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LMNOM LMNOM LMNOM LMNOM =(9 LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM 8(A ?(= =(' ?(8 <('= LMNOM @(8 9(; 8(' <(>> 8(8 <(A8 LMNOM 8(' <(9A 8(; @(; <(A> '(< @(@ LMNOM LMNOM LMNOM LMNOM LMNOM =(A =(A <(A8 8(; LMNOM LMNOM 8(A @(@ <(>= LMNOM =(= LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM 8(< ?(8 6C65=8, !56O !"BB%E1#@A'+0"%F%.G=56MH IJ+4?45%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% @1#56C<5=89 @AB4+4?"$A'(" 9)56 =(9 LMNOM ?(< <(98 LMNOM 8(> LMNOM ?(8 8(8 LMNOM LMNOM LMNOM 8(@ 8(' LMNOM 8(8 LMNOM =8 ?(8 LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM LMNOM A(< LMNOM LMNOM ;(A =@ ?(< LMNOM ?= LMNOM A= LMNOM LMNOM IJ*$2B%"$A"+ =1@AB4+4E1]B*4+4?"$A'(" @1#56C<5=1@AB4+4"$A"(" 6C65=1@AB4+4"$A"(" 6C65=1@AB4+4"$A'(" ,X*1D"+%!'$"+%-*'B1$2%3$'(E'+E# .3^%\% ."014('B%3@+""(1(0%^"Z"B# /+"4(566%\ 789%\ :89%\ ;7)9%\% /+"4(56<%\ @1#56C<5=89 6C65=89%\ 6C6C5=8,%\ ,!-3%\ (y SYNERGY ENVIRONMENTAL, LLC FIGURES RID So mpledwg 'nergy .2 U, 5 ID Plotted EXPLANATION Roosevelt Irrigation District Well Monitor Well Existing Canal or Pipeline Existing Canal Open Seg Interstates Water Sample Air Sample Estimated Extent of Impacted Groundwater in WVBA WQARF Site Base on 1st Quarter 2008 Data (T erranext, 2008a) Estimated Extent of Impacted Groundwater in West Central Phoenix WQARF Site Estimated Extent of Impacted Groundwater in Motorola 52nd Street Superfund Site ?5 {it man -. New ?Asian, ?Wu AW Abbreviations WVBA - West Van Buren Area WQARF - Water Qu Assurance Revolv 9 Fund WWTP - Waste Water Treatment Plant RID - Roosevelt Irrigation District AMPLE LOCATIONS Roosevelt Irrigation District West Van Buren Area WQARF Site 0 1,550 3,100 APPROXIMATE SCALE IN FEET Drawing Path. N,\Synergy\RooseveIt Irr\SompIe Locations\Drowing Nome Synergy RID 9271M Sample PIot Date. 09/09/1172 27pm, PIotted bvaineDesign, RID-92 LOCATION SCALE 1 EXPLANATION HP Exis?ng 6ft Chain Link Fence A1 Air Sample RID-114 LOCATION 20? SCALE 1" APPROXIMATE SCALE IN FEET AIR SAMPLE LOCATIONS at RID-92 and RID-114 Roosevelt Irrigation District West Van Buren Area By: LD I Date: 09/09/1 1 Project No. 802.10 10645 N. Tatum Blvd. Suite 200437 . Sumner mm AZ 35m Flgul?e 2 Emmi.? souwms [A9]-[A12] [A20] [A21] [W20] Open Lateral Enclosed Lateral [A14] - Background [W21] Main Canal [A22] FIGURE 3 TCE Results of RID-92 Water System Sampling [W2] Virtual/Actual Fence Line RID-92 [A4] [A2] Receiver Box [A5]-[A8] [W18] [A17] [W19] [W11] RID-113 [A19] [W22] Main Canal [A23] [W3] – [W10] – RID-105 to RID-112 [A13] - Background FIGURE 4 TCE Results of RID-114 Water System Sampling [W1] Virtual/Actual Fence Line RID-114 [A1] [A3] [A16] [A15] [A18] Open Salt Canal (West of 75th and 79th Avenues) Enclosed Salt Canal Manhole Diversion Box Receiver Box Figure 5. Wind Rose Diagram of Average Wind Speed and Dominant Direction, RID-92 Well Site, June 28, 2011 0 315 45 270 90 0% 10% 20% 30% Percent of Total Samples 225 135 180 Degrees Azimuth Average Wind Speed (miles per hour) <=1 >1 - 3 >3 - 5 >5 - 10 >10 Figure 6. Wind Rose Diagram of Maximum Wind Speed and Dominant Direction, RID-92 Well Site, June 28, 2011 0 315 45 270 90 0% 5% 10% 15% 20% 25% Percent of Total Samples 225 135 180 Degrees Azimuth Maximum Wind Speed (miles per hour) <=1 >1 - 3 >3 - 5 >5 - 10 >10 Figure 7. Wind Rose Diagram of Average Wind Speed and Dominant Direction, RID-114 Well Site, June 29, 2011 0 315 45 270 90 0% 20% 40% 60% 80% Percent of Total Samples 225 135 180 Degrees Azimuth Average Wind Speed (miles per hour) <=1 >1 - 3 >3 - 5 >5 - 10 >10 Figure 8. Wind Rose Diagram of Maximum Wind Speed and Dominant Direction, RID-114 Well Site, June 29, 2011 0 315 45 270 90 0% 20% 40% 60% 80% Percent of Total Samples 225 135 180 Degrees Azimuth Maximum Wind Speed (miles per hour) <=1 >1 - 3 >3 - 5 >5 - 10 >10 \1'181920<" -2~ ,,~ /"> ~- ~ EARLY RESPONSE ACTION § 4;.~ > ,. ~ /_"ro ~ 9'J'.. r .- <'0 o '(""(» Q) ~ '\/") 4" /;:. v? tzr.'VA.~),.I' <%. of' N ./ ,:J V> i\.l ,,"') ,. \) -...~ /l;~ r{O <,9 ..91> E' G L _ \,<;:,Cl PUBLIC HEALTH EXPOSURE ASSESSMENT MITIGATION SUMMARY REPORT Volume 2: Appendices Prepared for: Gallagher & Kennedy, P.A. On Behalf of the Roosevelt Irrigation District WESTVAN BUREN AREA WATER QUALITY ASSURANCE REVOLVING FUND SITE September 16, 2011 D . ,rl\ XIX. xf\ sz. ,le fix .IIK (K (y {1k xf\_ .xrk. .xr\ ..elx. ., ((~SYNERGY " ' ENVIRONMENTAL, LLC APPENDIX A COPY OF AIRTECH ENVIRONMENTAL LABORATORIES FINAL ANALYTICAL REPORTS AND FIELD DATA SHEETS Airtech Environmental Laboratories (AEL) - AZ 0740 Date: Client: Company: Address: Andrew J. MacHugh SYNERGY Environmental, LLC 10645 N. Tatum Blvd. Suite 200-437 Phoenix, AZ 85028 July 8,2011 Work Order #: Project Name: Project Number: Received Date: 1106113 RID 802.10 6/28/2011 Dear