1.71 trig/kg dry 10 426 ND 98 75-125% --. Arsenic 94.2 0.853 1.71 85.4 2.12 108 Barium 164 0.853 1.71 53.0 130 0'04 Beryllium 46.7 0,171 0.341 42.6 0.240 109 Cadmium 90.5 0,171 0.341 85.4 ND 106 Chromium 95.2 0.853 1.71 5.22 105 Cobalt 96.7 0.171 0 341 19 107 Copper 115 0.853 1.71 12.2 120 Q-04 DRAFT REPORT The ream/Ix provided in this reporl are and we nix/{feet In change hatred (m QC wr/n/m/on urjimr/ dam rev/cw, I ?lcme we {have rum/M w/Ih {he l/ml ?my may have not heel/finalized by lhe DRAFT REPORT, SUBJECT TO CHANGE Page 15 0122 Apex Labs Polk County Public Works 12232 S.W. Garden Place Tigard,OR 97223 503-718?2323 Phone 503-71841333 Fax PO Box 188 Philomalh. OR 97370 Project: 095 Project Number: 095 - Reported: Project Manager: Ross McMakin 08/12/17 06:23 QUALITY CONTROL (QC) SAMPLE RESULTS I Total Metals by EPA 6020 (ICPMS) I Reporting Spike Source RPD Analyte Result MDL Limit Units Dil. Amount Result Limits RPD Limit Notes Batch 7080565 - EPA 3051A 5011 Matrix Spike (70805654181) Prepared: 08/10/17 09:23 Analyzed: 08/11/17 20:10 QC Sample: (A7110255-01) EPA 6020A Lead 97.4 0.171 0.341 mg/kg (lry 3.98 109 Mercury 1.84 0.0683 . 0.137 1.7] ND 108 Molybdenum 43.4 0.853 1.71 42.6 ND 102 Nickel 95.5 0.853 1 71 85.4 3.48 108 Selenium 49.8 0.853 171 426 ND 117 Silver 43.6 0.171 0,341 ND 102 Thallium 46.5 0.171 0.341 ND 109 Vanadium 118 0.853 1.71 85.4 17.1 119 . Zinc 119 3.41 6.83 14.5 122 0'04 DRAFT REPORT The rem/M ,nmw?dca' in Ilifx repay! are l?li?lflJA/IflV/lk1' um! are .i'u/y'ucr to change based on unu?'xis?. QC var/Idaho? (Ir/inn! dam review. Weave use Illexc rcxu/M' will; {he they may have HUI beerrfinu/fzcd [2.1/1th DRAFT REPORT, DATA SUBJECT TO CHANGE Page 16 01?22 Polk County Public Om 12232 s.w. Garden Place Apex Labs Tigard, OR 97223 503-718?2323 Phone 503-718-0333 Fax NWFF Project: 095 PO BOX 188 Project Number: 093 Reported: 97370 Project Manager: Ross McMakin 08/12/17 06:23 QUALITY CONTROL (QC) SAMPLE RESULTS I Percent Dry Weight 1 Reporting Source RPD Analylc Result MDL Limit Units Dil. Amount Result 0AREC Limits RPD Limit Notcs Batch 7080529 - Total Solids (Dry Weight) Soil DRAFT REPORT Thu run/Ixprovided in (him rupnri am! my KthL?L'l change based rm (mu/?ix, QC i'cilicltiliim nr?finril dam review. l?lt'm?e 1m: Ilium: mm [11? I/ml Ilwy magi have nor [Jae/ifimtlizad by tho laboratory DRAFT REPORT, SUBJECT TO CHANGE Page '7 ??23 Apex Labs Tiga rd, OR 97223 Polk County Public Works Y6318?012-l7 0.9 12232 S.W. Garden Place 503-718-2323 Phone 503-718-0333 Fax NWFF PO Box 188 PhilomaIILOR 97370 Project; 095 Project Number: 095 l?rojeel Manager: Ross MeMakin Reported: 08/12/17 06:23 SAMPLE PREPARATION INFORMATION Organochlorine Pesticides by EPA 8081B Prep: EPA (GPC) Sample Default RL Prep Lab Number Matrix Method Sampled Prepared lnitial/Final Initial/Final Factor Batch: 7080569 Soil EPA 808113 08/08/17 11:50 08/09/17 13:35 10109g/40mL 10g/5mL 7.93 I Organophosphorous Pesticides (OPPs) by EPA 8270B Prep: EPA 3546 Sample Del?ault RL Prep Lab Number Malrlx Method Sampled Prepared Initial/Final Initial/Final Factor Batch: 7080573 A7HOZSS-01 Soil 8270B OPP 08/08/17 11:50 08/10/17 11:48 1.14g/5mL. 8.77 $011 82701) Olr?l) 08/08/17 11:50 08/10/17 11:48 1.14g/5mL 8.77 I Total Metals by EPA 6020 (ICPMS) Prep: EPA 3051A Sample Default RL Prep Lab Number Matrix Method Sampled Prepared Initial/Final 191113?me Factor Batch: 7080565 A7l'l0255?01 Soil EPA 6020A 08/08/17 11:50 08/10/17 09:23 0:496g/50mL 0.5g/50mL 1.01 I Percent Dry Weight Prep: Total Solids (Drv Weiqht) Sample Default RL PFEP Lab Number Matrix Method Sampled Prepared Initial/Final Initial/Final Factor Batch: 7080529 Soil EPA 8000C 08/08/17 11250 08/09/17 13:45 NA DRAFT REPORT The ram/Ix prov/deal in Ilrr?x repur/ are 1? and are 511/7]ch In change hmrer/ on QC r'rr/r'r/cuirm urjimr/ r/mu rev/en: Home use I/icxc rem/H 1/10 ruu/r?rxlum/iug r/ra.? {hey may have mu been?nrr/fzer/ by 1/10 la/Jru'urmjy' DRAFT REPORT, DATA SUBJECT TO CHANGE Page 18 0f22 Apex Labs Polk County Public Works Y63l8-Ol2-l7 12232 SW. Garden Place Tigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax NWFF Project: 095 PO Box 188 Protect Number: 095 Reported: Philomath, OR 97370 Project Manager: Ross McMakin 08/12/17 06:23 Notes and De?nitions Quali?ers: 8-02 Analyte detected in an associated blank at a level between one-halfthe MRL and the MRL (See Notes and Conventions below.) C-OS Extract has undergone a GPC (Gel-Permeation Chromatography) cleanup per EPA 3640A. Reporting levels may be raised due to dilution necessary for cleanup. Sample Final Volume includes the GPC dilution factor, see the Prep page for details. 1 Estimated Result Result detected below the lovvest point of the calibration curve, but above the specified MDL. Q-04 Spike recovery and/or RPD is outside control limits due to a non-homogeneous sample matrix. Q-US Analyses are not controlled on RPD values "from sample and duplicate concentrations that are below 5 times the reporting level, 9 Blank Spike Duplicate (BSD) sample analyzed in place of Matrix Spike/Duplicate samples due to limited sample amount available for analysis. Q-4l Estimated Results. Recovery ofContinuing Calibration Verification sample above upper control limit for this analyte. Results are likely biased high. R-02 The Reporting Limit for this analyte has been raised to account for interference from coeluting organic compounds present in the sample. R-04 Reporting levels elevated due to dilution necessary for analysis. Surrogate recovery for this sample is not available due to sample dilution required from high analyte concentration and/or matrix interference. . S-OS Surrogate recovery is estimated due to sample dilution required for high analyte concentration and/or matrix interference. Notes and Conventions: DET Analyte DETECTED - ND Analyte NOT DETECTED at or above the reporting limit NR Not Reported dry Sample results reported on a dry weight basis. Results listed as ?wet' or without 'dw'clesignation are not dry weight corrected. RPD Relative Percent Difference MDL [f MDL is not listed, data has been evaluated to the Method Reporting Limit only. WMSC Water Misciblc Solvent Correction has been applied to Results and MRLs for volatiles soil samples per EPA 8000C. Batch Unless specifically requested. this report contains only results for Batch QC derived from client samples included in this report. All QC analyses were performed with the appropriate Batch QC (including Sample Duplicates, Matrix Spikes and/or Matrix Spike Duplicates) in order to meet or exceed method and regulatory requirements. Any exceptions to this will be qualified in this report Complete Batch QC results are available upon request. In cases where there is insufficient sample provided for Sample Duplicates and/or Matrix Spikes. a Lab Control Sample Duplicate (LCS Dup) is analyzed to demonstrate accuracy and precision ofthe extraction and analysis. Blank Apex assesses blank data for potential high bias down to a level equal to V: the method reporting limit (MRL), except for conventional Policy chemistry and HCID analyses which are assessed only to the MRL. Sample results ?agged with a or 8-02 qualifier are potentially biased high it?they are less than ten times the level found in the blank for inorganic analyses or less than five times the level found in the blank for organic analyses. For accurate comparison ol'volatilc results to the level found in the blank; water sample results should be divided by the dilution factor, and soil sample results should be divided by 1/50 ofthe sample dilution to account for the sample prep factor. RAFT REPORT The in Ilrrli' report are Rl? and (111? subject to change hatred on .rri/iscqircrir analysis. QC validation dam review. Please use I/ws?t? rem/Lt n'ilh I/ic ruir/r'm'runa'mg I/iru [hey may have by {he lubnrulory DRAFT REPORT, DATA SUBJECT TO CHANGE Page l9 of 22 i - Polk County Public Works 12232 s.w. Garden Place Apex Labs ?grim 97223 503-713-2323 Phone 503-713?0333 Fax NWFF Project: 095 PO Box l88 Project Number: 095 Reported: Philomalh, OR 97370 Project Manager: Ross MeMakin 08/12/17 06:23 Results qualified as reported below the MRL may include a potential high bias ifassociated with a or 8?02 qualified blank. and 8-02 qualifications are not applied to] qualified results reported below the QC results are not applicable. For example, Recoveries for Blanks and Duplicates, RPD for Blanks, Blank Spikes and Matrix Spikes, etc. Used to indicate a possible discrepancy with the Sample and Sample Duplicate results when the is not available, In this case, either the Sample or the Sample Duplicate has a reportable result for this analyte, while the other is Non Detect (ND). DRAFT REPORT The provided in {hit report are PREIJMIM4 Rl' and are .virbfucl in change hunted (in trim/twin QC t'rilir/ruirm ru?jimil dam review. l?lem?c m?e thew reat'iiltx with the I/ml they may have not hru?ii?rrm?izcd by ihe DRAFT REPORT, DATA SUBJECT TO CHANGE Page 20 RI s. .Ikl Od V_ch1 imoa OJ, ,4 bayqnx 1m 1mm 30 APEX LABS CHAIN OF CUSTODY 1.7335 3' 11'. [Winn Tigm?n?. 9731} I?ll: Fm: Lam/47W)ng (Inc: \m Pm i Pmicci Wigwam?) A: I 0?15? mm VD eat?: 1W mi 617270 Sinnpiui NW9: ('3'va . . nualmm [Dug/Ln: AmeJuL/m my all [walnut/mam}! mu Inn: (fat/J mt": mupumwapun iM'Qlfl DNH pm'm] u} main/m am pun A 31 am undm 311:]; u; pnpjurud w/mw mu ZZJO 932d 34m,- lmruliun(\Ihgr,AiigNwma? Turr- Mound :10 335mm; Days NH I'll LYN- [my 3 Day TAT Requested lL?ia vie) 4 DAY 5. DAY SAMPLES ARE HELD FUN HATS mum If.? '1 ?Ln-1n: In: .. Sunni" c: l'rynL-d Nana r?4 L'Tf?ai um "umpum: {'rmuunx' MW I: ,2 Dale: i 11:13 me' (1 1 Primal . - i'x-mpam. Av) u} FF r'numn'?: 'l Alp/{w 881 X08 Od HO ?lemOlNd quq xadV g60 Ilaqull1N130!bJ(] zlnafmd umewnw :m?euew 133mm S60 mo-su-ws auoud am 110 ?pw?LL 33PM uapwg ZEZZI ?2390 :pnumlau 3% 5310M 3and Alunog >H0d Polk County Public Works Y63lS-Ol2~l7 12232 S.W. Garden Place Apex Labs ?gm, OR 97223 503-718-2323 Phone 503-7l8-0333 Fax Project: 095 PO Box Hill Project Number: 095 Reported: Philomalh, OR 97370 Project Manager: Ross McMakin 08/12/l7 06:23 APEX LABS COOLER RECEIPT FOR Client: NANFF . Elemenl Projectll?rojeet ll: 5 info: 7 Datefl'ime Received: Y?ll By: Delivered by: Cooler Inspection Inspected by: Ml '7 (EB ?ll Chain ol?Custody Included? Yes? No Custody iSeails?? Signed/Dated byClient'? Yes? Signed/Dated by Apex? Yes zNo Cooler fl] Cooler #2 Cooler #3 Cooler #4 Cooler #5 Cooler #6 Cooler #7 Temperature (deg. C) Received on ice? 