March 19, 2819 Env?mnme?tai Labarate?es 685 Stone Road Ste. 9 ~12 'Ti F: 701361.553? Ane?y?m? Repe? Client: Aim: Work Order Project: Pruject 53.0. Number: Project Received: Project Reperted: Sincerely, Timea Laboratory Director President Saiano County 675 Texas 3., Suite 5500 Fairfeild, CA 94533 Colby LaPiace 1903044 Fiue Gas Scrubber no me} March 15, 2019 13:50 March 19, 2019 11:41 Air+mter+ Soil WORK ORDER: 1903044 CDC Number: Fviranmentai Labaramries 585 Stone Road Ste. 9 - Benicla, CA 94510 T: F: 707.361.5589 wadeltaen?mnmentallahcom Solano County 675 Texas 5., Suite 5500 Fairfeild, CA 94533 Project: Hue Gas Scrubber PD Number: Project Manager: Colby LaPlaca Project #:[nonej Sampie Summary Lab ID Sample Matrix Date Sampied Date Received 1903044-01 FGS (3521 Aqueaus March 15, 2019 12:20 March 15, 2019 13:50 1903044?02 Petroieum Coke Solid March 15, 20:9 13:15 March 15, 2019 13:50 me con tents of W2: rem? away to Me anagrzed in accords-nae wib?r ma mam of msiaa?r darument. rLr'o mimics rim of (his (PM is affo meat except in its entirety Page 2 bf 13 rm?ted Sewica Testing Air Watar +53% WORK ORDER: 1903044 CDC Number: Envimnmentai Labarateries 685 StoneRnadSteB- 12 Beni?ia, 0319451 T: F: ?0?.361.5689 vmv?eltam?mnmta?ahm Salami) County 575 Texas 5., Suite 5506 Fairfeiid, CA 94533 Project: Fiue Gas Scrubber PD Number: Project Manager: Colby LaPlace Project #:[none] Sample Resuits Sampie: F65 6521 Sample Date: March 15, 2019 12:20 1903944-91 {Aqueous} Sample Type: Prep Date: March 18, 2019 10:18 - Dilution Analyte RepPrFIng Qual Result Unit Fact Date Method Batch! Limit 0" Analyzed Anaiyst Total Mercury by EPA 245.1 Mercury 0.0002 1.21 ugn. 1 EJ191154 EPA 245.1 IQCDIIGIBV The coma-#5 arms; rem-t appiy to the sewage-{s} anafyz-ed accordance mm #35 aim: of custoojr Mama-at. Na dupifra?on of this report is album: grep: .9: its entrref}: Page 3 of 13 Trusted Sea-mice ng m: Water 5311 E0111 101101011091 1000101101105 585 50:101.- Ruad 519.9 -12 Eenicia, CA 911510 T: F: 7913615689 00919.09lt09091mnm00t01100m WORK ORDER: 1903044 COG Number: Soiano County Progect: Flue Gas Scrubber 6251111159., Suite 5500 . 1: 111 1911011011, CA 99533 ?09 0000912 0 11 a ace Praject #:[11000] Sample Resuits (Continued) Sample Date: March 15, 2019 12:20 Sample: FGS G521 (Continued) 1903044-91 (Aquem?) Sample Type: Prep Date: March 18, 2019 10:42 01111111119 Reporting Qua, 911111: Unit Diluti?? Date Method 011112111 Limit Factor Analyzed Analyst Totai Metals by EPA 200.? (ICP-AES) Ammo"? 1.00 7.55 11011 2 3110119 EPA 200.2 19120119100 Arsenic 4.00 29.9 1191!. 