Client: Airtech Environmental Laboratories received eight (8) samples for analysis. All analyses met laboratory QA/QC with any exceptions addressed in the Case Narrative. If you have any questions or concerns regarding your samples analysis, please contact the laboratory at 480-968-5888 Sincerely, Yu Min Shi ADHS License No. AZ0740 Page 1 of 25 Jil Airtech Environmental Laboratories (AEL) - AZ 0740 Client: Company: Address: Andrew J. MacHugh SYNERGY Environmental, LLC 10645 N. Tatum Blvd. Suite 200-437 Phoenix, AZ 85028 Date: July 8, 2011 Work Order #: Project Name: Project Number: Received Date: 1106113 RID 802.10 6/28/2011 SAMPLE SUMMARY One Hour Sampling Start LAB ID 1106113-02 One Hour Sampling End Gauge Reading (in. Hg) CLIENT 10 METHOD DATE TIME DATE TIME Start Stop A4 TO-15 81M RID-3 6/28/2011 6/28/2011 6/28/2011 6/28/2011 6/28/2011 6/28/2011 6/28/2011 6/28/2011 0836 6/28/2011 6/28/2011 6/28/2011 6/28/2011 6/28/2011 6/28/2011 6/28/2011 6/28/2011 0936 28.1 10.8 0937 28.3 9.5 1106113-03 A9 TO-15 81M RID-3 1106113-04 A10 TO-15 81M RID-3 1106113-05 A11 TO-15 81M RID-3 1106113-06 A12 TO-15 81M RID-3 1106113-09 A21 TO-15 81M RID-3 1106113-10 A22 TO-15 81M RID-3 1106113-11 A14 TO-15 81M RID-3 0837 0838 0839 0840 0836 0835 0835 0938 28.4 9.6 0939 28.3 9.6 0940 28.4 9.6 0936 28.3 11.4 0935 28.2 11.1 0935 28.5 11.5 Page 2 of 25 ~~r~~~~~~~~~~~~~~~~~~~~~~~~~ .--.., ,,.-, ~ /..... i ~ ~, ~ /"-. - ~ ,-( " rc Airtech Environmental Laboratories (AEL) - AZ 0740 Date: Client: Andrew J. MacH ugh Company: SYNERGY Environmental, LLC Address: 10645 N. Tatum Blvd. Suite 200-437 Phoenix, AZ 85028 July 8,2011 Work Order #: Project Name: Project Number: Received Date: 1106113 RID 802.10 6/28/2011 Case Narrative r. All samples and QC associated with your samples met the quality control objectives. Data qualifiers in this report are in accordance with ADEQ Data Qualifiers. ~.' Page 3 of 25 rc Client: Project: Lab Order: Lab ID: Airtech Environmental Laboratories (AEL) - AZ 0740 SYNERGY Environmental, LLC RID 1106113 Sampling Kits QC Cal. Flow Rate before sampled 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Phone: 480-968-5888, Fax: 480-966-1888 Page 4 of 25 ~~~~~~~~~~\r~~~~~~0~~~~ ~ '~'I ~, /-,\ ,1'-"'" r"'. ,~ ,,--...,.) ~ ,~'\ ~ ".-...., ~ ~ ~ /-__, r-', (~ !\ I I ,.- i, '! . ( '! ". ( • ( ,( '. ( " ( \ ( ',( \ ( ,( ,( '( ',( \ ( ) ( / - ) r. ! ( ) ( ) ( ) ( ) ( ) ( ) ( ) ( ) ( \ ( ) ( _. ,/ - '- - , - JC Airtech Environmental Laboratories (AEL) - AZ. 0740 Client: Project: Lab Order: Lab ID: SYNERGY Environmental, LLC RID 1106113 Sampling Kits QC AEL ID# STD Name S-100927-01 """'."....."... ""~"~"""~"""""''' .. ''"'''!'''"... S-100927-02 i Stock "''~''"''"'''" ... "''''.... ".''""~ Vedor SGIOrder# Spectra Gases .. ".. .. ".. .....i"."...".... "."......- ..".. ~ Stock ~ I ~ ..... .. ......"..".. ~ ~ Spectra Gases ) ! '; ( TO-1439 Analytes CONC. 1.0ppmv I ~ 272227 i ) ( ) ( \ : \ . \ ( ) .. Accuracy !'""··.. _..•.. _..•.. _.."...•..·,,··.. _..•.. _..•.. _.."..T-..·..·...··,,....................."......".... _..... _.. _..... _..... _................_..... _.."'...... ..·.. .. ..·..•..".. ..·.. ..·.. .. i \ ( "" Description 272227; H"..... " .. • .... '" TO-1525 Analytes i ~ ~ ~ ~ 1.0ppmv ~ Exp.Date i ,:t5% . . ". -..·. ."""·"". . "'' . .' ' ' . . '''r. . I ,:t5% I , ~r ~ .::. 9/21/2011 . 9/21/2011 ""~'''"''"''~''"''~''" ~''"''''''·~'' ···~~2:?~:i:?~~~i::[~:.::::.::~i?~~::.:~.::I::~:p.~~~~~:~:~~~~::.r·-·-1-37340···I::±?~~~:~~:~:~?~p.~~~~:~::.:l.::·.:T?:·pp.0~_:.:.J :.~~~~:.::.:.L·::.::i.i!~!~?:~:~. A-110623-02 i Working Std i AEL Dilution , "~ . ""~"""-'""~"""'" . "" . ~ . ". ~ . "t . ·'. "·'' . ' · . ". ~ . ". ~ . ". .". ~ . ". . ". ~ . ",{. ". .". ~ . ". ~ . ". ~ . ". "","",". . ~,,, . . ",",, . ",,,,,"",~ A-110630-02 i WorkinglS I AELDilution : '" .. _'" ... ".. ~ .. ".. ~ .. ~ .. "... ".. "... "... "... "~~ .. ~ .. ".. ~ .. "... ".. ""... '''" .. "' .. ",,~ .. ""~ ... ,,~ ..,!.... "'""'" .. ""~ .. ""~ .. ""~ .. ""'""~"""~ .. ""_'" .. ~ .. ".~ A-110630-01 i Working IS I AEL Dilution TO-15 SIM Analytes ! 0.5 ppbv + 5% ! 9/23/2011 ""~ . ""~ . ""~ . ""~ . ~ . ""~ . ""~ . ""~ . ""~ . "' . "..."'",""",,'' ' . ,. ""'"". "'" . "!'""~ . ". ~ . ""'""~ . ". ~ . ". ~ . "..."'". .". .!"'". .". ". .,,:::::'". . "'' . . ". ~ . ". ~,+,~ . " . .". ~. ". .' '". .' '". .". ". .". .' ' . TO-15lS4Compounds ! 