Serial_No:10111814:04 ANALYTICAL REPORT Lab Number: Client: L1839803 Steel Curtain Capital 5 May Court Mahwah, NJ 07430 ATTN: Frank Pallota Phone: (201) 921-8384 Project Name: ARSENIC REMEDIATION Project Number: Not Specified Report Date: 10/11/18 The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in its entirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original. Certifications & Approvals: MA (M-MA086), NH NELAP (2064), CT (PH-0574), IL (200077), ME (MA00086), MD (348), NJ (MA935), NY (11148), NC (25700/666), PA (68-03671), RI (LAO00065), TX (T104704476), VT (VT-0935), VA (460195), USDA (Permit #P330-17-00196). Eight Walkup Drive, Westborough, MA 01581-1019 508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com Page 1 of 17 Serial_No:10111814:04 Project Name: Project Number: Lab Number: Report Date: ARSENIC REMEDIATION Not Specified Alpha Sample ID Client ID L1839803-01 L1839803 10/11/18 Matrix Sample Location Collection Date/Time Receive Date A-STORM DRAIN WATER MAHWAH, NJ 09/30/18 12:58 10/03/18 L1839803-02 B-RETENTION BASIN WATER MAHWAH, NJ 09/30/18 13:02 10/03/18 L1839803-03 C-STREAM WATER MAHWAH, NJ 09/30/18 13:12 10/03/18 Page 2 of 17 Serial_No:10111814:04 Project Name: Project Number: ARSENIC REMEDIATION Not Specified Lab Number: Report Date: L1839803 10/11/18 NJ DEP Data of Known Quality Protocols Conformance/Non-Conformance Summary Questionnaire 1 For each analytical method referenced in this laboratory report package, were all specified QA/QC performance criteria followed, including the requirement to explain any criteria falling outside of acceptable guidelines, as specified in the NJDEP Data of Known Quality performance standards? YES 1a Were the method specified handling, preservation, and holding time requirements met? YES 1b EPH Method: Was the EPH Method conducted without significant modifications (see Section 11.3 of respective DKQ methods)? N/A 2 Were all samples received by the laboratory in a condition consistent with that described on the associated chain-of-custody document(s)? YES 3 Were all samples received at an appropriate temperature (4 ± 2° C)? YES 4 Were all QA/QC performance criteria specified in the NJDEP DKQP standards achieved? YES 5a Were reporting limits specified or referenced on the chain-of-custody or communicated to the laboratory prior to sample receipt? YES 5b Were these reporting limits met? YES 6 For each analytical method referenced in this laboratory report package, were results reported for all constituents identified in the method-specific analyte lists presented in the DKQP documents and/or site-specific QAPP? YES 7 Are project-specific matrix spikes and/or laboratory duplicates included in this data set? NO Note: Page 3 of 17 For all questions to which the response was "No" (with the exception of question #7), additional information must be provided in an attached narrative. If the answer to question #1, #1a or #1b is "No", the data package does not meet the requirements for "Data of Known Quality". Serial_No:10111814:04 Project Name: Project Number: Lab Number: Report Date: ARSENIC REMEDIATION Not Specified L1839803 10/11/18 Case Narrative The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report. Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requirements for all NELAP accredited parameters unless otherwise noted in the following narrative. The data presented in this report is organized by parameter (i.e. VOC, SVOC, etc.). Sample specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter. Tentatively Identified Compounds (TICs), if requested, are reported for compounds identified to be present and are not part of the method/program Target Compound List, even if only a subset of the TCL are being reported. If a sample was re-analyzed or re-extracted due to a required quality control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is designated with an "R" or "RE", respectively. When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the associated samples for each element are noted in the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific % recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report. All specific QC information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed along with any associated usability implications. Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted. Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the back of the report. In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the associated QC table. The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed along with any associated usability implications. Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical Standards requested on the Chain of Custody. HOLD POLICY For samples submitted on hold, Alpha's policy is to hold samples (with the exception of Air canisters) free of charge for 21 calendar days from the date the project is completed. After 21 calendar days, we will dispose of all samples submitted including those put on hold unless you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples. Air canisters will be disposed after 3 business days from the date the project is completed. Please contact Client Services at 800-624-9220 with any questions. Page 4 of 17 Serial_No:10111814:04 Project Name: Project Number: ARSENIC REMEDIATION Not Specified Lab Number: Report Date: L1839803 10/11/18 Case Narrative (continued) Report Submission All non-detect (ND) or estimated concentrations (J-qualified) have been quantitated to the limit noted in the MDL column. DKQP Related Narratives Report Submission All DKQP required questions were answered with affirmative responses; therefore, there are no relevant data issues to discuss. I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report. Authorized Signature: Title: Technical Director/Representative Page 5 of 17 Date: 10/11/18 Serial_No:10111814:O4 METALS Page 6 of 17 F Serial_No:10111814:04 Project Name: ARSENIC REMEDIATION Lab Number: L1839803 Project Number: Not Specified Report Date: 10/11/18 Lab ID: Client ID: Sample Location: L1839803-01 A-STORM DRAIN MAHWAH, NJ Sample Depth: Matrix: Water SAMPLE RESULTS Parameter Result Qualifier Date Collected: Date Received: Field Prep: Units RL MDL Dilution Factor Date Prepared Date Analyzed 09/30/18 12:58 10/03/18 Not Specified Prep Method Analytical Method Analyst Total Metals - Mansfield Lab Arsenic, Total Page 7 of 17 16.27 ug/l 0.5000 0.1650 1 10/05/18 13:30 10/09/18 15:56 EPA 3005A 1,6020B AM Serial_No:10111814:04 Project Name: ARSENIC REMEDIATION Lab Number: L1839803 Project Number: Not Specified Report Date: 10/11/18 Lab ID: Client ID: Sample Location: L1839803-02 B-RETENTION BASIN MAHWAH, NJ Sample Depth: Matrix: Water SAMPLE RESULTS Parameter Result Qualifier Units Date Collected: Date Received: Field Prep: RL MDL Dilution Factor Date Prepared Date Analyzed 09/30/18 13:02 10/03/18 Not Specified Prep Method Analytical Method Analyst Total Metals - Mansfield Lab Arsenic, Total Page 8 of 17 16.66 ug/l 0.5000 0.1650 1 10/05/18 13:30 10/09/18 16:01 EPA 3005A 1,6020B AM Serial_No:10111814:04 Project Name: ARSENIC REMEDIATION Lab Number: L1839803 Project Number: Not Specified Report Date: 10/11/18 Lab ID: Client ID: Sample Location: L1839803-03 C-STREAM MAHWAH, NJ Sample Depth: Matrix: Water SAMPLE RESULTS Parameter Result Qualifier Date Collected: Date Received: Field Prep: Units RL MDL Dilution Factor Date Prepared Date Analyzed 09/30/18 13:12 10/03/18 Not Specified Prep Method Analytical Method Analyst Total Metals - Mansfield Lab Arsenic, Total Page 9 of 17 7.272 ug/l 0.5000 0.1650 1 10/05/18 13:30 10/09/18 16:24 EPA 3005A 1,6020B AM F Serial_No:10111814:04 Project Name: ARSENIC REMEDIATION Project Number: Not Specified Lab Number: L1839803 Report Date: 10/11/18 Method Blank Analysis Batch Quality Control Parameter Result Qualifier Units RL MDL Dilution Factor Date Prepared Date Analytical Analyzed Method Analyst Total Metals - Mansfield Lab for sample(s): 01-03 Batch: WG1164742-1 Arsenic, Total ND ug/l 0.5000 0.1650 1 Prep Information Digestion Method: Page 10 of 17 EPA 3005A 10/05/18 13:30 10/09/18 14:29 1,6020B AM Serial_No:10111814:04 Lab Control Sample Analysis Project Name: ARSENIC REMEDIATION Project Number: Not Specified Parameter Batch Quality Control LCS %Recovery Total Metals - Mansfield Lab Associated sample(s): 01-03 Arsenic, Total Page 11 of 17 109 Qual LCSD %Recovery Qual Lab Number: L1839803 Report Date: 10/11/18 %Recovery Limits RPD 80-120 - Batch: WG1164742-2 - Qual RPD Limits Serial_No:10111814:04 Project Name: Lab Number: L1839803 Report Date: 10/11/18 ARSENIC REMEDIATION Project Number: Not Specified Sample Receipt and Container Information YES Were project specific reporting limits specified? Cooler Information Cooler A Custody Seal Absent Container Information Initial Cooler pH Final Temp pH deg C Pres Seal Frozen Date/Time Analysis(*) Container ID Container Type L1839803-01A Plastic 250ml HNO3 preserved A <2 <2 3.7 Y Absent AS-6020T-PPB(180) L1839803-02A Plastic 250ml HNO3 preserved A <2 <2 3.7 Y Absent AS-6020T-PPB(180) L1839803-03A Plastic 250ml HNO3 preserved A <2 <2 3.7 Y Absent AS-6020T-PPB(180) Page 12 of 17 *Values in parentheses indicate holding time in days Serial_No:10111814:04 Project Name: Project Number: ARSENIC REMEDIATION Lab Number: L1839803 Not Specified Report Date: 10/11/18 GLOSSARY Acronyms EDL EMPC EPA LCS