2 3110119 EPA 200.7 19001191011 Barium 10.0 1111.1 ug1'L 2 3110119 EPA 200.2 191201191011 3&0?le 1.00 2.1.2 ug1L 2 3110119 EPA 200.1 191201191011 Cadmium 0.50 10.9 01111 2 3110119 EPA 200.2 191:01191011 Chromium 1.00 55.0 119111 2 3110119 EPA 200.2 10001191011 Cobatt . 1.00 54.3 0911. 2 3110119 EPA 200.1r 1900119100 0.20 52.2 01111 2 3110119 EPA 200.7 191201191011 Lead 1.00 3.92r 01111 2 3119119 EPA 200.2 191301191011 Molybdenum 1.00 114.1 0911 2 3110119 EPA 200.? 191301 1911111 Niche! 2.00 231' 09111. 2 3110119 EPA 200.7 19001191011 SPEBnium 0.100 37.0 0911. 2 3113119 EPA 200.2 191:0: 191011 0.500 09.5 0011. 2 3118119 EPA 2110.? 19001191011 Thaliium 2.00 43.7 091L 2 3110119 EPA 200.2 191:0.11 91011 Vanadium 2.00 545 ug1L 2 3110119 EPA 2001 19c0119101r Zinc 0.20 40.9 ug1L 2 3110119 EPA 2110.? 191201191011 ?re contents 01?1?1?11?5 raped 3121115110 1119 5010,0191?) 01101112190111 accordance 11110 00.9 drain of 0050:0111 document 110 51012150011 01? 1111'; 1.9100111; 011011190; 6200101101215 011111.902. Page 4 0f 13 Tn?tedSer?ceesting 1011' +WAber+ 5011 WGRK ORDER: 1933044 i'l" Env?renmersbal Leberate?es 685 Stone Road Ste. 3 -12 Benicia, CA 94519 T: F: @1361 .5689 CDC Number: Solano County 6?5 Texas 5., Suite 5500 Fairleilcl, CA 94533 Project: Flue Gas Scrubber PO Number: Project Manager: Colbyr LaF?laee Project Sample Results (Continued) Sample Date: March 15, 2019 13:15 Sample: Petroleum Coke 1903044~92 (Solid) Sample Type: Prep Date: March 18, 2019 10:22 Analyte Reporting Qua; Result .t Dilution Date Batch] Limit 53?1? Analyzed Analyst Total Mercury by EPA 1471 0.200 NI) 1 mam EPA rm 190311?le ?re contents of may report a?oat]: to me ?ame-(5) arr-3.5112953? (retardants. the drain of rumor document. No duplical?lm of this ream? is allowed except in its enrrlety Page 5 of 13 meted SermeTe??ng Air Meter Sail 51100000101113 1.311010121711100 685 Stone R030 5100.9 - 12 3001013, CA 94510 12 7'017416001 F: 3117.361 .5689 W?eitaem'imn man 131100.000: WORK ORDER: 1903944 CDC Number: Project: Flue Gas Scrubber PO Number: Project Managar: C0101 LaPlace Project #:[none] 5013110 County 675 Texas 5., Suite 5500 Fairfeiid, CA 94533 Sampie Results {Continued} Sampie Date: March 15, 2919 13:15 Sample: Petroleum Coke (Cantinued) 1903044412 Sample Type: Frag: Date: March 18, 2019 10:25 Analvte Reporting Qua; Result Unit Dilutian Date Math? 0001111 Limit Factor Analyzed Analyst Total Metals by EPA. 60108 An?rnony 0.20 110 010119 1 3110110 EPA 50100 1000110100 Arsenic 0.40 110 I mg1kg 1 3110110 EPA E0103 10001101011r Barium 2.42 ND 0191119 1 3119119 EPA 60103 191201 181131! Bendiium 0.24 mg1kg 1 3110110 EPA 60103 101201101011 Cadmium 0.24 00 11.9119 1 3110110 EPA 00100 10130110101! Chromium 0.20 0.00 0101110 1 3110110 EPA 60100 1000110100 Cobalt 0.40 1.00 010119 1 3110110 EPA 00100 1000113100 Copper 0.10 0.07 mg1kg 1 3110110 EPA 00100 1000110100 Lead 0.48 ND 11101110 1 3110110 EPA 0010B 10110110100 Mofvbdemm 0.00 1.05 1 3110110 EPA 00100 1000110100 Nickel 0.07 0.10 0191119 1 3110110 EPA 00100 10120110100 Selenium 0.40 0.05 019119 1 3110110 EPA 50100 101201101011 Siiver 0.24 1.10 mg1kg 1 3110110 EPA 50100 10110110100 Thallium 0.001 1.31 mg1kg 1 3110110 EPA E0100 10001101011 11000010111 0.0? 