50ppbv : ,:t5% : 9/29/2011 . D" .. ~ .. ".. ~"" .. ~ .. "·_ .. ~"" .. ~"" .. "·""'· .. ·"·· ... ~·_,· .. ~"" .. ""'" .. _," ... ".. ~ .. ".. "!," .. ~"" .. ~ .. ".. '" .. ~"" .. ~ .. ".. ~"" .. ~"" ... "",!, .. """""""" .. """"'"""'''''"'''"''"''"'''!,,~''"'''"''~ .. "''~ .. "''~''"''~''"'''"'''' ,TO-15 SIM IS 4 Compounds i 2.5 ppbv i + 5% I 9/29/2011 Phone: 480-968-5888, Fax: 480-966-1888 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Page 50f25 ) .. ',! '\ " .. . rc Airtech Environmental Laboratories (AEL) - AZ 0740 Date: Client: Project: Lab Order: Lab ID: July 8, 2011 SYNERGY Environmental, LLC RID 1106113 LCS/LCSD LCS Result 3 ppbv ugIM Analyses VOLATILE ORGANICS IN AIR LCS %REC LCSD Result ppbv ugIM LCSD %REC 3 T.V. %RPD 1,1-Dichloroethene 0.41 0.49 0.53 Tetrachloroethene 1.62 2.63 82.0 0.50 98.0 3.59 106 0.48 0.51 106 Surr: 4-Bromofluorobenzene 70-130% 1.98 2.58 3.46 Pass/fail LCSD RPD 70-130% 70-130% <25% Date Analyzed ppbv TO 15SIM Trichloroethene LCS 100 96.0 102 1.98 2.69 3.39 Analyst: JJ 19.8 2.1 612912011 612912011 3.8 612912011 96 70-130% 4620 E.Elwood Street, Suite 13, Phoenix p;z. 85040 Phone: 480-968-5888, Fax: 480-966-1888 Page 6 0125 '~,r", ~ I~ ,~ ,.---..., ""----', ,~ ~, ~\ ~ ~ r--", ~, ,~, ,~ : ' r--, /-" .,.---.... ~ .,--..., ,/'. _~ ,r-\ /""", ~, ~ ~i ,~. i'-~' ,~ ,~ ,....--., :~' ( -.... ,~,~,~ '. ( • ( '( '( ,( ',( \ I \ ( '( '( '( ' ( '\ ( '\ ( 'C ' ( ) ( '\ ( '\ ( 1 JC Airtech Environmental Laboratories (AEL) - AZ 0740 Client: Project: Lab Order: LablD: SYNERGY Environmental, LLC RID 1106113 LCS/LCSD ( '\ C) ( "1 ( ) ( '\ I ) ( '\ ( '\ ( '\ ( ') Date: LCS Result Analyses ppbv VOLATILE ORGANICS IN AIR 1.1-0ichloroethene Trichloroethene Tetrachloroethene Surr: 4-Bromofluorohenzene ug/M LCS %REC 3 LCSD Result ppbv ugfM LCSD %REC 3 T.V. %RPD Pass/fail LCSD RPD 70-130% 70-130% <25% July 8, 2011 Date Analyzed ppbv TO 15SIM 0.54 2.14 108 0.57 2.26 114 1.98 0.48 0.45 2.58 3.05 96.0 90.0 0.50 0.46 2.69 3.12 100 92.0 2.69 80 70-130% LCS r, ()' '\ ('. ('\ ., .'\ .",'\' . 3.39 5.4 4.1 2.2 Analyst: JJ 6/30/2011 6/30/2011 6/30/2011 84 70-130% 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Phone: 480-968-5888, Fax: 480-966-1888 Page 7 0125 Airtech Environmental Laboratories (AEL) - AZ 0740 Date: Client: Project: Lab Order: Lab 10: July 8, 2011 SYNERGY Environmental, LLC RID 1106113 Blank Analyses VOLATILE ORGANICS IN AIR 3 ugIM Limit Qual Result TO-15sIM 1,1-Dichloroethene < 0.04 Trichloroethene < 0.04 Tetrachloroethene < 0.04 Surr: 4-Bromofluorobenzene ( ppbv Result Limit 128 DF Date Analyzed Analyst: 0.04 0.04 0.04 0.16 0.21 0.27 < 0.16 < 0.21 < 0.27 70-130 JJ ( ( 5/30/2011 5/30/2011 5/30/2011 %REC ( C ( C ( ( ( ( ( ( ( ( ( ( ( ( ( C ( C ( C ( C ( ( ( c ( 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Phone: 480-968-5888, Fax: 480-966-1888 Page 8 of25 ( ( ( ( Airtech Environmental Laboratories (AEL) - AZ 0740 Date: Client: Project: Lab Order: Lab 10: July 8, 2011 SYNERGY Environmental, LLC RID 1106113 Blank Analyses VOLATILE ORGANICS IN AIR 1.1-Dichloroethene Trichloroethene Tetrachloroethene Surf: 4-Bromofluorobenzene ppbv Result Limit 3 ugIM Limit Qual Result TO·1S SIM < 0.04 < 0.04 < 0.04 BB DF Date Analyzed Analyst: 0.04 < 0.16 0.04 0.04 < 0.21 < 0.27 70·130 0.16 0.21 0.27 6/30/2011 6/30/2011 6/30/2011 %REC 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Phone: 480·968·5888, Fax: 480·966·1888 Page 9 0125 JJ ( ( Airtech Environmental Laboratories (AEL) - AZ. 0740 ( Date: July 8, 2011 "Client: Project: Lab Order: Lab ID: ppbv Analyses VOLATILE ORGANICS IN AIR 1,1-Dichloroethene Result Limit 0.34 2.0 0.04 0.20 Tetrachloroethene 0.77 0.04 SUrr: 4-Bromofluorobenzene 116 ( ( ( U9IM' Result Limit Qual DF TO-15 SIM Trichloroethene ( Client Sample ID: A4 Project Number: 802.10 Collection: 6/28/2011 Matrix: Ambient Air SYNERGY Environmental, LLC RID 1106113 02 70-130 Date Analyzed Analyst: 1.35 0.16 10.7 5.22 1.07 0.27 JJ ( 6/29/2011 5 6/30/2011 6/29/2011 %REC ( C ( C ( C ( ( ( ( \. ( ( ( ( C ( ( ( ( ( ( C C ( C ( C C ( 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Phone: 480-968-5888, Fax: 480-966-1888 Page 10 of 25 ( ( ( ( Airtech Environmental Laboratories (AEL) - AZ 0740 Date: Client: Project: Lab Order: Lab 10: SYNERGY Environmenlal, LLC RID Client Sample 10: A9 Project Number: 802.10 6/28/2011 Collection: Matrix: Ambient Air 1106113 03 Analyses VOLATILE ORGANICS IN AIR 1,1-Dichloroethene Trichloroethene Tetrachloroethene Surr. 4-Bromofluorobenzene ppbv Limit Result ugIM3 Result Limit Qual TO·1581M 0.13 1.03 0.29 108 July 8, 2011 0.04 70·130 Date Analyzed Analyst: 0.51 5.53 1.97 0.04 0.04 OF 0.16 0.21 0.27 6/29/2011 6/29/2011 6/29/2011 %REC c r L· c 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Phone: 480·968·5888, Fax: 480·966·1888 Page 110125 JJ \ ( ( Airtech Environmental Laboratories (AEL) - AZ 0740 Date: Client: Project: Lab Order: Lab ID: 1106113 04 ugIM3 ppbv VOLATILE ORGANICS IN AIR Result Limit 0.29 1.7 0.04 0.20 Tetrachloroethene 0.63 0.04 1,1-Dichloroethene Surf: 4-Bromofluorobenzene Result Limit Qual ( DF 110 70·130 Date Analyzed Analyst: TO-15 SIM Trichloroethene C Client Sample ID: A10 Project Number: 802.10 Collection: 6/28/2011 Matrix: Ambient Air SYNERGY Environmental, LLC RID Analyses ( ( July 8, 2011 