'l'etn .Blanks?.? ll {9 lee Type: Gel cal/Other) Condition: . Cooler oul ol?lemp? (VIE) Possible reason why: ll'some coolers arc in temp and some out 'ere green dot applied oft mperaturc lies?? Yes/Nola)? Samnles Inspection: inspected by: g; All Samples Intact? Yesmn Nonm Comments: Bottle agree? Yes No Comments: Containers/Volumes Received Appropriate for Analysis? No Commenrs: Do VOA Vials have Visible Yes No NA . . Water Samples: pH Checked and Appropriate (except VOAS): Comments: Additional Int?rn?malion; ital-teled by: W?x Cooler Inspected by: See Project Contact Form: 1' I, Clo-Elli Lt DRAFT REPORT The ram/1.x- provider] in thin: P'Uptll?l are Ill' and are ?Inject Iu Change baxcrl on .vuhrequeitr nought-Lt: QC validation or?ttu/ dam review. Please we {have it'll/1 {he rim! {/1th may have nor bec'tt?nalizert' by the DRAFT REPORT, DATA SUBJECT TO CHANGE Page 32 CDC SULFOTEP - International Chemical Safety Cards - NIOSH Page 1 of4 Control and Prevehtlon CDC 24/7: Saving LIVES- Peop'em Polk County Public Works Y6318-012-l7 /?losH' Promoting productive workplaces through safety and health research ICSC: 0985 Thiodiphosphoric acid tetraethyl ester Ethyl thiopyrophosphate AS 3689-24?5 Tetraethyl dithiopyrophosphate (TEDP) RTECS UN 1704 Molecular mass: 322.30 EC 015?027?00?3 ICSC 0985 October 18, 1999 Validated TY ES 0 ACUTE FIRST PREVENTION FIRE FIGHTING EX POS RE Combustible. Gives off NO open ?ames. Water 'spray, foam, FIRE irritating or toxic fumes powder, carbon dioxide. (or gases) in a fire. Container may explode In case of fire: keep EXPLOSION Violently in heat of fire. drums, etc., cool by spraying with water. STRICT IN ALL CASES CONSULT AVOID EXPOSURE OF A EXPOSURE ADOLESCENTS AND Blue skin. Dizziness. Ventilation, local exhaust, Fresh air, rest. Arti?cial Drowsiness. Headache. or breathing protection. respiration may be Pupillary constriction, needed. Refer for medical muscle cramp, excessive attention. 0 INHALATION salivation. Sweating. Laboured breathing. Nausea. Convulsions. Unconsciousness. Weakness. See Ingestion. 8/16/2017 CDC - SULFOTEP International Chemical Safety Cards NIOSH pg?p 4 Polk County Public Works Y6318-012-l7 MAY BE Protective gloves. Rinse and then wash skin Redness. Sweating and Protective clothing. with water and soap. Refer OSKI twitching in the area of for medical attention. absorption. (Further see Inhalation). Redness. Pain. Pupillary Face shield or First rinse with plenty of constriction. protection in combination water for several minutes 9 EYES with breathing protection. (remove contact lenses if easily possible), then take to a doctor. Abdominal cramps. Do not eat, drink, or Induce vomiting (ONLY 0 ON Confusion. Diarrhoea. smoke during work. Wash IN CONSCIOUS Vomlting. Loss of appetite. hands before eating. Refer for (Further see Inhalation). medical attention. SPILLAGE DISPOSAL STO RAG PACKAGING LABELLING Ventilation. Collect leaking liquid in sealable containers. Absorb remaining liquid in dry sand or inert absorbent and remove to safe place. Personal protection: complete protective clothing including self? contained breathing apparatus. Do NOT let this chemical enter the environment. Dry. Well closed. Separated from strong oxidants, food and feedstuffs . Keep in a well- ventilated room. Do not store in metal containers. Store in an area without drain or sewer access. Provision to contain ef?uent from fire extinguishing. Do not transport with food and feedstuffs. Marine pollutant. symbol symbol R: 27/28?50/53 S: UN Hazard Class: 6.1 UN Packing Group: II Prepared in the context of cooperation between the International Programme on Chemical Safety 81 the Commission of the European ICSC: 0985 Communities (C) IPCS CBC 1994. No modifications to the International version have been made except to add the OSHA PELs, NIOSH RELs and NIOSH IDLH values. ICSC: 0985 SU LFOTE 8/16/2017 CDC SULFOTEP - International Chemical Safety Cards NIOSH Page 3 of4 A PHYSICAL APPEARANCE: PALE YELLOW LIQUID WITH CHARACTERISTIC ODOUR. PHYSICAL DANGERS: CHEMICAL DANGERS: The substance decomposes on heating producing highly toxic fumes of phosphorous oxides and sulfur oxides . Reacts with strong oxidants. Attacks iron, some forms . of plastic, rubber and coatings. OCCUPATIONAL EXPOSURE LIMITS: OSHA PEL: TWA 0.2 mg/m3 skin NIOSH REL: TWA 0.2 rug/m3 skin NIOSH IDLH: 10 rng/m3 See: 89245 TLV: (inhalable fraction vapour) 0.1 mg/m3 as (skin); A4 (not classifiable as a human carcinogen); BEI issued; (ACGIH 2008) EU OEL: 0.1 mg/m3; (skin); (EU 2000. ROUTES OF EXPOSURE: The substance can be absorbed into the body by inhalation, through the skin and by ingestion. INHALATION RISK: A harmful contamination of the air will not or will only very slowly be reached on evaporation of this substance at EFFECTS OF SHORT-TERM EXPOSU RE: The substance is irritating to the eyes and the skin . The substance may cause effects on the nervous system resulting in convulsions, reSpiratory failure. Cholinesterase inhibitor. Exposure far above the OEL may result in death. The effects may be delayed. Medical observation is indicated. EFFECTS OF OR REPEATED EXPOSURE: Cholinesterase inhibitor; cumulative effect is possible: see acute hazards/ PHYSICAL PROPERTIES Boiling point at 0.2666 kPa: 136? Relative density (water 1): 1.2 Solubility in water: 110116 Vapour pressure, Pa at 0.0226 Octanol/water partition coefficient as log Pow: 3.99 gov/oiosh/ipcsneng/neng098 5 him] 8/16/2017 u-l" Polk County Puinc Wo Y6318-OI2-I7 CDC SULFOTEP - International Chemical Safety Cards - NIOSH Page 4 of4 The substance is very toxic to aquatic organisms. This - NVI RD ENTAL substance does enter the environment under normal use. Great 4 care, however, should be given to avoid any additional release, DATA . . . e.g. through Inapproprlate dlsposal. Polk County Public Works NOTES Depending on the degree of exposure, periodic medical examination is suggested. Specific treatment is necessary in case of poisoning with this substance; the appropriate means with instructions must be available. Technical grade is a dark?coloured liquid, boiling point at 0.267 kPa. Do NOT take working clothes home. ASP 47, Bay?E393, Bladafurn, Dithion, Dithiotep, Dithiofos are trade names. Card has been partly updated in October 2004 and 2005. See sections Occupational Exposure Limits, EU classi?cation, Emergency Response. Transport Emergency Card: TEC Card has been partially updated in November 2008: see Occupational Exposure Limits, ADDITIONAL INFORMATION I ICSC: 0985 SULFOTEP (C) IPCS, CBC, 1994 Neither NIOSH, the CEC or the IPCS nor any person acting on behalf of NIOSH, the CEC or the IPCS is responsible for the use which might be made of this information. This card contains the collective views of the IPCS Peer Review Committee and may not reflect in all cases all the detailed requirements included in national legislation on the subject. The user should verify compliance of the cards with the relevant legislation in the country of use. The only modi?cations made to produce the US. version is inclusion of the OSHA PELs, NIOSH RELs and NIOSH IDLH values. IMPORTANT LEGAL NOTICE: Page last reviewed: July 22, 2015 Page last updated: July 1, 2014 Content source: National Institute for Occupational Safety and Health 5 .html 8/16/2017 COOKE Garnet DCBS From: Sent: To: Subject: Begin forwarded message: From: Theodore Bunch Jr Subject: Fwd: 2017 Theodore Bunch Jr Wednesday, August 23, 2017 1:08 PM COOKE Garnet DCBS Fwd: 2017?3436 Polk Co -3436 I Polk Co Date: August 22, 2017 at 11:40:14 AM PDT To: Michael Odenthal Begin forwarded message: From: FELDON Leah Subject: RE: 2017-3436 I Polk Co Date: August 17, 2017 at 4:1 6:27 PM PDT polk Ounr . Y6.) [510129; :Ublic ?/0st To: Geoff 'Alexis Taylor' Bruce HANSON Don Leah' 'Linda Hayes Gormsn' 'Theodore Bunch Jr' HANSON Lisa Cc: MASTROS David Kimberlee' Thanks, Geoff. Adding Lisa Hans, Leah K. Feldon Deputy Director on, ODA. Oregon Department of Environmental Quality Executive Assistant: Stacey O?Neil 0 'neilstacengdegista tear. us From: BROWN Geoff Sent: Thursday, August 17, 2017 2:28 PM To: 'Alexis Taylor'; Bruce HANSON Don; BROWN Geoff; Leah'; 'Linda Hayes Gormsn'; 'Theodore Bunch Jr' Cc: MASTROS David; Geoff?; Kimberlee'; Nancy?; BUNCH Theodore ?Whitaker, Todd' Subject: RE: 2017-3436/ Polk Co Polk County Public Works Y6318?012-l7 Yesterday our contractor scraped the surface soils that were affected by this pesticide release, which secured the site so people can't casually come into contact with the pesticides, however additional work needs to be done to secure the site for the long term. The affected area is immediateiy from a road crossing culvert. The release was initially discovered when maintenance workers began g?et-rodding the culvert to clean it out. When they started up the jet rod, pesticide dust/powder emerged from the end of the culvert. So in addition to the contamination we cleaned up from the ditch line soil, there is also likely pesticide inside the culvert. In order to make sure that we don't have a problem when it rains and the roadside ditch starts flowing, we need to clean out the culvert. So contractor NRC wiil be cleaning out the culvert next week by jetrodding it and recovering the jet rod residue/liquids. After the cuivert is cleaned out, they will sample soil and upstream of the culvert to make sure the cleanup was complete. Please let me know if you have any questions. Geoff Brown State On?Scene Coordinator Oregon DEQ 541-686-7819 ?gwwn .s. ?Mania-m From: BROWN Geoff Sent: Wednesday, August 16, 2017 4:31 PM To: Linda Hayes Gormsn; GILLES Bruce FELDON Leah; Theodore Bunch Jr; Alexis Taylor; HANSON Don Cc: BUNCH Theodore Geoff'; Kimberlee'; SAWKA Nancy; MAST ROS David Subject: RE: 2017-3436/ Polk Co Our contractor, NRC, responded and assessed the scene eariier today. Based on their reported observations, the spill/dump area was pretty small. They cleaned up the spilled material and surrounding soil, bagged it up and transported it back to their facility for characterization and disposal. We will be conferring internally tomorrow about the need for any additional work or sampling. Geoff Brown State On-Scene Coordinator Oregon DEQ 541-686?7819 From: GILLES Bruce A Sent: Wednesday, August 16, 2017 4:24 PM To: 'Lisa Hanson'; Linda Hayes Gormsn Cc: GILLES Bruce FELDON Leah; Theodore Bunch Jr; Alexis Taylor; HANSON Don; BROWN Geoff Subject: RE: OERS 2017-2436 Polk Co. Lisa, DEQ dispatched our contractor to clean up the spill this morning. Geoff Brown from our Eugene office has been in contact with the contractor and will send a follow up to this email with status of our response work. Thanks Bruce Bruce Gil/es, Manager Department of Environmental Quality P015 County Public Works Cleanup and Emergency Response Program Y6J [8-012-l7 C)perations Division, lwleadquarters 700 NE Multnomah Street, Suite 600 (gt Portland, OR 9 2324100 Phone: {503) 2296391 Cell: (9 7.1) 24652300 From: Lisa Hanson Sent: Wednesday, August 16, 2017 4:08 PM To: Linda Hayes Gormsn Cc: GILLES Bruce A FELDON Leah Theodore Bunch Jr Alexis Taylor Subject: Re: OERS 2017-2436 Polk Co. Thank you for the information. Please let us know what we can do to stay coordinated. On Aug 16, 2017, at 4:02 PM, Linda wrote: DEQ dispatched NRC this morning to clean up the pesticide spill. Bruce will check on status and get back to us. From: HAYES-GORMAN Linda Sent: Wednesday, August 16, 2017 3:56 PM To: 'Lisa Hanson' Linda Hayes Gormsn FELDON Leah Subject: RE: OERS 2017?2436 Polk Co. Thanks for sharing. ljust spoke with Keith Andersen (WR admin) he is tracking down his cleanup lead Don Hanson to see what he knows. 