12.2 11191119 1 3110110 EPA 60100 1000110100 Zinc 0.10 1.34 0191119 1 3110110 EPA 00100 101301101011 HIE contents mam? 010.0111? :0 the 30111101013) 01101112000; accurdance with me 1-0010 of 111510.00 dammenr. 1113 dop?ca?bn 01100 rem-rt 1?5 31111111005 except 120 00 6110911001. .h Page 6 0f 13 Trustee: 51101101100110 0.111.101.0100: Envirenme?tal Labaratns?ieg 535 Stone Road Stag-12 Benicia,?A9451U T: ?17416681 F: T0136i5689 ww?altaemimmantailabmm WORK ORDER: 1903044 CBC Number: Solano County Project: Flue Gas Scrubber 675 Texas 5" SURE 5500 Sigyl?gger- Colby LaPIace Fatrfelld, CA 94533 Project #:[none} Quality Cantrul Total Mercury by EPA 245.1 Prepared: Mar-18-19 ?nalvzed: Mar-i949 Analyte Source Result Qua! Reporting Unit Spike RFD RFD Result Limit Level REC Limits Limit Batch: 1.960116 Blank (19C0116-BLK1) me con tents of this repart apply In Me analwed in accordance mm the sham ofwsrady documnt Na dupirlcanbn of Ms report is a?bwed, except .rh its entirem Page 7 0f 13 Analyst: UV 0.9992 2-00. 3:93.. 3911.3? . . a 00112 ugfL 2 on 119 30420 10 2 29 Tmsi'ed Sam Testing Air Water 4: Su? WORK ORDER: 1903044 CDC Number: Environmeetal Laborataries 585 Ste-me Road Ste. 9 -12 Benicia, CA 94510 T: F: mm?eltaewiranmente?ahmm Sula no County 6?5 Texas 5., Suite 550D Fairfeild, CA 94533 Project: Flue Gas Scrubber PO Number: Project Manager: Ceiby LaPlac?e Project #:{none] Total Mercury by 74?! Quality Contmi {Continued} Prepared 81 Analyzed: Mar-1849 Source Analyte Result Qua! Reporting Unit Spike OIDREC RFD RFD Result Limit Level REC Limits Limit Batch: 1.960117 Analyst: DV Blank . .3339"?! .31? 92.0.9 LCS {19(33117'351} . 9.2.99 91.537: 1.93 39:12.9 LCS Dup (19(30117-3501) Mercury 0.198 200 167 119 80-120 10 2 20 The contents of {his remrt 5;:th to the arrafyzed .c'n accordance with the chalk! of ELEM document, #0 animation rm? is 3th wee; except In it; antiwar. Page 8 of 13 Tmeted Eerwce?res?ng AEH WEter +Sei? E?vimnme?tal Laberatea?ies 085 Starla Fla-ad Shell-12 Benicia, 04510 T: ?0?.74?.0031 R?0?.35?l.5609 mwdeltaeevimnmentellabmm WORK ORDER: 1903044 Number: Solano County Project: Flue Gas Scrubber 67.5 Texas 5" SURE 5500 22:35::ager: Colby LaPlace Fairfelld, CA 94533 Project #:[none] Quality Control (Continued) Total Metals by EPA 200.7 Prepared El. Analyzed: Mar-1805 Analyte source Result Qua! Unit Spike ??0355 an RFD Result Limit Level REC Limits Limit Batch: 1960119 Analyst: 00 Blank (1950119-BLK1) Arsenic ND 2.00 ugll. Copper ND 0.10 ugfL Chromium ND 0.500 uglL Lead ND 0.500 ugfL Cadmium ND 0.25 ugfL Selenium ND 0.200 ug/?L Barium ND 5.00 ugii. Cobalt ND 0.500 ugfL Vanadium ND 1.00 ugfl. Beryllium ND 0.500 09.0. Zinc ND 0.10 ugfL Antimony ND 0.500 ugli. Molybdenum ND 0.500 0911. Nickel Ni: 1.00 ugfL Silver ND 0.250 ugll. Jewish! w. 9-00-. ?are LCS (19(30119-351) Arsenic 695 2.00 ugfL 600 116 80120 Barium 614 5.00 ugjL 600 102 80-120 Beryllium 599 0.500 09.11. 600 99.0 00-120 Cadmium 5178 0.25 ugfL 600 113 80?120 Chromium 595 0.500 ugfL 600 90.2 80120 Antimony 576 0.500 0911. 500 113 80?120 Nickel 69 2 1 .00 ugjL 600 115 80-120 Selenium 669 0.200 ugfl. 600 112 00?120 Molybdenum 620 0.500 0911. 600 103 80-120 Vanadium 598 1.00 000 99.? 30-120 Cobalt 52? 0.500 ugl?l. 000 105 80-120 Silver 562 0.250 ugli. 600 93.6 80-120 Lead 644 0.500 uglL 000 Die mutant: of this report and? to the sample?s) analyzed in accordance mm Elie main of (051003: Moment No duplicatbn of this rem: is allowed except in :13 en tire-l}: Page 9 of 13 10? 304 20 Eyed Trusted Serwce Testing Air Water Sell Envirmme?tal L000r0t0005 68551300 30005110342 8001010. 019451 0 T: F: ?0?.361.5689 Wdettaenuimnmtaliabmm WORK ORDER: 1903044 CDC Number: Satanic County Project: Fiue Gas Scrubber 6:25 Texas 5" Suite 5500 :30 Cnib LaPiac . . Fairfeild, CA 94533 Project Control (Continued) Total Metals by EPA 200.? (Continued) Prepared 8: Analyzed: Mar-IB-is Analyte 50?? Result Qua: Remmng Unit Spike REC man RPB Resuit Limit Level REC Limits Limit Batch: 1.960.119 {Continued} Analyst: DU LCS (19(30119-381} Copper 593 0.10 ugfL 500 98.8 80-120 Tha?iilm 68? 1.00 09,0. 000 114 80-120 2311c: 642 0 10 0011. 1500 10? 00'120 LCS Dun (191001193591) Siiver 556 0.250 0911. 600 92.? 80-120 1.00 20 Barium 614 5.00 ugfL 600 102 80-120 0.14? 20 MolydenHm 51? 0.500 ugfL 500 103 80-120 0.420 20 Lead 639 0.500 09,0. 600 106 80-120 0.357 20 Vanadium 594 1.00 ug?. 600 99.0 80-120 0.?22 20 ?ntimany 63"1 0.500 Hg! 600 112 80-120 0.590 20 Zinc 641 0.10 ugJL 000 107 80-120 0.265 20 Copper 586 0.10 uglL 500 97.7 00020 1.05 20 Thailium 723 1.00 ugfL 600 120 530-120 5.14 20 Chromium 591 0.500 ugg?L 500 00.5 30?120 0.658 20 Cadmium 681 0.25 ugj?L 600 114 30-120 0.383 20 Beryliium 691 0.500 ugfL 600 115 80420 14.3 20 Nickei 699 1.00 ugfi. 600 116 80-120 1.01 20 Seienium 662 0.200 ugjL 500 110 80-120 1.14 20 Arsenic 684 2.00 ugfL 600 114 30?120 1.35 20 Cabait . . . 0.500 .. 09:11. __600 .104 . 