1.15 0.16 9.13 4.27 1.07 0.27 6/29/2011 5 6/30/2011 1 6/29/2011 %REC JJ ( C ( ( ( C ( ( ( ( ( C ( ( ( ( o c c ( r ( c ( c ( ( ( C ( C (' o 4620 E.Elwood Street, Suile 13, Phoenix AZ 85040 Phone: 480·968-5888, Fax: 480-966-1888 Page 12 of 25 ( ( ( c Airtech Environmental Laboratories (AEL) - AZ. 0740 Date: Client: Project: Lab Order: Lab 10: SYNERGY Environmental, LLC RID Client Sample 10: A11 Project Number: 802.10 6/28/2011 Collection: Matrix: Ambient Air 1106113 05 ugIM ppbv Analyses VOLATILE ORGANICS IN AIR Result July 8,2011 Limit Result 3 Limit Qual TO-1S SIM OF Date Analyzed Analyst: 1,1-Dichloroethene 0.18 0.04 0.71 0.16 612912011 Trichloroethene 1.45 0.04 7.79 0.21 612912011 Tetrachloroethene 0.39 0.04 2.64 0.27 612912011 Surr: 4-Bromofluorobenzene 108 70-130 %REC ,. ,- Phone: 480-968-5888, Fax: 480-966-1888 4620 E.Elwood Street, Suite 13, Phoenix AZ. 85040 Page 13 of 25 JJ ( ( Airtech Environmental Laboratories (AEL) - AZ 0740 ( Date: Client: Project: Lab Order: Lab 10: 1106113 06 VOLATILE ORGANICS IN AIR 1,1-Dichloroethene Result ppbv Limit Trichloroethene 0.04 0.04 Tetrachloroethene 0.12 0.04 Surf: 4-Bromofluorobenzene Result uglM' Limit Qual 106 0.20 1.88 0.81 70-130 OF ( C ( c Date Analyzed Analyst: TO-15 SIM 0.05 0.35 ( Client Sample 10: A12 Project Number: 802.10 6/28/2011 Collection: Matrix: Ambient Air SYNERGY Environmental, LLC RID Analyses July 8, 2011 JJ e 0.16 6/29/2011 ( 0.21 0.27 6/29/2011 ( 6/29/2011 %REC C ( C ( I. e ( ( ( ( ( ( ( ( ( C ( ( ( ( ,. ( C l ( ( C C 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Phone: 480-968-5888, Fax: 480-966-1888 Page 14 of 25 ( ( ( ( Airtech Environmental Laboratories (AEL) - AZ 0740 Date: Client: Project: Lab Order: LablD: Client Sample ID: A21 Project Number: 802.10 Collection: 6/28/2011 Matrix: Ambient Air SYNERGY Environmental, LLC RID 1106113 09 Analyses VOLATILE ORGANICS IN AIR 1,1-Dichloroethene Trichloroethene Tetrachloroethene Surr. 4-Bromofluorobenzene ppbv Result Limit uglM Result J Limit Qual DF Date Analyzed 1 6/29/2011 5 6/30/2011 TO-15 SIM 0.24 2.2 0.57 86 0.04 0.20 0.04 70-130 Analyst: 0.95 11.8 0.16 1.07 3.86 0.27 6/29/2011 %REC 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 ~. July 8, 2011 Phone: 480-968-5888, Fax: 480-966-1888 Page 15 of 25 JJ ( ( Airtech Environmental Laboratories (AEL) - AZ 0740 ( ( Date: Client: Project: Lab Order: Lab 10: RID 1106113 10 ppbv Result 13 37 0.80 0.80 Tetrachloroethene 4.6 0.80 1,1-Dichloroethene Surr: 4-Bromofluorobenzene U91M Limit Trichloroethene 120 ( Result Limit Qual ( OF Date Analyzed Analyst: 3.17 4.30 5.42 51.5 199 31.2 70-130 C 3 TO·15SIM VOLATILE ORGANICS IN AIR ( Client Sample 10: A22 Project Number: 802.10 Collection: 6/28/2011 Matrix: Ambient Air SYNERGY Environmental, LLC Analyses July 8, 2011 JJ ( ( 20 6/30/2011 ( 20 20 6/30/2011 C C 6/30/2011 %REC ( C ( ( ( ( ( ( C ( ( C ( ( C C C C ( ( C 4620 E.Elwood Sireel, Suile 13, Phoenix AZ. 85040 Phone: 480-968-5888, Fax: 480·966·1888 Page 16 of 25 C C ( \- ( Airtech Environmental Laboratories (AEL) " AZ 0740 Date: Client: Project: Lab Order: Lab 10: Client Sample ID: A14 802.10 Project Number: Collection: 6/28/2011 Matrix: Ambient Air SYNERGY Environmental, LLC RID 1106113 11 ppbv Analyses VOLATILE ORGANICS IN AIR uglNe Limit Result Limit Qual DF Date Analyzed Analyst: TO-15SIM 1,1-Dichloroethene < 0.04 0.04 < 0.16 0.16 6/3012011 Trichloroethene < 0.04 < 0.04 0.04 0.04 < 0.21 0.21 6/30/2011 0.27 0.27 6/3012011 Tetrachloroethene Surr: 4-Bromofluorobenzene ~ Result July 8, 2011 104 < 70-130 %REC . .... _-' , . 4620 E.Elwood Street, Suite 13, Phoenix {l;Z 85040 Phone: 480-968-5888, Fax: 480-966-1888 Page 17 of 25 JJ "' ( Airtech Environmental Laboratories (AEL) - AZ 0740 .. ( ( ( Canister Cleaning Certificate Canister size: 1.oLD 6.0LE] Other: Serial Number: _-"14"'7..=2_ _ _ __ ( ( ( AEL Canister Clean Batch#: .-.:1...:.1"'06::..-.::.04-'-_ _ _ _ _ __ Comments: Analytical Method: ( ( ( T015 SIM ( ( Comments: This canister has been cleaned and has been individually analyzed to certify the analytes in the box are below the Report Limits. ( c ( ( Report Limits Analyte ppbV! 1,1-Dichloroethene i < Tetrachloroethene ."""'''''".""....... "......... " .. " ..... " .... "."''',, .... ,, .......... 0.04 ! ugIM ! 3 tody QA-Form S8-Rev.02-0810 Page 1 of2 '\ ~ 1 ' rc ~'.'~! nofCustody Airtech ERvixonmentalLaborijtories (AEL) 4620 E.Elwoo,~LStr,eet. Suite 13, Phoenix, AZ ,85040 480~968~58~8 (Ilhone)' 480~966~1888 (fax) Results: Hours ICustody;seals Intact: Yes___ "0_ __ of Contaloers:_~_ __ ,___ Standard 10Worklng Days indoor air . soil extraction vapor other 'Speclai Requ'irernents; ,~~~--~~~~~--.