1) is the area cordoned off so it is safe, 2) has there been any cleanup/is it planned, and 3) we need a shared agency understanding of what happened and what will happen. I will try our HQ folks again whose names I saw on the email exchange. From: Lisa Hanson Sent: Wednesday, August 16, 2017 3:46 PM To: Linda Hayes Gormsn FELDON Leah Subject: Fwd: OERS 2017?2436 Polk Co. ?rst one Begin forwarded message: Polk County Public Works From: Dale Mitchell Subject: Fwd: OERS 2017-2436 Polk C0. Date: August 15,2017 at 4:58:07 PM PDT T0: Theodore Bunch Jr Cc: Lisa Hanson Lauren Henderson , Brian Ted, You may have already received this ORES report. Pesticides Program, Mike and I are receiving call about how to coordinate. Kimberly Van Patton from DEQ also contacted me. OROSHA has referred to PARC. A PARC coordination call need to be scheduled First thing in morning. Incident occurred August 7, 2017, and just reported to ORES. With three individuals already affected a HasMat team may be needed to evaluate site. ODA staff are not trained on Spill response cleanup. If we need to discuss tonight let me know. Dale M. Begin forwarded message: From: ?Staff, Oers" Subject: FW: OERS 2017-2436 Polk C0. Date: August 15,2017 at 4:37:00 PM PDT To: MITCHELL Dale From: Staff, Oers Sent: Tuesday, August 15, 2017 4:03 PM To: OHD DUTY Of?cer Subject: OERS 2017-2436 Polk Co. Polk Co. PW reported the discovery ofa pesticide Spill on 08/07/17. Tracie Long Duty Officer Oregon Of?ce of Emergency Management Email: Phone: (503) 378?6377 Polk County Public Works ?313-01247 This e?mail may contain information that is privileged, con?dential, or otherwise exempt from disclosure under applicable law. If you are not the addressee or it appears from the context or otherwise that you have received this e-mail in error, please advise me immediately by reply e?mail, keep the contents con?dential, and immediately delete the message and any attachments from your system. Lisa Hanson hanson@oda.state.or.us Lisa Hanson Ihanson@oda.state.or.us Polk County Public Works COOKE Garnet DCBS Y6318-012-17 From: Theodore Bunch Jr Sent: Wednesday, August 23, 2017 1:31 PM To: COOKE Garnet DCBS Subject: Fwd: 2017-3436/ Polk Co Attachments: Incident Order 17-06 Begin forwarded message: FrOm: VAN-PATTEN Kimberlee Subject: RE: 2017?3436 Polk Co Date: August 16,2017 at 3:57:40 PM PDT To: SAWKA Nancy Cc: BUNCH Theodore Geoff Dave Mastros sent NRC Environmental Services out to cleanup the spill today. I don?t know anything more than that. Geoff Brown said he was going to touch base with NRCES earliertoday. He might have more information. No need to log in complaints as it was handled in spiils. Kimberlee ?9..th ?mrrwemn . ?.1me Wm? ?a . .. ., WW may mm. ambusmut ?many-mm? From: SAWKA Nancy Sent: Wednesday, August 16, 2017 3:24 PM To: VAN-PATTEN Kimberlee Subject: FW: 2017-3436/ Polk Co 'Hi Kimberlee ?Ted Bunch forwarded this to me and was asking if DEQ was going to respond. Should i be logging this as a complaint or will OERs be responding and then contacting Spills? Not sure of the process for this one especially since it?s a pesticide. Thanks Nancy From: Theodore Bunch Jr Sent: Wednesday, August 16, 2017 3:05 PM To: SAWKA Nancy Subject: Fwd: 2017-3436 Polk Co Begin forwarded message: From: Kimberlee Subject: FW: 2017-3436 Polk Co Date: August 15,2017 at 4:28:21 PM PDT To: BUNCH Theodore Polk County Public Works - - 18- 3- I got an ?undeliverable? on my first attempt. E9 3 01 ?7 From: Kimberlee Sent: Tuesday, August 15, 2017 4:20 PM To: BUNCH Theodore Cc: MASTROS David Subject: FW: 2017?3436 Polk Co Thanks for your assistance. Please let us know how we can help. Kimberlee Van Patten Duty Officer Emergency Response Program Oregon Dept. of Environmental Quality 503-229-5256 office 971?563?8034 cell 700 NE Multnomah St., Suite #1400 Portland, OR 97232 From: STAFF Oers Sent: Tuesday, August 15, 2017 4:02 PM To: DREHER DAVID Folsom, Jamaal; Giffin, Sandy; GRIFFIN Dennis HUBBELL Raymond Kuenzi, Chris; martenson, eric; Ron Modjeski Szumski, Mike Subject: 2017?3436 Polk C0 Polk Co. PW reported the discovery of a pesticide spill on 08/07/17. Keelyn Fawcett CJIS Specialist Information Technology Oregon State Police Email: Helpdesk.LEDS@state.or.us Phone: (503) 378-5565 To provide premier public safety services. This e-mail may contain iuli?irmation ihai. is privileged. con?dential. or olhcm?ise exempt from disclosure umlcr applicable law ?you are not llie addressee or it appears lrom llie context or Otherwise that you have received this e-niail in error. please. advise me immediately reply e-mail, keep lhe. conic-ms confidential. aml immediately (lelele the message anrl any allarl'rnimils lrom your system. COOKE Garnet DCBS From: Theodore Bunch Jr Sent: Wednesday, August 23, 2017 1:42 PM County PUbiiC Works To: COOKE Garnet DCBS ?Jig-013'? ,y Subject: Fwd: oeasrr 2017?3436/ Polk Co Begin forwarded message: From: BROWN Geoff Subject: RE: 2017-3436 1 Polk Co Date: August 17, 2017 at 2:28:14 PM PDT To: 'Alexis Taylor' Bruce HANSON Don BROWN Geoff Leah' 'Linda Hayes Gormsn' 'Theodore Bunch Jr' Cc: MASTROS David Geoff' Kimberlee' Nancy' BUNCH Theodore ?Whitaker, Todd'? Yesterday our contractor scraped the surface soils that were affected by this pesticide release, which secured the site so people can't casually come into contact with the pesticides, however addit?onal work needs to be done to secure the site for the long term. The affected area is immediately from a road crossing culvert. The release was initially discovered when maintenance workers began jet-rodding the culvert to clean it out. When they started up the jet rod, pesticide dust/powder emerged from the end of the culvert. So in addition to the contamination we cleaned up from the ditch- line soil, there is also likely pesticide inside the cuivert. In order to make sure that we don?t have a problem when it rains and the roadside ditch starts flowing, we need to clean but the culvert. So contractor NRC will be cleaning out the culvert next week by jetrodding it and recovering the iet rod residue/liquids. After the culvert is cleaned out, they will sample soil and upstream ofthe culvert to make sure the cleanup was complete. Please iet me know if you have any questions. Geoff Brown State On?Scene Coordinator Oregon DEQ 541?686-7819 a. b. a? mew? mam," 1..- m: Ti ,i From: BROWN Geoff Sent: Wednesday, August 16, 2017 4:31 PM To: Linda Hayes Gormsn; GILLES Bruce FELDON Leah; Theodore Bunch Jr; Alexis Taylor; HANSON Don 1 Cc: BUNCH Theodore Geoff"; Kimberlee?; SAWKA Nancvr MASTROS David - . Polk Count bli .. #217-4 YUCOFS Subject RE OERS 0 3 36/ P0 Co ?$801247 Our contractor, NRC, responded and assessed the scene earlier today. Based on their reported observations, the Gib spill/dump area was pretty small. They cleaned up the spilled material and surrounding soil, bagged it up and transported it back to their facility for characterization and disposal. We will be conferring internally tomorrow about the need for any additional work or sampling. Geoff Brown State Orr?Scene Coordinator Oregon DEQ 541-686?7819 From: GILLES Bruce A Sent: Wednesday, August 16, 2017 4:24 PM To: 'Lisa Hanson?; Linda Hayes Gormsn Cc: GILLES Bruce FELDON Leah; Theodore Bunch Jr; Alexis Taylor; HANSON Don; BROWN Geoff Subject: RE: OERS 2017?2436 Polk Co. Lisa, DEQ dispatched our contractor to clean up the spill this morning. Geoff Brown from our Eugene office has been in contact with the contractor and will send a follow up to this email with status ofour response work. Thanks Bruce Bruce Gil/es, Manager Department of Environmental Quality Cleanup and Emergency Response Program Operations Division, lvleadquarters 700 NE Multnomah Street, Saite 600 Portland, OR 97232-4100 Phone: {503) 229?6391 (9 71) 246?2300 From: Lisa Hanson Sent: Wednesday, August 16, 2017 4:08 PM To: Linda Hayes Gormsn Cc: GILLES Bruce A FELDON Leah Theodore Bunch Jr Alexis Taylor Subject: Re: OERS 2017-2436 Polk Co. Thank you for the information. Please let us know what we can do to stay coordinated. On Aug 16, 2017, at 4:02 PM, Linda wrote: DEQ dispatched NRC this morning to clean up the pesticide spill. Bruce will check on status and get back to us. From: HAYES-GORMAN Linda Polk County public Works Sent: Wednesday, August 16, 2017 3:56 PM Y6313'012?i7 To: 'Lisa Hanson? Linda Hayes Gormsn FELDON Leah 5 Subject: RE: OERS 2017-2436 Polk C0. Thanks for sharing. just spoke with Keith Andersen (WR admin) he is tracking down his cleanup lead Don Hanson to see what he knows. l) is the area cordoned off so it is safe, 2) has there been any cleanup/is it planned, and 3) we need a shared agency understanding of what happened and what will happen. I wiil try our HQ folks again whose names I saw on the email exchange. From: Lisa Hanson Sent: Wednesday, August 16, 2017 3:46 PM To: Linda Hayes Gormsn FELDON Leah Subject: Fwd: OERS 2017-2436 Polk Co. first one Begin forwarded message: From: Dale Mitchell Subject: Fwd: OERS 2017?2436 Polk Co. Date: August 15, 2017 at 4:58:07 PM PDT To: Theodore Bunch Jr Cc: Lisa Hanson Lauren Henderson Brian Ted, You may have already received this ORES report. Pesticides Program, Mike and are receiving call about how to coordinate. Kimberly Van Patton from DEQ also contacted me. OROSHA has referred to PARC. A PARC coordination call need to be scheduled First thing in morning. Incident occurred August 7, 2017, and just reported to ORES. With three individuals already affected a HasMat team may be needed to evaluate site. ODA staff are not trained on Spill response cleanup. If we need to discuss tonight let me know. Dale M. Begin forwarded message: From: ?Staff, Oers" Subject: FW: OERS 2017-2436 Polk Co. Date: August 15, 2017 at 4:37:00 PM PDT To: MITCHELL Dale Polk County Public Works vans-01247 From: Staff, Oers Sent: Tuesday, August 15, 2017 4:03 PM To: OHD DUTY Of?cer Subject: OERS 2017?2436 Polk Co. Polk Co. PW reported the discovery ofa pesticide spill on 08/07/17. Tracie Long Duty Of?cer Oregon Of?ce of Emergency Management Email: Phone: (503)378-6377 This e-mail may contain information that is privileged, con?dential, or otherwise exempt from disclosure under applicable law. If you are not the addressee or it appears from the context or otherwise that you have received this e-mail in error, please advise me immediately by reply e-mail, keep the contents con?dential, and immediately delete the message and any attachments from your system. Lisa Hanson lhanson@oda.state.or.us Lisa Hanson lhanson@oda.state.or.us iglleoumy PUblic Works COOKE Garnet DCBS 8'012-17 From: BROWN Geoff Sent: Wednesday, September 06, 2017 3:17 PM To: COOKE Garnet DCBS Subject: RE: ll7041?--epartial draft report??A7H0678 Attachments: 117041 Samplejpg Yes. The green sample was sent to another lab. I don?t have results for it yet. I?m also not sure if DEQ is going to conduct more work or not, I may have NRC do some shovel work over the top of the culvert and beneath the culvert where the muddy area is and sample the water. W, .. 2w, wows, -. emu.? ms gunman-u. m, .. . mum-n u'ciwmeuw AMA New. n? From: COOKE Garnet DCBS Sent: Wednesday, September 06, 2017 3:12 PM To: BROWN Geoff Subject: RE: draft report?-A7H0678 Hi Geoff, - Thanks. Do you know which sample was taken where? Were these taken after the jet rodding? And if so, was the water collected sampled? Also, the green stuff sample went to another lab, right? Thanks for you:r help on this! Garnet From: BROWN Geoff Sent: Wednesday, September 06, 2017 2:38 PM To: COOKE Garnet DCBS Subject: FW: draft report--A7H0678 Good timing. ljust received the results from NRC. The results are orders of magnitude lower than the initial samples, with one of three samples containing chlorpyrifos at 101 ppm, somewhat above risk based screening level for residential receptors (which is 63 ppm), which is based on a 30?year residential exposure. lt is also above the leaching to protect groundwater screening level, which would apply if the release was very close to a residential drinking water well. From: Geigle, Roman [mailtozRGeiqle@nrcc.com] Sent: Wednesday, September 06, 2017 11:56 AM To: DEQ Geoff Brown (qeoff.brown@state.or.us) Subject: FW: 117041-?