00-120 0.03798 . _20 . T00 mnfmis? arm: repair 3,5300! to the 5.301pr 00.31sz :10 acmrdance with 30.: chain of custody document. No dup?c?a trim of this name-t 1'5 Mam-d, map: :?rs anthem Page 10 0f 13 Mr Water Sci! I En?renmentalmberata?es 605 Stone Road Ste. 9 -12 Beulah. CA 94510 T: 201242.500? F: .5689 ww?eltaenvirenmenm?a?mm WORK ORDER: 1903044 CDC Number: Sulano county Project: Flue Gas Scrubber 57.5 Texas 5" SURE 550D Colby LaPiace Fairferld, CA 04533 . Pro1ect #:[nonej Quality Control (Continued) Total Metais by EPA 60108 Prepared: Nerds-.19 Anaiyzed: Mar-19-19 Analyte Source Result Quai Reporting Unit Spike RFD RFD Result Limit Lave! R?c Limits Limit Batch: 1.963118 Analyst: DV Blank {19C0118-Btk1) Chromium Ni] 0.25 Copper MB 0.10 Silver ND 0.25 High; Barium ND 2.50 Lead MB 0.50 Cadmium ND 0.25 mgikg Molybdenum ND 0.50 rug/kg Beryllium Ni) 0.25 Nickel ND 1.00 Selenium MB 0.50 Vanadium ND 1.00 mg/kg Arsenic ND 0.50 mgikg Antimony ND 0.25 Thallium ND 0.001 Zinc Ni) 0.10 mg/kg ND 0-50 mm . 1C5 {1960113-351.) Barium 30.? 2.50 30.0 102 80-120 Beryl?um 30.0 0.25 30.0 00.9 80-120 Antimony 34.4 0.25 30.0 115 30?120 Cadmium 33.9 0.25 mg?cg 30.0 113 80?120 Chromium 29.8 0.25 30.0 99.2 80?120 Arsenic 34.3 0.50 30.0 116 00?120 Nickel 34.5 1.00 30.0 115 80?120 Zinc 32.1 0.10 30.0 10? 30-120 Copper 29.6 0.10 30.0 98.8 00-120 Vanadium 29.9 1.00 mgg'kg 30.0 09.5 30?120 Lead 32.2 0.50 mgikg 30.0 10? 80020 Thaliium 34.3 0.001 30.0 114 30-120 Molybdenum 31.0 0.50 30.0 103 80120 ?re con tents arms report 3,0pr to Me sanders; analyzed xi: accordance will (he Chain of rusted)? document. No dapka?bn of mi! rayon is 30mm except in its entirety. Page 11 13 Treated Senate Testing exit Water Soil Labaratar?as 605 Stone Road Ste. 9? ?12 Benicia, CA 94510 T: 7023410001 F: ?0?.361.5?09 mwadaltaen?mnmenta?ahmm WORK ORDER: 1903044 CDC Number: Sofano County Project: Flue Gas Scrubber 6?25 Texas 5., Suite 5500 :fojig?e"ager Com Lama . an CA Farrfedd, 94533 Project #:[none] Quality Control (Continued) Total Metals by EPA 60103 (Continued) Prepared: Mar-1849 Analyzed: Mar-19d?) Analyte 50?? Result Qua! RePf??-mg Unit 59"? map RFD Result leit Level REC Limits Limit Batch: 1909128 (Continued) Analyst: 0V LCS (19(39118-651} Silver 23.0 0.25 30.0 93.4 00?120 Cobalt 31.4 0.50 30.0 105 80?120 33 5 ?3 5D 313.9 1&2 3012?} LCS Dun {19(20118-3591) Zinc 32.0 0.10 30.0 10? 00?120 0.265 20 Thallium 35.? 0.001 30.0 119I 00-120 4.04 20 Silver 27.3 0.25 mgikg 39.0 92.? 30-12:} 0.7?0 20 Antimony 33.6 0.25 30.0 112 80-120 2.41 20 Selenium 33.1 0.50 30.0 110 80?120 1.14 20 Vanadium 29.? 1.00 30.0 99.0 80-120 0.554 20 Nickel 34.9 1.00 mgf'kg 30.0 116 00-120 1.01 20 Barium 30.7 2.50 mg/kg 30.0 102 30-120 0.14? 