-~--. Page 2 of 2 ~~~0~0n~rnrnr~rn~r~n~n~n~n~nrnrn~nn~~~~~~r ~ ,-- ·, '\ Ainech Environmental laboratories, llC Ambient Air Sampling Plan (MSP) #: A2 Sampling Co. Date: CItion Location: .cR"ID"."A2"--_ _ _ _ _ _ _ _ _ _ _ _ __ Client's 10: HeadSpa'ce...RIDMQ2 Receive Box CAa) . . .Olher: _ _ _ _- _ _ __ Address: Describe the site location: - Sampling Train 1.0. L Canister: 0 6.0. L D Silanized: 0 D Grab l?amp_ler; On~ inin Two niln One, min = TakinQ one m'inule to fill one Utercanister; Time integrated Sampler ~Sampling duration: Five min One hour -0 24hour Sampling start: Date: 612812011 Time: () Sampling . End: Dale: 612812011 Time: Any tubing used on the sampling train? Tygori [K] Tubing type: TeflonO 4hourO Other: 23 S ~ PVC Weather Gauge read: If yes, fill the infomlatidn below: o Other. ---.,._ _--'-_ _ __ inch Length: Wind: coD FO [ ] Mild Sunshine Strong At the sampling point: Upwind D D ID 0.125 inch v[K] NO Cloudy D DownWind ~ If Yes, fill in the blanks blow: D Comments: Field Duplicate V 0 N Describe the duplicate sample site position and fill separate AASP Form: Sampling site Inspection Note: 4620 E. Elwood Str'eet, Suite 13, Phoenix, AZ '8504:0 • Phone:4S0 968-5888 • Fax: 480 966-1S8S·. ysru@azairlab.coin ,S" Hf"ge 1 f~j'~ M M q' ~ til ~ - D _____ ~ inch, Hg ~ inch. Hg ~~~S~~v4\\..L.~~J Tern 12 hour _~_--,=--.,, Are all parts of Sampling Train le'sled in the lab before samp'ling? Comments: 8 hourD Gauge reael: t29 -;] 'i NOD' Yes Vin~ 0 Tubing used from the s~mpling point to canister: ~ oNO .Rain 0 ( ( ( ( ( ( ·.irlec,~ El1Viriinmenlal[aboraI9rl,~"LLC Ambient Air Sampling Plan (A!I;SP) C #: A4 Sampling Co. ri.t~:, , 6128!20{f: >~> GomPany Name,:, ,,',-,'S",Yh",<~,"'gux",IPJ""rte,,':;ch'-..,.,,-----sa'mpler's ' ~al)J~: ~A"'n.::;dr""ew:.:;f'{",:;(I"M"jn'-'~'-"""'_--,\;Q:I\l\ulting Fil1Jl( , Cpmpany Name: ~s~yn",eeJrg"ycf""_'=:o---;-'-_----;,-___ Project Nar:Q,e:, ."R",ID",-'-o,--;-~-~---- P'roje.clM,aijager. ~ y~ Project Nu:ril,~~(: ,:-~~~ \0 - Sampling Site's Information ., ( ( C ( ( ( C ( C Samplingtrarri ' Canister: ,', 1.0 L Si:lmetei: D 6.0 L []] Silanized: 0' _ D Grab One:min Two,JninOne min,:;(taking_one mipute.to fill one liter-carii~fer; Time Five :min N[J [J' Other: _ _ _~_ _'--;-,"" JiJ~~~;_~_t~d--S~~pjer-~SainPHng dUiati9!J::>: ,'One_ hour ~l -4hourD- sa!Jl~in~ start: 24_-~6~r:_-_ Gfl~:- Date: 61281201,1 s.a~Pclj'ng End:" Date: 612~/iot1" , An,y"t9bing, j.lsed on the sarnpiin~ TubinQ)YJ~e:< ' 'Time:' Time: t~in}t,; \, ", N'~, Tefl9,i;i:[1 TY9,onD D Vinyl PVC TUbing:b:~'¢d from tl)l?,~ai'fip!j~g POilJrio'6~'ni~fer: Length: Are,alVlfaJts of SC[lml?I'i~~:Trajl) t?s~:~Un the lab'before sainpling? \'V)\ Comments: Weather Tempera Wind: ' Gauge read~i- / 'Pets /; D 8 haurO 12_hour Other: _-,-_--,:-,:-_ _ 4:&ti; Yes -;< G~uge'read: I tJ If yes, fill the inf'!rmatlon D Other: +'-;---'-_~~ in,n, Hg .5 in~h, pe1ow,: Hg +>, ~~~",,""~"'-.,~-'-_ U),'":,, inch -"1'< ~1 'In6'h' yOSJ---;:;-[J >', " ' ...,.,~;!!'~-:-':"-';--~---~~---""7---,:-,---"",""--,-j'-'=:::--T~-~, 8\§~::,~'W~€:\2: S~~:'N\\L ~ US~J \ FI) X CO D Sunshme D Clo"udy DRain D Mild D ' ,~'lidd[e At the .sampling point: - ro D Upwind ' Dow~wind D Comffi'en~:/_ --'-.,.---,----,--T-,-----,--,.;-"-~--,----~-,------=-_==:::. Field Duplicate,,! 0 N It Yes, filJ in the bl--o ,~.I ~ ( ( C ( ( ( ( ( , , ,r , Ainech Envjronmental Laboratories, ltC Ambient Air Sampling Plan (AASP) #: A9 Sampling Co. 612812011 Oat.: Cqmpahy Name: ~S""yn",e'"tg"y",/PJ",'rt",e,,,ch,--_ _ _ _ _ Sampler's Name: .c.A",n",dr-'Cew",lY.!.u,,-'"'M"'irl_ _ _ _ _ _ __ Consulting Firm: Cdmpcmy Na'me: ~S":Yh=e'"rg"y_ _~~_ _--,;-_ _ Project Name: ~ ~sol. Project Manager: "'R"'[D'-_ _ _~_ _ __ Project Number: Sampling Site's Information Location: R[D.A9 Clien!'s [0: BZ R[D·92 Fence ,L'ie -~ (~- Descnoe the site location: (; c Sampling Train CalJf~ter: 1.0 L o 6.0 L 0 IZI D 6/28/2011 One hour Sampling End: Date: 6/2812011 Time: Any tubing used on the s'anipling train? Tubing type: Tygon D Tef[qn _ D ~ Vinyl 4 hourD D D PVC Weather inch,Hg 1r 5 inch, Hg Gauge read_: 0 Other, _ _ _ _ _ _ _ __ Length: inch [0 inch ylZI :l ' CCrol\ ~ ~~ 'NIL\.- B,~~) IKJ O Mild D At the sampling point: CO 0 Sunshine 0 Cloudy 0 Middle' Upwind 0 DownwindD Comments: Field Duplicate Y O N § " [IYes, fill in the blanks blow: Describe, th'e duplicate sample site position and fill separate AASP Forni: 4620 E. Elwood Street, Suite 13, Phoeirlx; AZ 85040 • Phone:480-968-5888 * Fax: 480-966-1888 * yshi@azairlab.com Q. C'l Page30Jll ,., 7 ," /"8".7 ~ 10,r -:=::-- ~'''7 Il.~ ~ D If yes, fill the infonnation below: ' F Wind: 12/:lour Gaugeread:2.3.~ , Me all parts of Sampling Train tested in the lab before sampling? Comments: 8 hourD Other. _ _ _-,:_ _- '_ _ __ ~ Time: ~(~ 9NO~ Ye-s D Tubing used from the sampling poinUo canister: " Other. _ _ _ _ _ _ _ __ Five min 24 hour Sampling start: Date; C~Oe:n+ ylZI Silanized: Grab ,Sampler: One'min Two min One f!1in = Taking one minute to'fill oiie liter canister. Tfm'e IIlte~rateci Sam~l,er l&JsamPling duration: 0 _~ ....O.:.."2.