--partial draft report--A7H0678 Photos to follow Roman Geigle Portland Emergency Response Manager NRC rgeigle@nrcc.com From: Darrell Auvil Sent: Wednesday, September 6, 2017 10:51 AM To: Geigle, Roman Cc: Darwin Thomas Subject: 117041--?-partial draft report?-A7H0678 Hi Roman, see attached, updated report, with organophosphorus pesticides (OPPs). sample 551 on page 7. 8151 herbicide data is still pending. Regards, Darrell Auv?l Project Manager O: 503.718.2323 M: 503.459.6522 Hours of Operation: 7:30am 6:30pmM?F Saturday 9am?i\toon only. We Welcome Your Feedback Help us improve'vom' experience by raking our short. survey. Apex Client Survey Polk County Public Works Y6318-012-l7 Note Chlorpyrifos data on Apex Laboratories, LLC - 12232 SW Garden Place - Tigard, Oregon COOKE Garnet DCBS Polk County Public Works Y63l8-Ol2-l7 From: . BROWN Geoff Sent: Wednesday, September 06,2017 2:38 PM To: COOKE Garnet DCBS Subject: FW: 117041-vaartial draft report?-A7H0678 Attachments: A7HO678 partial DRAFT O9 06 17 Good timing. ijust received the results from NRC. The results are orders of magnitude lower than the initial samples, with one of three samples containing Chlorpyrifos at 101 ppm, somewhat above risk based screening level for residential receptors (which is 63 ppm), which is based on a 30-year residential exposure. It is also above the leaching to protect groundwater screening level, which would apply if the release was very close to a residential drinking water well. .. -.- - . is ?we ?and?. . 54 is. my?. A From: Geigle, Roman [mailtozRGeiqle@nrcc.com] Sent: Wednesday, September 06, 2017 11:56 AM To: DEQ Geoff Brown (Geoff.brown?state.or.us) Subject: FW: draft report?~A7H0678 Photos to follow Roman Geigle Portland Emergency Response Manager NRC rgeigle@nrcc.com From: Darrell Auvil Sent: Wednesday, September 6,2017 10:51 AM To: Geigle, Roman Cc: Darwin Thomas Subject: 117041-mpartial draft report--A7H0678 Hi Roman, see attached, updated report, with organophosphorus pesticides (OPPs). sample 551 on page 7. 8151 herbicide data is still pending. Regards, Darrell Advil Project Manager O: 503.718.2323 M: 503.459.6522 Hours of Operation: 7:30am -- 6r30pm Saturday 9am-Noon only. Note Chlorpyrifos data on Apex Laboratories, LLC - 12232 SW Garden Place - Tigard, Oregon Works lC .4 Y6318-Ol2-Polk County Public Works COOKE Garnet DCBS - Y6318?01_2jl7 From: BROWN Geoff Sent: Wednesday, September 20, 2017 9:12 AM To: COOKE Garnet DCBS Subject: FW: w/ herbicides?"A7HO678 Attachments: A7H0678 DRAFT O9 O6 17 Here is what we have for that sample. have asked NRC to look into why they only ran herbicides and if it's too late to get a more complete data set. . .. From: Geigle, Roman Sent: Tuesday, September 12, 2017 4:53 PM To: DEQ Geoff Brown (qeoff.brown@state.or.us) Subject: FW: w/ This just in sample results for 55?4 green substance Page 23 Roman Geigle Portland Emergency Response Manager NRC From: Darrell Auvil Sent: Tuesday, September 12, 2017 12:13 PM To: Geigle, Roman Cc: Darwin Thomas Subject: 117041-?-?draft w/ Hello, herbicide data is now included. Regards, Darrell Auvll Project Manager O: 503.718.2323 M: 503.459.6522 Hours of Operation: 7:303m 6:30pm Saturday SammNoon only. Apex Laboratories, LLC - 12232 SW Garden Place - Tigard, Oregon We Welcome Your Feedback Help us improve your experience by Fairing ourshortsurvey. Apex Client Survey COOKE Garnet DCBS From: BROWN Geoff Sent: Tuesday, October 24, 2017 2:26 PM Works To: COOKE Garnet DCBS Polk County Pubf1C Subject: RE: ll704l?--?partia draft report-?A7HO678 lS? 011? ?7 No. That was it. From: COOKE Garnet DCBS Sent: Tuesday, October 24, 2017 2:18 PM To: BROWN Geoff Subject: RE: draft report-?A7H0678 Hi Geoff, Was any more work or sampling done on this case? Thanks Garnet kw .M -- w? mm Wmmu-w?. -.- um.? a? vw1~uwm~r w?w? mm ?a Wm" From: BROWN Geoff [mailtoz qeoff. brown@state. or. us] Sent: Wednesday, September 06,2017 3:17 PM To: COOKE Garnet DCBS Subject: RE: draft report--A7H0678 Yes. The green sample was sent to another lab. I don?t have results for it yet. I?m also not sure if DEQ is going to conduct more work or not, I may have NRC do some shovel work overthe top ofthe culvert and beneath the culvert where the muddy area is and sample the water. From: COOKE Garnet DCBS [marlto Garnet Cooke@oreqon qovl Sent: Wednesday, September 06, 2017 3:12 PM To: BROWN Geoff Subject: RE: 117041??--partial draft report??A7HO678 Hi Geoff, Thanks. Do you know which sample was taken where? Were these taken after the jet rodding? And if so, was the water collected sampled? Also, the green stuff sample went to another lab, right? Thanks for your help on this! Garnet From: BROWN Geoff Sent: Wednesday, September 06, 2017 2:38 PM To: COOKE Garnet DCBS Subject: FW: 117041-??-partial draft report?-A7HO678 Good timing. just received the results from NRC. The results are orders of magnitude lower than the initial sa with one of three samples containing chlorpyrifos at 101 ppm, somewhat above risk based screening level for residential receptors (which is 63 ppm), which is based on a 30?year residential exposure. It is also above the leaching to protect groundwater screening level, which wouid apply if the reiease was very close to a residential drinking water well. From: Geigle, Roman Polk County Public Works Sent: Wednesday, September 06, 2017 11:56 AM To: DEQ Geoff Brown (qeoff.brown@state.or.us) Subject: FW: draft report??A7HO678 Photos to follow Roman Geigle Portland Emergency Response Manager NRC rgeigle@nrcc.com From: Darrell Auvil Sent: Wednesday, September 6,2017 10:51 AM To: Geigle, Roman Cc: Darwin Thomas Subject: 117041-?--partial draft report--A7H0678 Hi Roman, see attached, updated report, with organophosphorus pesticides (OPPs). Note Chlorpyrifos data on sample 551 on page 7. 8151 herbicide data is still pending. Regards, Darrell Auvil Project Manager O: 503.718.2323 Hours of Operation: 7:30am 6:30pm Saturday 9am?Noon only. Apex Laboratories, LLC - 12232 SW Garden Place - Tigarcl, Oregon We Welcome Your Feedback Help us improveyour experience by taking our short Survey. Apex Client Survey 12232 S.W. Garden Place Apex Labs Wire]; 97223 503-7l8-2323 Phone 503-718-0333 Fax Polk County Public Works was-01247 Wednesday, September 6, 2017 Roman Geigle NRC 6211 Ensign St Portland. OR 97217 RE: 117041 [117041 Enclosed are the results of analyses for work order A7H0678, which was received by the laboratory on 8/24/2017 at Thank you for using Apex Labs. We appreciate your business and strive to provide the highest quality services to the environmental industry. If you have any questions concerning this report or the services we offer, please feel free to contact me by email at: or by phone at 503?718?2323. DRAFT REPORT The provided in link report are and are .riibjucl tr) change based rm (rimb?m. (II/?rm! dam review. Harare me thew rm?u/rx with 1116? H?mr they may have no! bear/?nalized by the labnmm?i? Page I of2l DRAFT REPORT, DATA SUBJECT TO CHANGE Report is complete only if it includes Calscience Euro?ns 8151 Data. Page 1 of 33 09/12/2017 Apex Labs 1 12232 SW. Garden Plac Tigard, OR 97223 503-718-2323 Phone 5111-71 2-11313 Fax- NRC 6211 Ensign St Portland, OR 97217 Project 117041 Project Number: 1 17041 Project Manager: Roman Polk County Public Works Y6318~012-l7 Reported: 09/06/17 10:45 ANALYTICAL REPORT FOR SAMPLES 1f SAMPLE INFORMATION Sample 11) Laboratory ID Matrix Date Sampled Date Received 58-] A7110678-01 Soil 08/23/17 10:05 08/24/17 14:12 SS-2 A71-10678-02 Soil 08/23/17 10:11 08/24/17 14:12 88-39 A7HO678-03 Soil 08/23/17 10:16 08/24/17 14:12 RA FT REPORT 7716 {Ii/x rc/mrl arc RV and are .s?ubjeci In change lit/Md (m mm/yx/x, QC unlit/(Ilium Ur?na/ dam review. News Inc More raw/Ix u?r'ih (/10 [but they may have no! heel/?nalized by the laboratory DRAFT REPORT, DATA SUBJECT TO CHANGE Report is complete only if it includes Calsclence Euro?ns 8151 Data. Page 2 of 33 Page 2 0121 09/12/2017 Polk County Public Works Y6318-012-17 12232 SW. Garden Place Apex Lab Tigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax NRC Project. 117041 6211 Ensign St Project Number: 117041 Reported: Portland. OR 97217 Project Manager: Roman Geiglc 09/06/17 10:45 ANALYTICAL SAMPLE RESULTS ll Organochlorine Pesticides by EPA 80818 Reporting Analytc MDL Limit Units Dilution Date Analyzed Method Notes SS-1 (A7H0678-01RE1) Matrix: Soil Batch: 7081054 0'05 Aldrin ND 6.06 Lug/kg dry 1 08/30/17 12:57 EPA 80818 R-02 alpha-1311C ND 4? 18 R-OZ bela~BHC ND 10.5 R-02 delta-BHC ND 4,95 R-02 gamma-1311C (Lindane) ND 7.38 R-02 cis-Chlordanc ND 4.73 R-O2 trans-Chlordane ND 6.94 R-02 ND 8.70 R-02 ?1 - 28.9 - 2.20 Q-42 ND 14.2 Dieldrin ND 3.74 R-02 Endosulfanl ND . 4.18 R-OZ Endosulfan 11 ND 5.17 R-02 Endosulfan sulfate ND 2.20 Eodrin ND 8.37 R-oz Endrin Aldehyde ND 7.82 R-02 Endi'in ketone ND 2.20 Hoptachlor ND 10.3 R-OZ l-lcptachlor cpoxldc ND 10.2 R-02 ND 100 R-02 Chlordane (Technical) ND 66.1 Toxaphcne (Total) ND 66.1 Sit/Toggle: (Si/riff Recovery: 57 Uni/M: 42-129 (Sun) 76 Lint/M; 65-l5/ DRAFT REPORT T/ic ram/m prov/clad in mm are PRELIMINARY and are ,i'ii/ijuci in change Imed (m .i'u/Mcqim? amt/1111.1. QC validation ur?rml dam rev/cw. I?lcm'e we {have rmn/M u'H/i {he r/m! I/icy may have no! hem/?nalized by 1/10 DRAFT REPORT, DATA SUBJECT TO CHANGE Page 3 012? Report is complete only if it includes Calscience I Euro?ns 8151 Data. Page 3 of 33 09/12/2017 Apex Labs I2232 S.W. Garden Place 'I?igard, 503-718-2323 Phone OR 97223 503-7] Polk County Public Works NRC Project: 1I7041 8'012'17 621l Ensign St Project Number: ll704l Reported: Portland. OR 97217 Project Manager: Roman Geigle 09/06/17 l0r45 ANALYTICAL SAMPLE RESULTS ll: Organochlorine Pesticides by EPA 8081B ll Reporting Analyte RPSUH MDL Limit Units Dilulion Date Analyzed Method Notes SS-2 (A7H0678-02RE1) Matrix: Soil Batch: 7081054 0-05 Aldrin ND 2.47 ug/kg dry 1 08/30?? l3:32 EPA 808113 alpha-BHC ND 2.47 bela-BHC ND 2'47 .. .. delta~BHC ND 2.47 -- .. .. gamma-BHC (Lindane) ND 2.47 .. .. (sis-Chlordane ND 2.47 .. .. trans-Chlordane 2.47 ND 2.47 .. LUV-DDT ND 247 .. .. .. Dieldrin ND 2.47 .. .. Endosult'Endosult?an ll ND 247 .. Endosull?an sulfate ND 2.47 .. .. Endrin ND 2.47 Endrin Aldehyde ND 247 v' .. .. .. Endrin kctone ND 247 .. .. .. Heptaehlor ND 247 .. .. .. Hcptachlor epoxidc ND 2_47 .. .. ND 740 .. .. Chlordane (Technical) ND 740 .. .. Toxaphene (Total) ND 740 .. .. Sm?mgufc: 2, 5 . 