20 Molybdenum 30.9 0.50 30.0 103 80-120 0.420 20 Beryllium 29.6 0.25 30.0 93.6 80-120 1.34 20 Lead 31.9 0.50 mgj'kg 30.0 105 80120 0.857 20 Cadmium 34.0 0.25 30.0 114 80420 0.383 20 Copper 29.3 0.10 mg/kg 30.0 97.? 80?120 1.05 20 Chromium 29.6 0.25 30.0 90.5 00-120 0.058 20 Cobalt 31.3 0.50 30.0 104 80-120 0.0290 20 hygienic . 34.2 0.50 . _n_1gfkg 30.0 114 . . 80-120 1.35 20 Fine contents of 051's 3pm to the saxmfersj :11 accordance mm dram of msfady document. i No mwramn 0f rm; repor?s airmen: may! in .1: Emmy. Page 12 13013 Trusted Senate Tasting air Water.? 501% Environmeamt Laboratories 685 Stone Road Ste. 9 ~12 Benicia. CA 9451 T: F: rams: .5689 weavxieitaemiro nmealaiiabmm WORK 1933844 Number: Project: Flue Gas Scrubber 90 Member: Project Manager: Colby La Place Project #:[none] Soiano County 675 Texas 5., Suite 5500 Fairfeiid, CA 94533 Notes and De?nitions yam DMion Dry Sampie results reported on a weight basis. ND Anaivte NOT DETECTED at or above the reporting limit. Percent Recovery DF Dilution Factor LCS Lab Control Sample LCSD Lab Control Sampie Duplicate MDL Minimum Detection Limit MRL Minimum Reporting Limit MS Matrix Spike MSG Matrix Spike Dupiicate RPD Reiative Percent Difference Source Sample that was matrix spikeo? or duplicated 3 Results MDL but MRL lire meteor: of this rem-2? appfy to the sampier?sj a?a??zc?di? actombnce ate char}: document 4? Mo eradication cirrus report is aligned, except in its anthem Er; ?Il Page 13 of 13 .- Trusted EEFWEE Testing air Water Soil. Hashim to: - jig/1655'? Eight Name: ~59; Addfess: . :I'ijeui Name: ?u .i if? mg 947131 I - up Analysis-Re ues?ted_ - . Teiephone: KID Va? df~r . $6.933} Fb?k?fiiew De? . ,6 Hpmw? 412? I 5e ?grain aff??af 5393'?! 5.5- ?/1255 pm; mag?ran 74w}: (fag/2 Irma 755 ray/?: an}? 0% ?53 ?dial/53f 7L9 3%?ng Pf ~14 maugawm g0 Hd mummy-u magma IUH LAB NJ Ref 1'1! 3m mo W9 M39- 'Cl'HciJ. Innis Presanrs Eive Cant. Sampie ID in Location Date ?rime Matrix Type QUAKE - .- id?i?i . x313 - . xx. Comments: an dez? ,w $5 aw; (pa-$93) r3: 41% W0- gal/Id? 'K?lr?afc-BUM (:3ij (5t {0 W92 8) if Date x351":- ilaie? 2141'} 3:31;? Data Date Refinquishe?d . 2; bv:x%% Recawed . {j Reiinquished by: Received By: er 44} I Haveall sampkes received been stored on ice? Did any VOA samples received have any head sp a? Were sampies in containers; and packaged properly?? . . - 5 Were samples renamed In good mnditmn? 193,22 {if TYPES: AL Ambe; Liter; AHL *4 500 mi Amber: Pil'li (Plastic): QT Quart {Plastfc}; HG Half Gallon {Plastic}; SJ Sail Jar; B4 402. BT Brass Tube; VOA ??mL OTC Other Type Container Aquenus Waiter. Digested Metals; FE Low A?ueaus Nemdrinking Water, Digested Metais; DW Drinking Waiter; 3L 803E SJudge, So?e! 2 Fraa Product Managementx?sxm?c Template 2:ch 4=Na23203; ?:ZnAce