=,,",I.>Q",,-_~___ Rain 0 ~ ( ( ( ( ( ~.. Ainech ERvironmentallaboratories, uc AtnbientAirSampling Plan (AASP) ( ( #: A10 ( 6128/2011 Date: C CompahY Nan:'le: ~S,,-y",ne,"~rgay"-/A"'irt"'e"'ch'--_ _-'-'~_ Sampler's Name: ~A"'n"'dr."ew"'NC!.·"'u:"'M"'in'-·.c.::..c..._ _, -_ _ ( . CClnsultingFirm: Company Naljler:-< :.~,t",y",ne",rg"y~~_ _ _ _-,_"-~~ Project Name: 8[0 prOjectManagef:.•;'§~~.J ~1l:Q',"~,,"~'''i''tc!\'@1!'\=:'''''----- Sampling .' Location: A.adress: Project Number: Sit~i~~i,forITIation .\.::~:;:; .... ~R!!:ID~·A~1~O.,-,.. _~_ _ _~c...,.~_~~ , Describe the ] '~~~~~~4--.'§§T .•.•. 6.gL@ 1.0LO D ( Sampling ~~ta:rt: Date: 6/2"812011 Time: Date: 612812011 Time: TygOn'O 0 8hourD 0 Vinyl D PVC Gauge read: q, b 0 Other. inch Are all parts of Sampling Train tested:in'tlie lab before sampling? y 10 ' inch 0~Cr C ( ( ( ( ( C Comments: ( Weather, . '. . 0 F' IKJ ·'C O ' o Middle At.the sampti(l9 point: Sunshine D Cloudy 0 D rang Upwind 0 DG1l11cate. yO N Rain'D r ( Downwind Comments:,,' ,:, Field inCh'; H~' If yes, fill the information below: , -Tubing u!>ed from th,e sampling point t~ canister: Mitd 12hour 0 .~ Nog Yes Teflon l&] '4'hOUrO OlheJ-: ~+----_--'.fic7lt ~ Gauge r~ad: ;;ll. <....f inch, Hg > 24 nour Any tubing used on the ~a'mpl[h'g'train? C Five min One hout Wind: C ( S[lanized: Grab 'S~inpler: One min [J TWO)nl~ One:'mi,~'::= Taking one minute to fill one liter canister. Tem ( C Sampling Trai11. Tubing type: ( ( site I,Qcation: SampJiri;~{End: ( If Yes, flll in the blanks blow: ( ( Describ~'ihe dUPlicai~ sample site P9sition and ffn separafe'AASP Form: ( Sampling site Inspection Note: C '. ",. " ( 4620 E. Elwood'~freet, Suite 13, Phdel)ix, AZ 85040 ( . Phone:480-968-5888 .,'Fax:A8.0.,~9.J)6-1888 • ySh.i@azairlab.lXlffi Page4.qf11 , ./0 0'" 'L,W . . 9' • . . oQ ,~,r ~ ~'I6" iJ: /'tj) .2.'.:1 -::? ~ ( C ( C C ( ( ( ( r~ r c ,r~~ Airtech Environmentallaboratpries, LtC , Ambient Air Sampling Plan (AASP) r~ #:A11 SamPling Co. ,~ c Date: "- 6/2'8/2011 r Company Name: ..=S"'yn"e"'rgu.y/:!.Ai::.·rte=ch'-_ _ _ _ _ Sampler's Name: ~A",n",dr"ew",N.:..::.u"'M"'in'-_ _ _ _ _ __ "- Consulting Firni: r~ c;:o~pany N.ame: ~~. ,~ Project Nam-e: RID Project Manager: ...:j.J;}-& ..._...,'=-_~"""...tJ;~~'""¢'--__ prOject Number: r~ "- r 1·C(2. • \ \) Sampling Site's Information Location: "R"'ID"',A"l"l'-_ _ _ _' -_ _ _ _ _ _ __ r~ '- Address: r Describe the site location: ,~ r~ '- "'-, Sampling Train Canister: c' ,-,' 1.0 L Grab Sampler: r '-j c', ,-, D 6.0 L One rnin D 0 Silanized: Two min. 0 Five min oNO Dther. _ _ _ _ _ _ __ One min = Taking one minute to fill orle liter canister. Time Integrated sampler~Sampling duration: r '-, One hour ~ 24 hour 0 r-, Sampling start: Date: 612812011 Time: '-, SamplingEnd: Date: 612812011 Time: "'- -Anylubing used on the sampling traIn? r'-- Tubing type: Tygon 0 Teflon t2'$29 IJ 13 '7 N~ 0 Yes 0 Vlnyl D r '- Are all parts of Sampling Train tested in the iab before sampling? Gauge read: o "-J r' '-- Weather , ,~ '- ,-- . ,~ i ;;{/'< FO IKJ Wind: Middle At the sampling point: Upwind CO 0 Sunshine inch, Hg Other. ~_~_ _ _ __ 10 inch C\N~~~~ ~\'JILLj£ u,~~) Temper D y0No r~ Comments: 12 hour Other. '----c_..."..-----Gauge read:;21.::S inch. Hg _ _ inch Length: 8hourD If yes, fill the information ,below: PVC Tubing us~d fro'm the' sampling point to canister: 4hourD D Cloudy DRain 0 D D Downwind Comments: Field Duplicate ~ yO [fYes, fill in the blanks blow: Describe the duplicate sample site position and fill separate AASP Form: ~, ~, Sampling site Inspection Note: '-~ JI~I.' .. . 'I? ___ =I?b.[ I~ ~ oJ"iS\'\)c:; \N~Of ~~~-r '- 4620 E. Elwood Street, Suile 13, Phoenix, AZ 85040 • Phone:480-968-S888 • Fax: 480-966-1888 • yshi@azairlab.com '- f.5° 0.'. <.0'\ 0'>1 9: ' 1 1"~ 11·2:- IS} --=- Page50f11 =- 'J!L1 IZ. ~ -:;::?" .j ! ( ( C ( I[]' . C Ai!Jpch EnVirOIfn1elnallaboratorieS,LLC ..•... . Ambient Air Sampling Plan (MSP) Sampling cdt, ( #: A12 (, ( 6128/2011 Date: ',Gqrnpany Name: "s",yn",e~iJJlL'yJ~'A"frt"'e"'ch'-_ _ _ _ _ Sampler's Name:, :..An=dr",ew",N=u",M",io,--,,~_..,-'_ _ __ , , con~uJting Firm: . C e~mpanyt,iame: -,;S;!:yn~ei;lrg~Y~,,","=::-"-~'-,-_-p_ _ _ PrOject Name: ~R'7ID",""_ _-c:--;-_ _ __ ( Project Manager:. C ;0&Y:~Shr j", " Project Numoer: . ~2 "Q' , ( Sampling Site's Informa.li?n • Lo~tion: ~R~ID~'~A1~2~_~~~_ _ _ _ _ _ _ __ C Address: ~_ _,--''-'-'-'-'-'---,~_ _ _ _ _ _ __ Describe the site location:','" ~_ _",.,-_ _ _ _ _ _ _ _ _ _~-+_ _ _ _ _ _ _ __ ( C ( Sampling Train Canistef::' 1'.O'l.':tJ 6.0L@ NO Silanized: 0 D Grab S~D1RI_e,~:' :~;~' One min Two min' One mlh','=: Taking'one minuteJo fill one liter canister. Tim~j~~hra!~~;~~~PI:( ~sampl~n9 duration: . Sa.