6? (Surr) [.r?nmx: 42?]29 "u LimitsDRAFT REPORT The rum/Is provided in Ihir report are Rl' and are .s'nhjecl In Change 15(1er rm (?railway QC validation nr?nal data review. Name me {have rem/M with {he {/1er ?my may have HUI by the laboratory DRAFT REPORT, DATA SUBJECT TO CHANGE Repon is complete only if it includes Calseienee Euro?ns 8151 Data. Page 4 of 33 Page 4 ol?2] 09/12/2017 Apex Labs NRC 6211 Ensign Sl Portland,OR 97217 Project: 11704] Project Number: 117041 Project Manager: Roman Goiglo 12232 S.W. Garden Place Tigurd,0R 97223 503-718-2323 Phone 503319-411? [Luv \0?1 Polk County Public Works Y6318?012-l7 Reported: 09/06/17 10:45 I ANALYTICAL SAMPLE RESULTS Organochlorine Pesticides by EPA 8081B Reporting Analyte Result MDL Limit Units Dilution Date Analyzed Method Notes 58-3 (A7H0678-03RE1) Matrix: Soil Batch: 7081054 0-05 Aldrin ND 2.17 ug/kg dry 1 08/30/17 13:49 EPA 8081B alpha-BBC ND 217 .. .. beta?BHC ND 2.17 .. delta-BHC ND 2.17 .. .. gamma-BHC (Lindanetrans-Chlordane ND 2,17 1. .. .. .. ND 2.39 .1 R412 - 4,4201?: 9.19 2.17 1. .. -- ND 4.89 R-02 Dicldrin ND 2.17 Endosulfan 1 ND 2,17 .. Endosull'zm 11 ND 2.17 .. .. EndosuH?an sulfate ND 2.17 .. Endrin ND 2? 17 r. .. Endrin Aldehyde ND 2.17 .. .. .. Endrin ketone Heptaehlor ND 217 .. .. .1 Heptachlor epoxide ND 217 .. .. ND 32.6 .1 R-02 Chlordane (Technical) ND 65.2 .1 Toxaphene (Total) ND 65.2 .. Sm?mgmu: (SHIT) (Sun) Recovery: 44 Lint/Ix: 4.7429 73 Urn/Ix: 6545] ?a DRAFT REPORT The rem/M provided in [hit report are 1' am! We In change boxed on (mu/mix. QC minimum m1 ?nal dam review. Hem-e me there ram/1.1 wit/1 1/10 lmderytundmg rlmi may have rm! brim/finalized by {he laboratory DRAFT REPORT, DATA SUBJECT TO CHANGE Report is complete only if it includes Calscience Eurofins 8151 Data. Page 5 of 33 Page 5 01'21 09/12/2017 Polk County Public Works Y6318-012-"l7 12232 S.W. Garden Place Ap 6X Labs Tigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax NRC 7 Project: 117041 6211 Ensign St Project Number: 117041 Reported: Portland, OR 97217 Project Manager: Roman Gciglc 09/06/[7 10:45 ANALYTICAL SAMPLE RESULTS ll: Organophosphorous Pesticides (OPPs) by EPA 82700 (GCIMS) Reporting Analyte Result MDL Limit Unlts Dilution Date Analyzed Method Notes 58-1 (A7H0678-01) Matrix: Soil Batch: 7090311 Azinphos methyl tGurhion) ND 475 ug/kg dry 10 09/05/17 17:24 82701) OPP Coumaphos ND 475 7. .7 77 Demeton Demeton ND 475 .7 .7 .7 7. Diazinon ND 475 77 .7 7. 7. Dichlorvos ND 475 7. Dimcthoate ND 475 77 .7 7. 7. Disulfoton Ethopmphos (ProphnsFenthion ND 475 77 7. 7. .7 Malalhion Methyl parathion ND 475 77 77 .7 77 (PhosdrinMonocrotophos ND 475 77 7. 7. .7 Naled (DibromParathlon, ethyl ND 475 .7 Phorate ND 475 Ronnei (Fenchlorphos) ND 47S .7 Sull?otcp ND 475 't Sulprofos (BolstarTEPP ND 1900 77 .7 77 7. Tctrachlorvinpl?los (RabonTokuthion (Prothiol?osanrngulc: (Sun) Rrrun'va.? 123 Limflx.? 50?]4! 12/ 7.7777777,- 6(1-130/ 7. DRAFT REPORT 7777' 7mm- provided in thix report arc and are 777/7747 Change 77mm on (mub'xis. QC validation nr?rml dam review. l?lc?aw me lime ram/Ix with {he mu/emundmg that Ilrey may have mu bcm?nahzcd by the lahm?mmjv DRAFT REPORT, DATA SUBJECT TO CHANGE Page 6 of21 Report is complete?only if it includes Calscience I Euro?ns 8151 Data. Page 6 of 33 09/12/2017 Polk County Public Works Y63 18-012-17 12232 S.W. Garden Place Apex Labs Tigard,OR 97223 503-718-2323 Phone 503-718-0333 Fax NRC Projccl: 117041 62 Ensign SI Project Number: 117041 Reported: Portland, OR 972]? Project Manager: Roman Geigle 09/06/07 10:45 ANALYTICAL SAMPLE RESULTS Organophosphorous Pesticides (OPPs) by EPA 82700 II Reporting Analylc RCSUH MDL Limit Units Dilution Date Analyzed Method Notes SS-1 (A7H0678-01RE1) Matrix: Soil Batch: 7090311 101000 4750 ug/kg dry l00 09/05/17 18:00 8270D OPP SS-Z (A7H0678-02RE1) . Matrix: Soil Batch: 7090311 Azinphos methyl (Guthion) ND 54.9 ug/kg clr}l 09/05/17 l9:49 8270D OPP 1 Chlorpyrifos 370 7 549 .. .. .. Coumaphos ND 549 .. .. .. Demcton 54.9 .. .. .. Dlazinon ND 54.9 .. l. Dichlorvos ND 54.9 .. Dimcthoale ND 54.9 .. .. .. Disull?oton ND (559 .. EPN ND 54.9 Ethoprophos (Prophos) ND 549 .. Fensult'olhion ND 549 .. .. .. Fenlluon ND ..- 5479 .. .. Malathion ND 54.9 .. Merphos ND 5419 .. ., Methyl parathion ND 54.9 Mevinphos (Phosdrin) ND 54.9 .. .. Monocrotophos ND 549 .. .. Naled (Dibrom) ND 549 .. .. .. Paralhlon. ND 54.9 .. l?horale ND 54.9 Ronnel ND 5459 .. .. Sulfotep ND 549 .. .. .. Sulprofos (Bolstar) I ND .L- 54.9 .. .. TEPP ND 220 .. (Rabon) ND 54.9 .. 'l'okuthion (Prolhiof?osSurrogate: l?l'ihmyl pinup/mic Rocrn?c?l?; 93 "n Umim.? 50-14] Yl?lp/wml/ plmJ?p/rulc (Surf) 86 Limil?x: 60-130 DRAFT REPORT The ram/Ix provided in [My rcpm"! um Ill? and mu to change bmed (m .vuhxcquenl cmab'.x't'.xg QC (Hf/inn] dam review. l?l?cm?c we threw raw/r." u'ilh rhc? r/mr Ilia)! may have not been?naliwd by the [aha/711mg: DRAFT REPORT, DATA SUBJECT TO CHANGE Page 7 of'2l Report is complete only if it includes Calscience Euro?ns 8151 Data. Page 7 of 33 09/12/2017 12232 S.W. Garden Place \lk Apex Labs Tigard,OR 97223 1 503-718?2323 Phone nana Polk County Public Works NRC . Project: 1171141 Y6318-01247 6211 Ensign St Project Number: 1 17041 Reported: Portland, OR 97217 Project Manager: Roman Gciglc 09/06/17 10:45 ANALYTICAL SAMPLE RESULTS Organophosphorous Pesticides (OPPs) by EPA 82700 (GCIMS) Reporting Analyte MDL Limit (711115 Dilution Date Analyzed Method Notes SS-3 (A7H0678-03) Matrix: 8011 Batch: 7090311 methyl (GuthionL ND 1870 ug/kg dry 40 09/05/17 16: 10 8270B OPP Chlorpyrifos . . . 17600 1870 .. .. .. Coumaphos ND 1870 .. .. 0 ND 1870 3 ND 1870 .. .. .. Diazinon ND 1370 .. .. .. .. Dichlorvos ND 1370 .. .. .. Dimcthoatc ND 1370 .. .. .. .. Disnltoton ND 2240 .. .. .. .. EPN ND 1870 .. -- .. Ethoprophos (Prophos) ND 1370 .. .. .. .. ND 1370 .. .. .. .. ND 1370 .. -- .. .. Malathion ND 1370 .. .. .. 1370 .. .. .. .. Methyl parathion ND 1370 .. .. .. .. Mcvinphos (Phosdrin) ND 1370 .. .. .. .. Monocrotophos ND 1370 11 .. .. .. Nalcd (Dibrom) ND 1370 .. .. Parathion; ethyl ND 1370 .. .. .. Phoratc . 1370 -- .. .. .. Ronncl ND 1370 -- .. .. .. Sul l'otcp ND 1370 .. .. .. .. Sulprofos (Bolstar) ND 1870 .. .. .. TEPP ND 7480 . .. .. .. Tctrachlorvinphos (Rabon) ND 1870 '1 .. .. Tokuthion (Prothiofos) ND 1870 .. .. .. .. Trichloronatc ND 1870 -. .. .. . .. Surrogate: Yl'iIJ111y/ [Warp/mm (Sm?r) 2611 Limilx; 511-] Va 5-05 phat-7711mm (Sun) 1'62 121111171:- 60-130 3-05 DRAFT REPORT The rem/Ix pmt-?ict?cu? 1.11121 11:72an We and mu .vubjecl 11) change boxed 1m umtb'wis?. QC dam I'm'ictt'. I?lr'rm'c 1.116311: re?ll/LY 1171/1 {he .?hc?v may have no! by 1/70 DRAFT REPORT, DATA SUBJECT TO CHANGE We 8 0f? Report is complete only if it includes Calscience/ Euro?ns 8151 Data. Page 8 of 33 09/12/2017 503-718-2323 Phone $04 "In "1'11 12232 SW. Garden Place Apex Labs ?gala, 9R 97223 ,5 ?t Polk County Public Works NRC Project: 117041 Y6318-012-l7 621 Ensign St Project Number: 117041 Reported: Portland, OR 97217 Project Manager: Roman Geiglc 09/06/17 10:45 ANALYTICAL SAMPLE RESULTS Percent Dry Weight Reporting Analytc Result DL Limit Units Dilution Date Analyzed Method Notes 53-1 (A7H0678-01) Matrix: Soil Batch: 7080981 Solids 89.5 1.00 by Weight 1 08/28/17 07:46 EPA 8000C SS-2 (A7H0678-02) Matrix: Soil Batch: 7080981 Solids 79.1 1.00 by Weight 1 08/28/17 07:46 EPA 8000C SS-3 (A7H0678-O3) Matrix: Soil Batch: 7080981 Solids 91.0 1:00 by Weight I 08/28/17 07:46 EPA 8000C DRAFT REPORT m- mum provided in :Im- rupur/ are ant/are .m/y'ucl change hated on .s?n/m?eqm?ni unubnwiv: QC ur?nu/ (lam rev/cw. I ?h?uxe me {have rum/{x w/rh lhr' r/m/ they may have mu been?nu/izct/ hv 1/71? DRAFT REPORT, DATA SUBJECT TO CHANGE Page 9 0121 Report is complete only if it includes Calscience Euro?ns 8151 Data. Page 9 of 33 09/12/2017 12232 SW. Garden Place Apex Labs 'l?igard, OR 97223 503-7 503-7 P011?Coun - Y6318?012i Works NRC Project: 117041 6211 Ensign St Project Number: 117041 Reported: Portland, OR 97217 Project Manager: Roman Geigle 09/06/17 10:45 QUALITY CONTROL (QC) SAMPLE RESULTS Organochlorine Pesticides by EPA 8081B Reporting Spike Source RPD Analyte Result MDL Limit Units Dil. Amount Result Limits RPD Limit Notes Batch 7080947 - EPA 3546 5011 Blank (7080947-BLK1) Prepared: 08/24/17 16:11 Analyzed: 08/25/17 10:59 EPA 8081 Dieldrin ND 0.909 ug/kg wet 1 Snrr.? (Surr) Recovery: 93 ?a Urn/12': 427/29 Di/mirm: Decac/r/uwhip/now] (Snrr) 92 65-15] LCS (7080947-881) Prepared: 08/24/17 16:11 Analyzed: 08/25/17 11:17 EPA 8081 Dieldrin 38.2 1.00 ug/kg wet 1 50.0 76 56?136% Sm?r.? 2.4.5.6-7171421' ('Snrr) Recovery: 92 42-1129 Dilution: I )ecuu/i/nm/iiphmnu? (Sun) Va 65?15! Batch 7081054 - EPA 3546 3011 Blank (7081054-BLKI) Prepared: 08/24/17 16:11 Analyzed: 08/30/17 12:22 EPA 8118113 Aldrin ND 1.82 ug/kg wet I alpha?1311C ND 1.82 beta~BHC ND 1.82 delta-1311C ND 1.82 gamma-1311C (Lindane) ND 1 82 cis-Chlordane ND 1,82 trans?Chlordane ND 1 .82 - ND 1.82 ND 1.82 ND 1.82 Dieldrin ND 1.82 - Endosull?an 1 ND 1.82 Endosull?an 11 ND 1.82 Endosullan sulfate ND 1.82 Endrin ND 1.82 Endrin A1dehyde ND 1.82 Endrin ketone ND 1.82 l-Icptachlor ND 1.82 Heplaelilor epoxide ND 1.82 Methoxyehlor ND 5.45 Chlordane (Technical) ND 54.5 DRAFT REPORT The in Ill/N rcpur! are and are ?Inject change based on QC min/mm? m??im/ dam review. Name me {have rem/Ix will; the I/m! I/iey may have no! been?nu/izer/ by Ike l'a/mrulmjt DRAFT REPORT, DATA SUBJECT TO CHANGE Page 10 012' Report is complete only if it includes Calscience Euro?ns 8151 Data. Page 10 of 33 09/12/2017 Polk County Public Works Y6318-012-17 12232 SW. Garden Place Labs 'l?igard, OR 97223 503-718-2323 Phone 503-718-0333 Fax . NRC Project: I 17041 621 Ensign St Project Number: 1 17041 Reported: Portland, OR 97217 Project Manager: Roman Geigle 09/06/17 10:45 QUALITY CONTROL (QC) SAMPLE RESULTS ll Organochlorine Pesticides by EPA 8081B Reporting Spike Source RFD Analytc Result MDL Limit Units Dil. Amount Result Limits RPD Limit Notes Batch 7081054 - EPA 3546 Soil Blank Prepared: 08/24/17 16:11 Analyzed: 03/30/17 12:22 C-OS EPA 8081 Toxaphcne (Total) ND 54.5 ug/kg wet Sm?r: (SHIT) Recovery: 61') 42-129 Dilution: 1X Dycac/iloru/n?p/miv/ SJ 65-1511 LCS (7081054-331) Prepared: 08/24/17 10:11 Analyzed: 08/30/17 12:39 C-OS EPA 8081 Aldrin 25.5 2.00 ug/kg Wei 1 50.0 51 45-136% alpha-BHC 24.1 2.00 1' 48 45?137% beta-BHC 35 .0 2.00 7o 50- 1 36% delta-1311C 33.1 2.00 76 47-139% gamma-BHC (Lindanc) 26.3 2.00 53 49-135% ciS-Chlordanc 34.6 2.00 69 54-133% trans-Chlordanc 35.0 2.00 70 53-135% 45.2 2.00 90 56-1 39% 42.8 2.00 86 56-134% 55.5 2.00 11 1 50-141% -M Dieldrin 1 36,7 2,00 73 56-136% Endosullim 1 34,2 2.00 68 52-132% Endosulfan 11 414 2.00 83 53-134% Endosulfan sulfate 40.7 2.00 8] 55?136% Endi'in 47.8 2.00 --, 96 56-140% Aldehydc 35.0 2.00 70 35-137% 2-- Endrin ketonc 42.2 2.00 84 55- 36% Heptachlor 25.0 2.00 50 47- 1 36% l-leptachlor cpoxide 30.8 2.00 62 52-136% 63.6 6.00 127 52-143% Sir/'7': 2.45641 714,1??5um?) 47 ?u Linn/Ix: 42?129 D0each/nm/ifp/wny/ ?a 65 5/ Duplicate (7081054-DUP1) Prepared: 08/24/17 16:11 Analyzed: 08/30/17 13: 14 C-05 QC Source Sample: (A7H0678-01RE1) EPA 80813 Aldrin ND 11.9 ug/kg dry 1 ND 30"u alpha-1311C ND 5.17 ND 30" 0 beta-BHC ND -2- 12 .0 1' ND 30% DRAFT REPO RT The ran/Lt provided I/im' are 1' and are mfg/cor Ir: change hatred on (mu/wilt, QC m/idmirm or??nri/ dam review. l?t'c?m'c we [have rem/tr Will? My Ihm? I/icy may have not been?nuhzcd by the DRAFT REPORT, DATA SUBJECT TO CHANGE Page 1? Report is complete only if it includes Calscience/ Euro?ns 8151 Data. Page 11 of 33 09/12/2017 Apex Labs 12232 SW. Garden Place Tigard, OR 97223 503-718-2323 Phone 503-718-0333 Fm: NRC 6211 Ensign St Portland, OR 97217 Project: [17041 Project Number: 1 17041 Project