LCSD - Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis of PAHs using Solid-Phase Microextraction (SPME). - Estimated Maximum Possible Concentration: The concentration that results from the signal present at the retention time of an analyte when the ions meet all of the identification criteria except the ion abundance ratio criteria. An EMPC is a worst-case estimate of the concentration. - Environmental Protection Agency. - Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. - Laboratory Control Sample Duplicate: Refer to LCS. MSD - Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. - Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. - Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. - Matrix Spike Sample Duplicate: Refer to MS. NA - Not Applicable. LFB MDL MS - Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit. NDPA/DPA - N-Nitrosodiphenylamine/Diphenylamine. NC NI - Not Ignitable. NP - Non-Plastic: Term is utilized for the analysis of Atterberg Limits in soil. RL STLP - Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL includes any adjustments from dilutions, concentrations or moisture content, where applicable. - Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precision of analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report. - Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples. - Semi-dynamic Tank Leaching Procedure per EPA Method 1315. TEF - Toxic Equivalency Factors: The values assigned to each dioxin and furan to evaluate their toxicity relative to 2,3,7,8-TCDD. TEQ - Toxic Equivalent: The measure of a sample¿s toxicity derived by multiplying each dioxin and furan by its corresponding TEF and then summing the resulting values. - Tentatively Identified Compound: A compound that has been identified to be present and is not part of the target compound list (TCL) for the method and/or program. All TICs are qualitatively identified and reported as estimated concentrations. RPD SRM TIC Footnotes 1 - The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the original method. Terms Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum. Final pH: As it pertains to Sample Receipt & Container Information section of the report, Final pH reflects pH of container determined after adjustment at the laboratory, if applicable. If no adjustment required, value reflects Initial pH. Frozen Date/Time: With respect to Volatile Organics in soil, Frozen Date/Time reflects the date/time at which associated Reagent Waterpreserved vials were initially frozen. Note: If frozen date/time is beyond 48 hours from sample collection, value will be reflected in 'bold'. Initial pH: As it pertains to Sample Receipt & Container Information section of the report, Initial pH reflects pH of container determined upon receipt, if applicable. Total: With respect to Organic analyses, a 'Total' result is defined as the summation of results for individual isomers or Aroclors. If a 'Total' result is requested, the results of its individual components will also be reported. This is applicable to 'Total' results for methods 8260, 8081 and 8082. Report Format: Page 13 of 17 DU Report with 'J' Qualifiers Serial_No:10111814:04 Project Name: Project Number: ARSENIC REMEDIATION Lab Number: L1839803 Not Specified Report Date: 10/11/18 Data Qualifiers A - Spectra identified as "Aldol Condensation Product". B - The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For MCP-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJAir-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit. For NJ-related projects (excluding Air), flag only applies to associated field samples that have detectable concentrations of the analyte, which was detected above the reporting limit in the associated method blank or above five times the reporting limit for common lab contaminants (Phthalates, Acetone, Methylene Chloride, 2-Butanone). - Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted analyses. - Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations of the analyte. - Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument. C D E G H - The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should be considered estimated. - The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection. I - The lower value for the two columns has been reported due to obvious interference. M - Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte. NJ - Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where the identification is based on a mass spectral library search. - The RPD between the results for the two columns exceeds the method-specified criteria. P Q R - The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing Calibration