~pling.start: Ohe hour ~_ 24 hour 0 Date: 612812011 . T!rne: ,SamplIng End: Date; 612812011 'Tltn'e: Ariytubi~,g used on the samplin'g, train? 'Tubing tYpe: Tygon D TIi)fl9n Five min Vinyl 0 PVC ~iriCh,Hg' GaUgeread:- ~inChiH9 If yes, fill the infqrmation bel,ow: D Are, atrparts qf ,SaniplingJ:-rajn f~sted',ii:1 the lab before-sampling? \iVe.ather ,+~mperat~te'; Wind: 'CJ 12 h!Jut Gauge read: Length: Comments: 8hourD _ __ other. --~-:::=:'7:;'>-,-'-""-"7--'-- ~ tJ Other: _ _ _ _- '4,hourD tfJ"JYO ,N~ Yes 0 o other: ·inch 10 ,_.__ in~~ Y@NO L\J~'I'l\U_+~~) • - ."'",, 'Fe [ ] CoD Sunshine D Cloudy D ~ain 0 Middle D Strong 0 ' C ( ( ( ( ( ( C ( ( ( ( C ( Field Duplicale Y!3TI N If Yes, fill in fhe blanks,~~: ( ( ( u.. ~ :, ,'tU?20 E. ElwoodBtreet, Suite 13, Phoenix, AZ 85040: • PfiQiie:480~968-5888. Fax:480-966-1888. yshi@azairlab.c6Jti \ '8':£-.:.---' .'~ . . ' . "" If 0 ", ""0 .. pa ge6of11 .. ~.---.., I: 0 " ~'VI) -1' ~ V v'" 1/11: I:S-,~ ('.1r ~ ;:--::? .-:;:::::. o. C C ( C C ( ( ( ( , (" t - ,. Ainech EIIVironmentallaboratOJieSiUC c c (" ",.- Ambient Air Sampling Plan '(AAS~k' 1 '.~ Sampling Co. '-_I r- Date: _--,6",/2",8,,/2:.:;·0.:..11,-~ ';., Company Name: ",S:z.yn",e,,·r9"'y"'/Ai.!!.rt"e"'c"'h_ _ _ _ _--Sampler's Name:),~A"'n"'dr"'~"'~'_'fY"'~'_'M"'i"h_ _~_"_''"''~··+~,-~o_',l-0j~ Consulting Firm: ,.j Company Name: .!!S:Ly"'ne"rg"'y'-_ _ _ _ _ _ _ _~_Project Nali1~. ",:,R",IO"",---.,....-,,,,"-c..-c-'-c-'-"j, ",' Project Num~.~5- ..-:,-;,_;~___".,-'_'_-,::-_'_<_ _ Project Manager. Sampling Site's Information L . '.,' • Location: .'-R"'ID'--'_'A2o:0'--_--_ _------~-­ Address: Describe the site location: Sampling Train c Canister: 1.0 L 11] 6.0 L D N Silanized: D -0 Grab Sampler: One rriin Two min One min = Taking one minute to fill one liter canister, Time'lntegrated Sampler I!Jsampling duration: Five min One hour [ ] 24 hour '-.. r· L ( .. 0 fJ,.r; J o -.;,Oth~r: 4 hOU~O. _ _ _ _-.,-~,,--',: '5 /' '0625 G'auge read: Sampling End: Date: 6128/2011 TIme: 0335 Gauge read: Tygcin~ Tubing type: Teflon 0 Vinyl Tubing used frb'm the sampling point to canister: 0 PVC D -=----=-__~__ Time: Yes:RI \':,., Other: _ _ _ _ 6128/2011 NoD ( :8 hourO \:.12 h?ur Sampling start: ,Date: Any tubing used on the sampling traJn? "-, '2R:>.?- inch, Hg ~inch' Hg If yes, fill the inform<;l.tion below: o Length: Other: _ _~_ _ _ __ inch ID yl1] Are all parts of Sampling Train tested in the lab'before sampling? inch NO Comments: L~ ~"" v-J~'€e '5~~ '4'I\\.\..-~",ut;;~) Weather rature: ," ',' Wind: F' [U C' Mild 0 Sunshine Strong At the sampling point: Upwind 0 0 0 Cloudy 0 Rain " '\ 0 . Downwl Comments: Field Duplicate Y 0 NO If Yes, fill in the blanks blow: Des ibe the duplicate sample site position and fill separate AASP Form: --n-n--s. "i-s. =\.A L-~ ~ Sampling site Inspection Note: . . .l II • ~ (;:ee ~\2l-o\ ~ ~) SI<\-\. _ f-I2.Ot-A, 'VJhBz-f.N~ "\V \~~ 4620 E. Elwood Street, Suite 13, -Phoenix:, AZ 85040 "Phone:480-968-5888" Fax: 480-966-\888" ysbi@azairlab.com Page 1 of 1 . ~ ( c ( ( Aidech E~v"q.~'Qkll,lboraIOrie~~ '~~~"" \ c AmBient Ail':Sarnplihg RJa,n,(M~e)} :., Sampling Co. c·~ . ~_ Company Name: #: Dup .. ' 1)JpJt~ C Z:' Date: _----'6"'/2"'8/"'20"'1"-1 ~s",y:.:;ne"rg",Y;:./Al",rt""e",ch"-_~_ _ _ Samplers Name: :. A",~a: :~: .'w",IY.-":lr""M",',,,(h_'_ _-',---"-'-'---"--,- Consulting I'irm( , . j Company Nam~i ,.;;S"-Ynfi;~e,,·rg,,,Y_ _ _ _ _ _ _ _ _ _ _ Project NameS' ,.!!f'J~D",:",","'"._ _ _ _-.,.--,-,--Project Mana~~f:; Proje~t NW:nb¢f .,.._.''-,':_~--''-'~~"_·.::..,:_'_ 4_ .... SamplingSilli's I n f o r m a t i o n G i_V::; , . , :, RIO-A~O Rld-I')U~ 6 - 2 8 - 2 0 1 1 C l i e n f s II;>: 1:M\1\C~~, 'G.~ Location: Address: ~ Describe the pite lo~,~~q~:-- ~ 'Z?) "";"-" j (,' :./f I " -, -- .... "r W ','l,pG Gral?_s,aI,i:lPJ~r::; -, 6.0L 0 Silanized: [j Two-jn~f1; One min tJ QneJnin:"~~':1~_k_j_ng-ooe minute to Jill one lite~;c~ni~ter Timelri!~d_~-ted Sampler ~sampling duratiqn: " N J]ve min 0: One hour ' 25 ~Y, t,,~Qing ~,P,Ii" ~ t(ain? A", used" on, I,hes, Tubing type: 'T¥g~n'" Teflon 0 NoO Vinyl ,TUbi~g used from the sampJJr;g,point to canister: DO YW Yes 0 ~ther: 'c''-' c . . '_ _ '-<,~- : "",",=~",,-_'_',- ,'~:;\\i{-t ":/ ~':- 4 hourD] . \8-~o\Jr[~Fj>.,~~(n~M! ,,: 0 Other;'- " , '~,', ,'" "Ga~ge r~ad:l 'Z£>,Q2d~1'Hg) W0 Gauge If yes, Length: read:\.0~;~\;~hi Hg fillth~ infOr,mati,'on be,Ipw: PVC Other: _ _- - _ - - inch Are all parts of Sampling T(~in' tested Ln the'la!; before sampling? - - Y ID, inc* EKl~0 'Tempe Wind: , ;GiJd'~r At the_S?I]:lRjin~:p_oin-~ F'II] c'O SunShine 0 Cloudy 0 Rain D DQwnwind Y W N 0 If Yes, fillJnthe blanks, blow: "" ( ( ( c ( ( ( ( ( Describe thE!\duplicate s~mple site position'and fill sep~~'~~,MSP Form:-" _ _------~--_ Sampling site Inspection Note: ( ( Comments: Field Duplicate c ( c c 0 Middle Upwind ( ( ,~' ~ ~~W.;;~~ ~\~~ IJS'C'D) " ( c Comments: Weather ( ( ( ,_ce' ~" c ( ( Sampling,.TrainJ Canister: c c ( ' ,vl \1 " c : fioM '-N'~ W~ 4620 E. Elwood Street, Suite l3, Phoenix, AZ 85040' .