Manager: Roman Geigle Polk County Y6318-013?l7 Reported: Public 09/06/17 10:45 1 QUALITY CONTROL (QC) SAMPLE RESULTS Organochlorine Pesticides by EPA 8081B Reporting Spike Source RPD Analyte Result MDL Limit Units Dil, Amount Result Limits RPD Limit Notes Batch 7081054 - EPA 3546 Soil Duplicate Prepared: 08/24/17 16:11 Analyzed: 08/30/17 13:14 C-OS QC Source Sample: 55?] (A7HOG78-01REI) EPA 80813 delta-1311C ND 6.28 tug/kg dry ND 30% 13-02 gamma-BHC (Lindane) ND 1 1.2 ND 30% 13-02 einhlordane ND 6.17 ND 30% R437- trans-Chlordane ND 10.3 ND 30% 13-02 ND 17.6 ND 30% 13-02 42.4 2.20 28.9 38 30% Q-17 ND 22.8 ND 30% R-02 Dieldrin ND 5.28 ND 30% 13-02 EndOSLillan 1 ND 6.39 ND 30% R-02 Endosull?an 11 ND 8.15 ND 30% R-02 Endosui fan sulfate ND 2,42 ND 30" R-02 13ndrin ND 12.8 ND 30% R-02 Endrin Aldehyde ND 14.6 ND 30% R-02 13ndrin ketone ND 2.20 ND 30% l-leptachlor ND 19.7 ND 30% 13-07- Heptachlor epoxide ND 16.3 ND 30% 13-02 ND 135 ND 30% 13-02 Chiordane (Technical) ND 66.1 ND 30% ND 66.1 ND 30% Surr: (Surr) Ream-wry: 79 ?a 71/29 "a Dilution: Ix (Sun) 87 65-1/5] Matrix Spike (70811154-MSI) Prepared: 08/24/17 16:11 Analyzed: 08/30/17 14:07 C-OS QC Source Sumpie: SS-3 EPA 8081 Aldrin 32.3 2.16 ug/kg dry 1 541 ND 60 45-136% alpha-BHC 27.6 2.16 ND 51 45-137% beta-BHC 37.9 2.16 ND 70 50-136% delta-BHC 40.6 2.16 ND 75 47-139% gamma-BHC (Lindane) 30.3 2.16 ND 56 49-135% (sis-Chlordane 39.2 2.16 ND 73 54-133% trans?Chlordane 40.9 7.16 ND 73 53-135% 52.0 2.16 ND 92 56-13900 DRA FT RIZPO RT The ram/1x provided in Ihii repm?l are 1' In change boxed UH (ma/livid". QC valit/crlt'tm nr?nu/ dam review. we [have with My 1rm/crrlum/iug that they may have no: hccn?uuhzcr/ by the [chum/my DRAFT REPORT, DATA SUBJECT TO CHANGE Report is complete only if it includes Calscienee Euro?ns 8151 Data. Page 12 0133 Page 12 oi'21 09/12/2017 Apex Labs [2232 SW. Garden I?lac Tigard, OR 97223 503-718-2323 Phone na?n Polk County Public Works NRC 62!! Ensign St Portland, OR 97217 Project: 11704] Project Number: 1 Protect Manager: Roman Geigle Y6318-0l2-l7 Reported: 09/06/17 10:45 QUALITY CONTROL (QC) SAMPLE RESULTS Organochlorine Pesticides by EPA 8081B Reporting Spike Source RPD Analyte Result MDL Limit Units Dil. Amount Result Limits RPD Limit Notes Batch 7081054 - EPA 3546 Soil Matrix Spike (70810544181) Prepared: 08/24/l 7 l6: ll Analyzed: 08/30/l7 14:07 C-OS QC Source Sample: SS-3 EPA 8081 60.1 2.16 ug/kg dry 9.19 94 56-134% 68.8 2. 6 ND l8 50-l4 1% Dieldrin 4 .l 2.16 ND 76 56-l 36% Endosulfan 2.l6 ND 74 52-] 32% Endosulfan ll 45.5 2,16 ND 82 53-84% Endosuli'an sulfate 48.4 2,16 ND 89 55- 36% Endrin 55.7 2. l6 ND 99 S6-l40% "w Endr'in Aldehyde 41.9 2.16 ND 75 35-137% Endrin ketone 47.6 2.16 ND 88 55-136% Heptaehlor 32.3 2. 6 ND 60 47-136?o Heptachlor epoxide 38.3 2. 6 ND 68 52- 36% Mcthoxyehlor l02 6.49 ND I30 52- 43? Q43 Sirl?r: 24,16- Recovery: 46' Limr'rx: 42?129 Dilution: Ix Dcurchinrohr?phenyl (Stirr) 6'2 ?u 65-151 DRAFT REPORT The in rupnrl are l' and are In change hated (m amdrxis. QC validation ur?nul (lam review. l?lem'c we ilrexc rest/11x wi'lh the muleJ's-landing firm they may have no! been/inalized by .1th fuhnrrumjv DRAFT REPORT, DATA SUBJECT TO CHANGE Report is complete only if it includes Calscienee Euro?ns 8151 Data. Page 13 of 33 Page 13 of2l 09/12/2017 12232 S.W. Garden [?13 Apex Labs ligation 97223 503-718-2323 Phone 503-718-0333 Fa . Polk County Public Works NRC Project: 117041 Y6318-012-l7 6211 Ensign St Project Number: 117041 Reported: Portland, OR 97217 Project Manager: Roman Geigle 09/06/17 10:45 QUALITY CONTROL (QC) SAMPLE RESULTS I Organophosphorous Pesticides (OPPs) by EPA 8270B Reporting Spike Source RPD Analyte Result MDL Limit Units Dil. Amount Result Limits RPD Limit Notes Batch 7090311 - EPA 3546 Soil Blank (7090311-BLK1) Prepared: 09/05/17 12:13 Analyzed: 09/05/17 14:57 82701) OPP Azinphos methyl (Guthion) ND 41.7 ug/kg wet I Chlorpyrilbs ND 41.7 Coumaphos ND 4 I ,7 Demeton 0 ND 41,7 Demeton ND 41,7 Diazinon ND 4 I ,7 Diehlorvos ND 41.7 Dimethoate ND 41.7 Disultbton Ethoprophos (Prophos) ND 41,7 Fensull'othion ND 41.7 Fenthion ND 4 I .7 Malathion ND 4 I .7 Merphos ND 41.7 Methyl parathion ND 41.7 Mevinphos (Phosdrin) ND 4 I .7 Monocrotophos ND 41.7 Naled (Dibrom) ND 41.7 Parathion, ethyl ND 41.7 Phorate ND 41.7 Ronncl (Fenehlorphos) ND 41.7 SUI I?otep ND 4 I .7 Sulprolos (Bolster) ND 4 I .7 TEPP ND 167 'I?etraehlorvinphos (Rabon) ND 41.7 Tokuthion (Prothiofos) ND 41.7 Triehioronate ND 41.7 - Snrr: 71-i/mtv/p/mxp/mle (Surr) Recovery: M3 "n Limits: 50-]4/ Dilution: Yi?ip/ieny/Idiom/raw (SHIT) 87 LCS (70903114181) Prepared: 09/05/17 12:13 Analyzed: 09/05/17 15:33 Q-IS 8270B Azinphos methyl (Guthion) 387 . 50.0 ug/kg wet I 400 97 38-156% Chlorpyrifos 324 50.0 SI 47- 140% DRAFT REPORT The provided in Ill/x repru'! are and are subjucl to change bowed rm (mu/mix. QC min/(4mm ur?nu/ (lam review, I ?lerme use {have rem/Ix with the inn/ehvlumfing rim! l/iey may have no! heel/finalized by Ike REPORT, SUBJECT TO CHANGE Page 14 012' Report is complete only if it includes Calseience Eurofins 8151 Data. Page 14 of 33 09/12/2017 Apex Labs 12232 S.W. Garden Place 'l?iga rd, OR 97223 503-718-2323 Phone 503-713-0311 - ks Polk County Publ?? wor 1 NRC Project: 117041 Y6313'0?1'l7 621 1 Ensign St Project Number: 117041 Reported: Portland. OR 97217 Project Manager: Roman Geigle 09/06/17 10:45 QUALITY CONTROL (QC) SAMPLE RESULTS Organophosphorous Pesticides (OPPs) by EPA 8270B (GCIMS) Reporting Spike Source RPD Analytc Result MDL Limit Units Di1. Amount Result Limits RPD Limit Notes Batch 7090311 - EPA 3546 Soil LCS (7090311?881) Prepared: 09/05/17 12: 13 Analyzed: 09/05/17 15:33 82700 OPP Coumaphos 417 50.0 ug/kg wet 104 37-160% Demeton 976 500 97.6 100 43-1 17% Demeton 245 50.0 268 91 Diazinon 369 50.0 400 92 42?134% Dichlorvos 422 50.0 106 39-142% Dimethoate 386 50.0 97 16-139% Disu11?oton 387 60.0 97 28- 144% EPN 423 50.0 106 44-137"o Ethoprophos (Prophos) 400 50.0 100 47~128% 501 50.0 125 27-147% .-- 0?41 Fenthion 352 50.0 88 44-134% Malathion 319 50.0 80 46-137% Merphos 331 50.0 83 0-153%? Methyl parathion 340 50.0 85 49-138?o Mcvinphos (Phosdrin) 372 50.0 93 12-176% Monocrotophos 432 50.0 108 65- 1 35% Q41 Naled (Dibrom) 398 50.0 99 0~174% Parathion, ethyl 329 50.0 82 50-139% Phorate 436 50.0 109 23-142?o 0-41 Ronne1 319 50.0 80 45-138% Sulf'otep 466 50.0 1 16 52- 26% 0-41 Sulprofos (Bolstar) 354 50.0 89 48-139% TEPP 425 200 106 30- 1 50% 0?41 "l'ctrachlorvinphos (Rabon) 305 50.0 76 54-129% Tokuthi?n (Prothiofos) 314 50.0 79 45-136% '1?rich1oronatc 294 50.0 74 37?140% Hru'r: Yir'ihiiry/ phm?p/m/c (Snrr) It)! 0 50-Hl Di/n/iwi.? 77'I'phetrv/ p/mxp/Ia/e 81') Duplicate Prepared: 09/05/17 12:13 Analyzed: 09/05/17 1837 QC Source Sample: (AH-10678411) 82700 OPP Azinphos methy1 (Guthion) ND 474 ug/kg dry 10 ND 30% Coumaphos. ND 474 ND 30?11 DRAFT REPORT 7711: prov/dad in report are 1' and are Iu change flawed (m (mu/W's. QC l'a/Iu'ai/rm m?jlnu/ rat/fen: l?lc'm?e me Ilicxe rosy/(x will: rim I/iu! Ilicy may have not beet/finalized by Ike laboratory DRAFT REPORT, DATA SUBJECT TO CHANGE . Report is complete only if it includes Calscience I Euro?ns 8151 Data. Page 15 of 33 Page 15 0121 09/12/2017 Apex Labs 12232 S.W. Garden Place 'l?igard, OR 97223 503-718-2323 Phone 1211 Polk County Public Works NRC 6211 Ensign St Portland, OR 97217 Project: Project Number: 1 17041 Project Manager: Roman Geiglo Y6318-012-17 117041 Reported: 09/06/1710:45 QUALITY CONTROL (QC) SAMPLE RESULTS Organophosphorous Pesticides (OPPs) by EPA 8270D 7' Reporting Spike Source RPD Analyte Result MDL Limit Units Dil. Amounl Result Limits RPD Limit Notes Batch 7090311 - EPA 3546 Soil Duplicate Prepared: 09/05/17 12:13 Analyzed: 09/05/17 18:37 QC Source Sample: 85-] (117110678411) 82700 OPP Dcmeton 0 ND 474 ug/kg dry ND 30% Demelon ND 474 ND 30% Diuzinon ND 474 ND 30% Dichlorvos ND 474 ND 30% Dimethoate ND 474 ND 30% Disulloton 30% Ethoprophos (Prophos) ND 474 ND 30% Fensulfothion ND 474 ND 30% ND 3130 ND 30% R-02 Malathion ND 474 ND 30% Merphos ND 474 ND 30% Methyl parathion ND 474 ND -.- 30% Mcvinphos (Phosdrin) ND 474 ND 30% Monocrotophos ND 474 ND 30% Naled (Dibrom) ND 474 ND 30% Parathion, ethyl ND 474 ND -.- 30% Phorate ND 474 ND 30% Ronnel (Fenchlorphos) ND 474 ND 30% Sull'otep ND 474 ND 300n Sulprofos (Bolstar) ND 474 ND 30% TEPP ND 1900 ND 30% 'I?ctrachlorvinphos (Rabon) ND 474 ND -.- 30% Tokuthion (Prothiofos) ND 474 ND -.. 30% Triohloronate ND 474 ND 30% Sure: "u Lim/l'x: 5/l-H/ [Jr/rum?: lf/x phosphate Ht) 60?131) Duplicate Prepared: 09/05/17 12:13 Analyzed: 09/05/17 19:13 QC Source Sample: 8270B OPP Chlorpyrilbs 114001) 4740 ug/kg dry 100 101000 12 30% DRAFT REPORT The rem/Irprovider! in this report are and are ,s'H/y'dc/ Change bm?m/ rm subsequent (inn/mix, QC m/idmiun ur?rm/ dam rev/cut tare {have rum/Ix wit/1 r/1e 1/le they may have no! been/inalizml' by 1/10 tuba/mam: DRAFT REPORT, DATA SUBJECT TO CHANGE Report is complete only if it includes Calscience I Eurofins 8151 Data. Page 16 of 33 Page 16 09/12/2017 0121 Apex Labs ,4/1 12232 SW. Garden Place Tigard, OR 97223 503-718-2323 Phone 503-718?0333 Fav - orks 1k CounW Pub? NRC Project: 1171141 ?90 a 18 0947 6211 Ensign SI Project Number: 1 17041 Reported: I?Ortland? OR 97217 Project Manager: Roman Gciglc 09/06/17 10:45 QUALITY CONTROL (QC) SAMPLE RESULTS Percent Dry Weight 11 Reporting Spike Source RPD Analytc Resuli MDL Limit Units D11. Amount Result Limits RPD Limit Notes Batch 7080981 - Total Solids (Dry Weight) Soil DRAFT REPORT The ram/1.1provided in flux rcpm'i' are and .1'11lqj'ccl change hm?uu? 1m (mu/111111" val/(lanai: ur?nul dam rev/cw, I'Icru?e me [have 1/111 Ilia! they may hm'c no! hcc'u?nulizet/ by 1/11) (?burglary DRAFT DATA SUBJECT TO CHANGE Report is compiete only if it includes Calscience Euro?ns 8151 Data. Page 17 of 33 Page 17 of21 09/12/2017 Apex Labs 12232 S.W. Garden Place Tigard, OR 97223 503?718-2323 Phone NRC 6211 Ensign St Portland, OR 97217 Project: Project Number: 117041 117041 Project Manager: Roman Geigle 1 Reported: 09/06/17 10:45 Polk County Public Works SAMPLE PREPARATION INFORMATION Organochlorine Pesticides by EPA 8081B Prep: EPA 3545 Sample Default RL Prep Lab Number Matrix Method Sampled Prepared ?1111910711131 Initial/Final 1299101 Batch: 7081054 A7H0678-01RE1 Soil EPA 8081B 08/23/17 10:05 08/24/17 16:11 710.15g/10mL 10g/5mL 1.97 Soil EPA 808113 08/23/17 10:11 08/24/17 16:11 10.25g/10mL 10g/5mL 1.95 A71-10678-03RE1 Soil EPA 808113 08/23/17 10:16 08/24/17 16:11 10.11g/10mL 10g/5mL 1.98 ll Organophosphorous Pesticides (OPPs) by EPA 8270B Prep: EPA 3546 Sample Default RL Prep Lab Number Matrix Method Sampled Prepared Initial/Final Initial/Final Factor Batch: 7090311 A7l?10678-01 Soil 8270B OPP (18/23/17 10:05 09/05/17 12:13 11.76g/5mL 10g/5ml, 0.85 Soil 82700 OPP 08/23/17 10:05 09/05/1712113 11.76g/5mL 10g/5mL 0.85 $011 82701) OPP (18/23/17 10:11 09/05/17 12:13 11.52g/SmL 10g/5m13 0.87 A71-10678-03 Soil 8270D OPP (18/23/17 10:16 09/05/17 12:13 11.76g/5mL 10g/5mL 0.85 Percent Dry Weight _1 Prep: Total Solids (Dry Weiqht) Sample Default RL Prep Lab Number Matrix Method Sampled Prepared Initial/Final Initial/Final 1730101 Batch: 7080981 Soil EPA 8000C 08/23/17 10:05 08/25/17 13:08 NA A71-10678-02 Soil EPA 3000C 08/23/17 10:11 08/25/17 13:08 NA A7110678-03 Soil EPA 8000C 