Standard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoveries when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less than 5x the RL. (Metals only.) - Analytical results are from sample re-analysis. RE - Analytical results are from sample re-extraction. S - Analytical results are from modified screening analysis. J - Estimated value. The Target analyte concentration is below the quantitation limit (RL), but above the Method Detection Limit (MDL) or Estimated Detection Limit (EDL) for SPME-related analyses. This represents an estimated concentration for Tentatively Identified Compounds (TICs). - Not detected at the method detection limit (MDL) for the sample, or estimated detection limit (EDL) for SPME-related analyses. ND Report Format: Page 14 of 17 DU Report with 'J' Qualifiers Serial_No:10111814:04 Project Name: ARSENIC REMEDIATION Lab Number: Project Number: Not Specified Report Date: L1839803 10/11/18 REFERENCES 1 Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates I - IV, 2007. LIMITATION OF LIABILITIES Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analytical shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable for any incidental, consequential or special damages, including but not limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha Analytical. We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding time and splitting of samples in the field. Page 15 of 17 Alpha Analytical, Inc. Facility: Company-wide Department: Quality Assurance Title: Certificate/Approval Program Summary Serial_No:10111814:04 ID No.:17873 Revision 12 Published Date: 10/9/2018 4:58:19 PM Page 1 of 1 Certification Information The following analytes are not included in our Primary NELAP Scope of Accreditation: Westborough Facility EPA 624/624.1: m/p-xylene, o-xylene EPA 8260C: NPW: 1,2,4,5-Tetramethylbenzene; 4-Ethyltoluene, Azobenzene; SCM: Iodomethane (methyl iodide), Methyl methacrylate, 1,2,4,5Tetramethylbenzene; 4-Ethyltoluene. EPA 8270D: NPW: Dimethylnaphthalene,1,4-Diphenylhydrazine; SCM: Dimethylnaphthalene,1,4-Diphenylhydrazine. EPA 6860: SCM: Perchlorate SM4500: NPW: Amenable Cyanide; SCM: Total Phosphorus, TKN, NO2, NO3. Mansfield Facility SM 2540D: TSS EPA 8082A: NPW: PCB: 1, 5, 31, 87,101, 110, 141, 151, 153, 180, 183, 187. EPA TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene, 3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 1-Methylnaphthalene. Biological Tissue Matrix: EPA 3050B The following analytes are included in our Massachusetts DEP Scope of Accreditation Westborough Facility: Drinking Water EPA 300.0: Chloride, Nitrate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N; SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500F-C, SM4500CN-CE, EPA 180.1, SM2130B, SM4500Cl-D, SM2320B, SM2540C, SM4500H-B EPA 332: Perchlorate; EPA 524.2: THMs and VOCs; EPA 504.1: EDB, DBCP. Microbiology: SM9215B; SM9223-P/A, SM9223B-Colilert-QT,SM9222D. Non-Potable Water SM4500H,B, EPA 120.1, SM2510B, SM2540C, SM2320B, SM4500CL-E, SM4500F-BC, SM4500NH3-BH: Ammonia-N and Kjeldahl-N, EPA 350.1: Ammonia-N, LACHAT 10-107-06-1-B: Ammonia-N, EPA 351.1, SM4500NO3-F, EPA 353.2: Nitrate-N, SM4500P-E, SM4500P-B, E, SM4500SO4-E, SM5220D, EPA 410.4, SM5210B, SM5310C, SM4500CL-D, EPA 1664, EPA 420.1, SM4500-CN-CE, SM2540D, EPA 300: Chloride, Sulfate, Nitrate. EPA 624.1: Volatile Halocarbons & Aromatics, EPA 608.3: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT, Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs EPA 625.1: SVOC (Acid/Base/Neutral Extractables), EPA 600/4-81-045: PCB-Oil. Microbiology: SM9223B-Colilert-QT; Enterolert-QT, SM9221E, EPA 1600, EPA 1603. Mansfield Facility: Drinking Water EPA 200.7: Al, Ba, Cd, Cr, Cu, Fe, Mn, Ni, Na, Ag, Ca, Zn. EPA 200.8: Al, Sb, As, Ba, Be, Cd, Cr, Cu, Pb, Mn, Ni, Se, Ag, TL, Zn. EPA 245.1 Hg. EPA 522. Non-Potable Water EPA 200.7: Al, Sb, As, Be, Cd, Ca, Cr, Co, Cu, Fe, Pb, Mg, Mn, Mo, Ni, K, Se, Ag, Na, Sr, TL, Ti, V, Zn. EPA 200.8: Al, Sb, As, Be, Cd, Cr, Cu, Fe, Pb, Mn, Ni, K, Se, Ag, Na, TL, Zn. EPA 245.1 Hg. SM2340B For a complete listing of analytes and methods, please contact your Alpha Project Manager. Document Type: Form Page 16 of 17 Pre-Qualtrax Document ID: 08-113 Serial_No:10111814:O4 JE Huh I: E: ENH- 35- 111111111 Fill Hulk! 5 P398 1 . Is . . CHAIN UF Albany. H11 12m: 14 19:11:.er :11 Data Rec. ALPHA Jana - - 1' 1 1-1 -1 Tm-mndl. 111111511: AH. sun- 1:15 in 1113 {la If}? W?lbg-?rzlul?L?u?-M?t Iii-lime] Il'fc-rlnHII-Im E: 313%: Elana-522.3% Pmisct Na me: Arsenic Ftamadlalinn NJ Fullr Reduced Same as Cllent Info I Praj?d Lucaljnn' Mahmh NJ EUUIS [1 Fil?} EQUIS {4 PD 1: Clnz-n'. 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