08/23/17 10:16 08/25/17 13:08 NA DRAFT REPORT DRAFT REPORT, DATA SUBJECT TO CHANGE Report is complete only if it includes Calscience I Euro?ns 8151 Data. Page 18 of 33 Thu rem/m prom/ml in Jim- rcpm'l are and are tilt/year change bm?cc/ (m (mu/um: QC mitt/(Him: nr?na/ c/Erm review, Hem-c we :?wac raw/Ix with {he r/ml r/my may no: been?ml/km/ by the [chord/my 09/12/2017 Page 18 0121 [2232 SW. Garden Place Apex Labs ?gator; 97223 503?718-2323 Phone 0 13.. Polk County Public Works NRC Project: 117041 Y6318-012-l7 62H Ensign St Project Number: ll704l Reported: Portland, OR 97217 Project Manager: Roman Geigle 09/06/l7 10:45 Notes and De?nitions Qualifiers: C-05 Extract has undergone a GPC (Gel?Permeation Chromatography) cleanup per EPA 3640A. Reporting levels may be raised due to dilution necessary for cleanup. Sample Final Volume includes the GPC dilution factor, see the Prep page for details. Q-l7 RPD between original and duplicate sample is outside ofestahlished control limits. Matrix Spike results for this extraction batch are not reported due to the high dilution necessary for analysis ofthe source sample. Q-4l Estimated Results. Recovery ofContinuing Calibration Verification sample above upper control limit for this analyte, Results are likely biased high. Q-42 Matrix Spike and/or Duplicate analysis was performed on this sample. Recovery or RPD for this analyte is outside laboratory control limits. (Refer to the QC Section ofAnalytical Report.) R-02 The Reporting Limit for this analyte has been raised to account for interference from coeluting organic compounds present in the sample. S-OS Surrogate recovery is estimated due to sample dilution required for high analyte concentration and/or matrix interference, Notes and Conventions: DET Analyte DETECTED ND Analyte NOT DETECTED at or above the reporting limit NR Not Reported dry Sample results reported on a dry weight basis, Results listed as ?wet' or without 'diy'designation are not dry weight corrected. RPD Relative Percent Difference MDL lf MDL is not listed, data has been evaluated to the Method Reporting Limit only. WMSC Water Miscible Solvent Correction has been applied to Results and MRl_.s for volatiles soil samples per EPA 8000C. Batch Unless specifically requested, this report contains only results for Batch QC derived front client samples included in this report. All QC analyses were performed with the appropriate Batch QC (including Sample Duplicates. Matrix Spikes and/or Matrix Spike Duplicates) in order to meet or exceed method and regulatory requirements. Any exceptions to this will be qualified in this report. Complete Batch QC results are available upon request. in cases where there is insufficient sample provided for Sample Duplicates and/or Matrix Spikes. a Lab Control Sample Duplicate (LCS Dup) is analyzed to demonstrate accuracy and precision ofthe extraction and analysis. Blank Apex assesses blank data for potential high bias down to a level equal to the method reporting limit (MRL), except for conventional Policy chemistry and l-lClD analyses which are assessed only to the MRL. Sample results llagged with a or 8-02 qualifier are potentially biased high ifthey are less titan ten times the level found in the blank for inorganic analyses or less than five times the level found in the blank for organic analyses. For accurate comparison ofvolatile results to the level found in the blank; water sample results should be divided by the dilution factor, and soil sample results should be divided by 1/50 of the sample to account for the sample prep factor. Results qualified as reported below the MRL may include a potential high bias if aSSociatcd with a or 8-02 qualified blank, and [3-02 qualifications are not applied tol qualified results reported below the MRL. QC results are not applicable. For example, Recoveries for Blanks and Duplicates, RPD for Blanks. Blank Spikes and Matrix Spikes, etc. Used to indicate a possible discrepancy with the Sample and Sample Duplicate results when the is not available. In this case. either the Sample or the Sample Duplicate has a reportable result for this analyte, while the other is Non Detect (ND). DRAFT REPORT The rem/ix provided in Jim repur.? are PREL/rl/HN/llt?l' and are In change based on rmah'xix. QC vrr/rri?rurrm (in/inn! dam rewaw. l?lerrse use these with 1/1? imu'erxi?rrnri'fng I/irn' they mrrir have not by the laboratory DRAFT REPORT, SUBJECT TO CHANGE Page '9 0f? Report is complete only if it includes Calseience/ Euro?ns 8151 Data. Page 19 of 33 09/12/2017 pnpuI 1! AIUO meldwoo podaa 123 sa 01,143 99 I0 03 962d "9190 L9L8 sugoma {aouagos VLVCI 1110:1318 .113qu OZ 332d Iii/1 LIILH if! ., 'g'jlnli?fllaml um .mmpanAIMd mu 75] )1 pnxuq dump mafquy am pm; .(H?A7f?l/mt7% 5211 En I, . Sign Street 513111.? Portland,OR97217 CHAIN 0F smwces 503-283-1150 mx 503-289-6568 LABORATORY ANALYSIS REQUEST - I Page I of_j__ Pregect: I Job #1 [7709 I 642% RIM: 2 Telephone: E0 ?3 5w 0 r? 29. Sampiers ?5 :53 Samgers SiggatureSEmmi?: a TIME MATRIX Naorcorm VOLUME 5% CD 00 ?5 :1 - We?? I i/ ?552:3; 5 I 7 9' {>53 5 I 5/7? Ll [01b 1 ?m vf l/ E: 2% [/?3233 SPECIAL Am: RE, :gmm?Ara-9x Date/TIme: ?1,1,1 Dare/Time;a i ME: :i'gmfaw e. ANALYIICAL LABORATORY (Ii-5?1 Due/Time; J6: Sampfes on Ice? Temperature: Revised 3i281201 qufI xedV urn-4 94% 4?1 330 9.374 ?3 1N 7N :94 :1 33'8ch names ZCZZI mom aIand riwnog Apex Labs Polk County ?3le lie 63 ?l 8'0 ?241?. mace l'igard, OR 97223 \7/9 503-718-2323 Plume 503-718-0333 Fax NRC 62H Ensign St Portland.OR 972i? Project: 11704] Project Number: 1 17041 Project Manager: Roman Geigle Reported: 09/06/17 10:45 APEX LABS COOLER RECEIPT FORM i. - CHEM: Element WOfl: A7 [thl?id l3: ii?) Li? Delivery info: . . Datefiime Received: i ii By: i Delivered byzApex Client FedEx Cooler Inspection Inspected by: filii it? ti Chain ofCuslody included? Yes A No Custody Seals? Yes?__ Signed/Dated by Client? Yes 5.. No Signed/Dated by Apex? Yes No Cooler #1 Cooler #2 Cooler #3 Cooler #4 Cooler #5 Cooler #6 Cooler #7 Temperature (deg. C) Received on lee? Temp. Blanks?@N) rbi} lce Type: Ere/i cal/Other) Condition: Cooler out oflemp? Possible reason why: if some coolers are in let and some out, 'recn dot applied 0 ul' ftemperalure?ampies? Yes/Nol@ Samples Inspection: Inspected by: i All Samples lntact?? Yes No Comments: Borne Labels/COGS agree? YesL No Comments: Received Appropriate for Analysis? Yes 3? No a? Comments: Do VOA Vials have Visible l-lcadspace?? Yes NA Comments -. Water Samples: pH Checked and Appropriate (except VOAs): Comments: Additional information: A Labeled by: Witness: Cooler Inspected by: See Project Contact For?Y/ km WK. DRAFT REPORT The Peru/Ix provided in [his are I l? and are nth/cc: to change based on .i'in'm'cqueiil cmtl/Vxl'n'. QC i?ci/idmiun (lam rcw'cn'. l?icm?c rm: thew resell? with lht? miri'i'rh?mnding Ilmi they may Inn-e imi been?nalized by {he laboratory DRAFT REPORT, DATA SUBJECT TO CHANGE Report is complete only if it includes Calscienee I Eurofins 8151 Data. Page 21 of 33 PageZl oi'21 09/12/2017 eurofins The (Ii/fei'ence is service AER SOEL i WATER Analytical Report For Client: APEX Laboratories, LLC Client Project Name: A7HO678 Attention: Darwin Thomas 12232 SW Garden Place Portland, OR 97223-8246 Approved for release on 09/12/2017 by: Lori Thompson Project Manager Euro?ns Calscience. Inc. (Calscience) certifies that the test results provided in this report meet all NELAC requirements for parameters for which accreditation is required or available. Any exceptions to NELAC requirements are noted in the case narrative. The original report of subcontracted analyses, if any, is attached to this report. The results in this report are limited to the sample(s) tested and any reproduction thereof must be made in its entirety. The client or recipient of this report is speci?cally prohibited from making material changes to said report and. to the extent that such changes are made. Calscience is not responsible, legally or otherwise. The client or recipient agrees to indemnify Calscience for any defense to any litigation which may arise. 5e; 1. masts Ewe LAME rteE Report is complete only if it includes Calscience Euro?ns 8151 Data Page 22 of 33 09/12/2017 \4 0? - - Pub 23f: euroflns 61) Calscience Y6) Contents Client Project Name: A7H0678 Work Order Number: 17-08-2176 1! 3 2 Sample Summary 4 3 Client Sample Data 7 5 3.1 EPA 8151A Chlorinated Herbicides (Solid) 5 4 Quality Control Sample Data 6 4.1 6 4.2 7 5 Sample Analysis Summary 8 6 Glossary of Terms and Qualifiers 9 7 Receipt Form 10 7440 Lincoln Way. Garden Grove, CA 92841-1427 - TEL: (714) 895-5494 . FAX: (714) 894-7501 Report is complete only if it includes Calscience/ Euro?ns 8151 Data? Page 23 of 33 09/12/2017 Page bl'ic WorkS ?33? EU I?Dfl ?5 Work Order Narrative Polk County ?97? Calscience Y63l3'm2" Work Order: 17-08-2176 Page of ?l Condition Upon Receipt: Samples were received under Chain-of-Custody (COC) on 08/26/17. They were assigned to Work Order 17-08-2176. Unless otherwise noted on the Sample Receiving forms all samples were received in good condition and within the recommended EPA temperature criteria for the methods noted on the (300 The CDC and Sample Receiving Documents are integral elements of the analytical report and are presented at the back of the report. Holding Times: All samples were analyzed within prescribed holding times (HT) and/or in accordance with the Calscience Sample Acceptance Policy unless otherwise noted in the analytical report and/or comprehensive case narrative, if required. Any parameter identified in 4OCFR Part 136.3 Table ii that is designated as "analyze immediately" with a holding time of 15 minutes (4OCFR-136.3 Table ll, footnote 4), is considered a "field" test and the reported results will be qualified as being received outside of the stated holding time unless received at the laboratory within 15 minutes of the collection time. Quality Control: All quality control parameters (QC) were within established control limits except where noted in the QC summary forms or described further within this report. Subcontractor Information: Unless otherwise noted below (or on the subcontract form), no samples were subcontracted. Additional Comments: Air Sorbent-extracted air methods (EPA EPA TO-10, EPA TO-13A, EPA TO-17): Analytical results are converted from mass/sample basis to mass/volume basis using client-supplied air volumes. Solid - Unless othenivise indicated, solid sample data is reported on a wet weight basis, not corrected for moisture. All QC results are always reported on a wet weight basis. 7440 Lincoln Way, Garden Grove, CA 92841?1427 - TEL: (714) 895-5494 . FAX: (714) 894-7501 Report is complete only if it includes Calscience Euro?ns 8151 Data. Page 24 of 33 09/12/2017 Page4of12 gotta 1 . ?32? EU ?5 Sample Summary Polk County works i Calscience y6318-012-l7 Client: APEX Laboratories, LLC Work Order: ?l7-08-2176 12232 SW Garden Place Project Name: A7H0678 Portland, OR 97223?8246 PO Number: Date/Time 08/26/17 09:30 Received: Number of 1 Containers: Attn: Darwin Thomas Sample Identification Lab Number Collection Date and Time Number of Matrix Containers 88?4 17-08?2176-1 08l23ll7 11200 1 Solid 7440 Lincoln Way, Garden Grove, CA 92841-1427 - TEL: (714) 895-5494 FAX: (714) 894-7501 Report is complete only if it includes Calscience/ Euro?ns 8151 Data. Page 25 of 33 09/12/2017 rOfi '15 Analytical Report Page 5 of 12 Polk County Public Works Y6318-012-l7 APEX Laboratories, LLC Date Received: 08/26/17 12232 SW Garden Place Work Order: 17-08?2176 Portland, OR 97223-8246 Preparation: EPA 8151A Method: EPA 8151A Units: ug/kg Project: A7H0678 Page 1 of 1 Client Sample Number Lab Sample Date/Time Matrix Instrument Date Date/Time QC Batch ID Number Collected Prepared Analyzed 58-4 17-08-2176-1-A 08/23/17 Solid GC 40 09/01/17 09/07/17 170901L12 11:00 17:44 Comment(s): - Results are reported on a dry weight basis. - Results were evaluated to the MDL (DL), concentrations to the MDL (DL) but RL (LOQ). if found, are qualified with a flag. Parameter Result Quali?ers Dalapon ND 420000 120000 1000 Dicamba 17000 2100 1000 MCPP ND 17000000 5300000 1000 MC PA ND 17000000 3500000 1000 Dichlorprop ND 170000 28000 1000 44,1 1' 320000 M?h . 170000 24000 1000 (Silvex) ND 17000 4000 1000 2.4.5-T ND 17000 1900 1000 ND 170000 27000 1000 Dinoseb ND 84000 8600 1000 Surrogate Rec. We) Control Limits Qualifiers 2,4-Dichlorophenylacetic acid 0 44-146 1.2.6 Method Blank 095-01-033-1499 NIA Solid GC 40 09/01/17 170901 L12 Comment(s): - Results were evaluated to the MDL (DL), concentrations to the MDL (DL) but RL (LOO). if found, are quali?ed with a ?ag. Parameter Quali?ers Dalapon ND 250 73 1.00 Dicamba ND 10 1.2 1.00 MCPP ND 10000 3200 1.00 MCPA ND 10000 2100 1.00 Dichlorprop ND 100 17 1.00 2.4-D ND 100 14 1.00 (Silvex) ND 10 2.3 1.00 ND 10 1.1 1.00 ND 100 16 1.00 Dinoseb ND 50 5.1 1.00 urr Rec. Limits Qualifiers 2,4-Dichlorophenylacetic acid 52 44-146 RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit. 7440 Lincoln Way. Garden Grove. CA 92841-1427 TEL: (714) 895-5494 - FAX: (714) 894-7501 Report is complete only if it includes Calscience I Euro?ns 8151 Data. Page 26 of 33 09/12/2017 eurofins Page 6 of12?.? diet Quality Control - Spike/Spike Duplicate We Works Polk 63 \8?0 114 APEX Laboratories, LLC Date Received: 08/26/17 12232 SW Garden Place Work Order: 17-08?2176 Portland. OR 97223-8246 Preparation: EPA 8151A Method: EPA 8151A Project: A7H0678 Page 1 of 1 Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed Batch Number 17-09-0001-17 Sample Solid GC 40 09/01/17 09/07/17 15:25 170901812 17-09-0001-17 Matrix Spike Solid GC 40 09/01/17 09/06/17 23:38 170901812 17-09-0001-17 Matrix Spike Duplicate Solid GC 40 09/01/17 09/07/17 00:02 170901812 Parameter Sam Ie Sm ?g MSD MSD %Rec. CL BBQ RPD CL Quali?ers Added Conc. %Rec. Conc. %Rec. 2.4-D 375.2 400.0 814.1 110 674.3 75 32-146 19 0-37 71.86 40.00 88.47 42 72.71 2 27-147 20 0-37 2.4-DB ND 400.0 484.1 121 417.3 104 31-151 15 0-42 RPD: Relative Percent Difference. CL: Control Limits 7440 Lincoln Way. Garden Grove, CA 92841-1427 - TEL: (714) 895-5494 FAX: (714) 894-7501 Report is complete only if it includes Calscience Euro?ns 8151 Data. Page 27 of 33 09/12/2017 eurofins Quality Control - LCS Page 7 of 12 xx. 479%.) k/ Polk County Public Works Y63l8?012-l7 APEX Laboratories, LLC Date Received: 08/26/17 12232 SW Garden Place Work Order: 17-08-2176 Portland, OR 97223-8246 Preparation: EPA 8151A Method: EPA 8151A Project: A7H0678 Page 1 of 1 Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 095-01-033-1499 LCS Solid GC 40 09/01/17 09/07/17 00:25 170901 L12 Parameter Spike Adged Conc. Recovered LCS %Reo O/oRec. CL Quali?ers 2.4-D 400.0 317.0 49-127 40.00 28.00 31-145 24-08 400.0 3510 48-132 RPD: Relative Percent Difference. CL: Control Limits 7440 Lincoln Way, Garden Grove, CA 92841-1427 TEL: (714) 895-5494 FAX: (714) 894-7501 Report is complete only if it includes Calscience Euro?ns 8151 Data. Page 28 of 33 09/12/2017 Page 8 3 ?a . eu I?Ofl ?5 i Sample Summary Report Polk County PubW I Calscience . Y6318-0l2-l7 Work Order: 17?08-2176 Page 1 of 1 Method Extraction Chemist ID Instrument Analytical Location EPA 8151A EPA 8151A 944 SC 40 1 Location 1: 7440 Lincoln Way, Garden Grove, CA 92841 7440 Lincoln Way. Garden Grove, CA 92841-1427 - TEL: (714) 895-5494 - FAX: (714) 894?7501 Report is complete oniy if it includes Calscience Euro?ns 8151 Data. Page 29 of 33 09/12/2017 Page 9 of 12 . 1 EU l?Ofl ?5 3 Glossary of Terms and Qualifiers 901k County PUblic Works Catscience 7 (L (\79?4 Work Order: 17-08-2176 Page 1 of 1 Qualifiers Definition See applicable analysis comment. Less than the indicated value. Greater than the indicated value. 1 Surrogate compound recovery was out of control due to a required sample dilution. Therefore, the sample data was reported without further clari?cation. 2 Surrogate compound recovery was out of control due to matrix interference. The associated method blank surrogate spike compound was in control and, therefore, the sample data was reported without further clari?cation. 3 Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to suspected matrix interference. The associated LCS recovery was in controlcontrol due to suspected matrix interference. 5 The or associated with this batch of samples was out of control due to suspected matrix interference. 6 Surrogate recovery below the acceptance limit. 7 Surrogate recovery above the acceptance limit. Analyte was present in the associated method blank. BU Sample analyzed after holding time expired. BV Sample received after holding time expired. Cl See case narrative. Concentration exceeds the calibration range. ET Sample was extracted past end of recommended max. holding time. HD The chromatographic pattern was inconsistent with the profile of the reference fuel standard. :2 HDH The sample chromatographic pattern for TPH matches the chromatographic pattern of the specified standard but heavier hydrocarbons 3. - were also present (or detected). HDL The sample chromatographic pattern for TPH matches the chromatographic pattern of the specified standard but lighter hydrocarbons were also present (or detected). .53 Analyte was detected at a concentration below the reporting limit and above the laboratory method detection limit. Reported value is estimated. JA Analyte positively identi?ed but quantitation is an estimate. ME LCS Recovery Percentage is within Marginal Exceedance (ME) Control Limit range 4 SD from the mean). ND Parameter not detected at the indicated reporting limit. Spike recovery and RPD control limits do not apply resulting from the parameter concentration in the sample exceeding the spike concentration by a factor of four or greater. 86 The sample extract was subjected to Silica Gel treatment prior to analysis. Recovery and/or RPD out-of?range. Analyte presence was not confirmed by second column or analysis. Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for moisture. All QC results are reported on a wet weight basis. Any parameter identified in 40CFR Part 136.3 Table II that is designated as "analyze immediately" with a holding time of 15 minutes (4OCFR-136.3 Table II, footnote 4), is considered a "field" test and the reported results will be qualified as being received outside of the stated holding time unless received at the laboratory within 15 minutes of the collection time. A calculated total result (Example: Total Pesticides) is the summation of each component concentration and/or. if flags are reported, estimated concentration. Component concentrations showing not detected (ND) are summed into the calculated total result as zero concentrations. 7440 Lincoln Way, Garden Grove, CA 92841-1427 - TEL: (714) 895-5494 - FAX: (714) 894-7501 Report is complete only if it includes Calscience Euro?ns 8151 Data. Page 30 of 33 09/12/2017 Ween Page 10of12 ?2-115 SUBCONTRACT ORDER Apex Laboratories A7H0678 SENDING LABORATORY: Apex Laboratories 12232 S.W. Garden Place Tigard, OR 97223 Phone: (503) 718-2323 Fax: (503) 718?0333 Project Manager: Darwin Thomas RECEIVING LABORATORY: Euro?ns_CalScience 7440 Lincoln Way Garden Grove, CA 92841-1427 Phone :(714) 895?5494 Fax: (714) 894-7501 Polk County Public Works Y6318-012-17 Sample Name: Soil Sampled: 08/23/17 11:00 (A7H0678-04) Analysis Due Expires Comments 8151A Herbicides (SUB) WTOO 09/06/17 11:00 Containers Supplied: (8)4 02 Glass Jar WM 7/7/r7 smoked (an 1/1/8th ?06165REIEahjd/By 1' Date Received By 9 Dat ?v Fed Ex (Shipper) - 17?? 0 CC 2g 730 Released By Date Received By Date Page 1 of] Report is complete only if it includes Calscience I Euro?ns 8151 Data. Page 31 of 33 09/12/2017 13 .2. 4.. . (503)718-2323 DATE: SAMPLE . 2.00 LB *2232 sw GARDEN PLACE CAD 471625MNH3920 OR 97223 SENDER UNTTEO STATES US To DANIELLE GONSMAN CALSCIENCE .7440 LINCOLN WAY GARDEN GROVE CA 92841 A (71:4) 895-5494 REF - DEPT: EDSinSATURDAY FIRST OVERNIGHT 7701 1808 6050 92841 CA us SNA Report is complete only if it includes Calscience I Euro?ns 8151 Data. Page 32 of 33 Page 1 of 12 Polk County Public Works 09/12/2017 WORKORDER NUMBER 17-5 9-123 Calscience SAMPLE RECEIPT CHECKLIST COOLER OF i CLIENT: WX DATE: 08/ [2017 TEMPERATURE: (Criteria: not frozen except sediment/tissue) - I Thermometer lD: SCB (CF: Temperature (w/o CF): CF): B??iank El Sat? . ?.10st El Sample(s) outside temperature criteria contacted by: . (New; El Sample(s) outside temperature criteria but received on ice/chilled on same day of sampling vowco?g?bm El Sampie(s) received at ambient temperature; placed on ice for transport by courier \(63 Ambient Temperature: Air [3 Filter Checked by; CUSTODY SEAL: Cooler Present and intact [3 Present but Not Intact ErNot Present El NIA Checked Sample(s) El Present and Intact El Present but Not intact Present El Checked by. 3/ SAMPLE CONDITION: Yes No received with samples ?Er COC document(s) received complete (Ei/ El Sampling date Sampling time Matrix Number of containers Cl No analysis requested Not relinquished No relinquished date No relinquished time Sampler?s name indicated on COC I El El Ei/ IIJ Sample container(s) intact and in good condition El" El 7 21/ Sufficient volume/mass for analyses requested l2/ El Samples received within holding time 12/ El Aqueous samples for certain analyses received within 15-minute holding time El pH El Residual Chlorine Dissolved Sulfide El Dissolved Oxygen CI Proper preservation chemical(s) noted on COC and/or sample container Ci [3 Unpreserved aqueous sample(s) received for certain analyses Volatile Organics Total Metals El Dissolved Metals Container(s) forcerlain analysis free of headspace Volatile Organics [3 Dissolved Gases (RSK-175) l2] Dissolved Oxygen (SM 4500) El Carbon Dioxide (SM 4500) Ferrous Iron (SM 3500) [3 Hydrogen Sulfide (Hach) TedlarTM bag(s)free of condensation El CONTAINER TYPE: . (Trip Blank Lot Number: Aqueous: Cl VOA CI 100PJ El 100PJna2 El 125AGB l3 El El 125PB El 125Panna 250AGB 250068 2500685 El 250PB 500AGB 500AGJ 500AGJs Ci 5OOPB D-TAGB iAGBna2 TPB 1PBna [3 El Solid:ja/4ozCGJ El El Sleeve EnCores?( El TerraCores?( CI Air: [3 TediarTM El Canister El Sorbent Tube PUF El Other Matrix Container: A Amber. Bottle. Clear, Envelope, Glass. Jan Plastic, and Ziploc/Resealable Bag Preservative: buffered. filtered. HCI, HNOs, na naz Nazszoa, H3PO4, Labeled/Checked by. 811/ H2804, ultra-pure. znna Zn Reviewed by: 22 2016-09-23 Revision Report is complete only if it includes Caiscience Euro?ns 8151 Data. Page 33 of 33 09/12/2017 4 2 (yr-IF Pam Pokcounw ??th works Y63 V3012 _17_ UW (2272122722 4W [Maj Caz/ Wm?