- Phone:480-968~5888 - Fax: 480-966-1888 _ yshi@azairlab.com , " ,Page1 of1 c c "\'0 IN\EL. ( c ( c ( c ( ( ( Airtech Environmentallaboratories~ UC Ambient Air Sampling Plan (AAs'i'>F' . #:p.21 Sampling Co. Date: 612812011 ., ., Comp~ny Name: _._~-SY=ne"rg"y",IA"i"rte:::c",h,-_ _ _~__ Sampler's Name;'\Ai1ir;wNu Min \ Consulting·Eirm: C9mpany NafTIe: , ~S,"y"ne"r"gy,-___________ Pr6ject.Na~me: ':c ;~' ).:....:"8".ID"--_ _~_~_ _ __ Project Number:' _,_.,_.___'_'_-'-'~_ _ __ Project Manager: Sampling Si'ie's Information -, '''' ; ':\ .\ ">, r- ._- o ' "• • Location: .!.R,"ID",-:ck2",-1,-_ _~_ _ _ _ _ _ _ _ _ __ Address: '--,-.\ Describe the site location: .::~~" Sampling Train 1.olD Canister: 6.0 L [8] D TIme'lntegrated N[],; Silanized: D Grab Sam'pler: 0':l~ min Two ,i'liin One min = Taking one minute to fiJi one titer canister. sampier~sampli~g duration: Five min D OO~ Sampling End: Date: 612812011 Time: . ()"\ D Teflon 0 '3lo N~ Yes D Vinyl D PVC Tubing used from the sampling point to. canister: , ,,~.,(~ ( 24 hour Time: Tygon 'ot~Jr: _ _~'_'.:_"~~',,-l'~_·_C-,--,-'\_ _ __ ,', \ .. ~ 4,~;ourD·· 612812011 Any tubing used 6n the sampling train? D One hour Sampling start: Date: Tubing type: Cu.; ,. -",. 8 hou~E3! 12'hour < Other:~-;- ' ' i ,.,,', f ~''" '? D ~~~~~~~-- '/.~Ga.,'u?~- read: ~!n?h'. Hg j Gaug~ read:'~ i~ch, Hg If yes, fill the information, below: o Length: Are all parts of Sampling Train tested in the lab before sampling? Other; ~_~_ _ _ __ inch ID _ _ inch y[Kj NO Comments: L~ ~ IN~ S~'C::N. i\1l\.. 'OB ~) Teniperatur . FO [ ] CO D Sunshine D Cloudy' 0 Rain 0 Weather Wind: Mi,d 0 At the sa'f!lpHng point: Strong D [DJ~~D~ow~n~W~i;nd;[1---______ Upwind Comments: Field Duplicate yO Describe'the duplicate sample N ~ite [fYes, fill in the blanks blow; position and fill separate AA~P Form: Sampling site Inspection Note: 4620 E. Elwood Street; Suite 13, Phoenix, AZ 85040 • Phone:480-968-5888 • Fax: '480-966-1888 • yshi@azairlab:.com Page90f11 \. ( ( ( ( ( ,jil1ech EnvilbUJn,ntQILllhQratories, LLC· Arnbient Air Sarnt)lil'1!:l. Plan (MSP) ( #: A22 /- Sampling Co: \ 6128/2d~~ Date:· Cpmpany Name: ,.~S:L'}~",~e:!lrg"Y!!./A",irt",e",ch,-_ _ _ _~samp[er's Name: ..A",n",dr",ew",fY=u",M",in,-_~_,-_~_ .C;onsulting Film;.' to~panYName,:.. S~YG .';';:"':". ""'.' "",' , Project Manager: ~,rere~::)t;l .!:R~[D~-.,._ _ _-'---:_.,- ,Project Na.me: 5!:D2· I'D. Project Number: ( ( ( ( ( Sampling Site:"lnfdrmation "'-,',',' , " :r :Lo~tion: RID-Ai2\ . : Clienr~ [D: Surface of Main Cana'[ RID~92 , Je.ddress: _ _ _'------~---_-- Discl1ar C e ( pescribe the,s!t~ [o'ca,tion: C ( Sampling Train CanisJ~~;:+ >1.0 L Ds', Grab ~a:fu,PI~r:- 6.0 L I]] 0 O~e"mi;' y, Silanized: , Tw? min 0 Fiv~ min One ~fhf:;'Taking:ol)e,mjnute to fill one liter canister;" nmiIrit~gra~ed -?jrnp1er E}sampling du~tion: " , .,~~mpling,~t,lr\;oate: '~a'hlpling",EnQ:' Date: . 612812011 6/2,8~O,11,'~ ,' AnY.~!~:biryg. used on :th.e. ,sa~;t:~{;?' Tubing typ~: Tyg6n~ . Teflon 0 0 NO o Other: _ _:..".~_ _ __ O~e hour ~ 4 hourD' 24 hour Othe'r: D 8'hq~rD T1me: dO"35 Gau~~Jea9: ~:R Time: eo,~' Gau~e'(ead: NoD Yes Vinyl Tuijing used from't!t~;,~amp.ling point to canister: 0 \\.. PYC 0 Length: 'inch Wind: '0, coD X 10 Cloupy 0 Hg U~J Rain 0 ( ( ( C ( ( C ( ( ( ( C ,<'A Field DupUcate YON 0 If Yes, ( nli 10 the. blanks blow: ( Describe}ti~,9~plicat~,~~nipl~ site,position arid,,~l! sepiifra~:MSP Form': , inch, inch '110\\-\.. 'f:£ Mild Comments: inch, Hg Y0~O L~~"" ~~.~ '~:,;,~,,,, I Other.: _ _ _ _ _ _ _o C - _ C.omments: $ D ~ lfxe,~'f',fjll the in,W[flJation below: Are all par:ts of ;SarnpUng Train testeq in the la~,~efore sampling? Temperature:' 12 hour ~_'-~.,....._ _ _ _ __ C ,,' " , C ' Sampling siter,,~Fection Note: ( 4620 E. Elwood Street, Suite 13, Phoenix,:AZ'85,040 • Phone:480:"968-5888. Fax: ~&0-966-1888. yshi@azairlab.,cl;ml " P~ge10of11 , ' C C C ( ( ( ( ( ( Ainech Environmental laboratOries, llC Ambient Air Sampling Plan (MSP) #: A14 Sam piing Co. Date: _ _6"12",8,,,12"0c.11-,--_ Company Name: .>S"-yn",e"rg",y",{AO!i"rte,,c,"h~_ _ _ _ _ _ Samprer's Name: ~An=dr"e",w"N"u"M",'I"n_ _ _ _ _ _ __ Conl;ulting Firm: "R"ID"-_ _ _ _ _~~-- Company Name: .,S"-yn"'e"rg"'y'-_ _ _ _ _ _ _ _ _ _ _ Project Name: Proje'ct Manager: Project Number: Sampling Site's Ihformation Location: ""R"ID'"'·A,,1,,4'-_ _ _ _ _ _ _ _ _ _~_ _ Client's ID: RID'BacLr(jun~.-28-.1.1 Address: ~~) . Describe the site location: Sampling Train Canister: 1.0L 0 6.0 L 0 00 yw Silanized: D Grab Sample'r: One min Two min One min = Taking one minute to fill one liter canister. Time' [ntegfat~d Sampler ~Salnpnng duration: Five min oNO Other: _ _ _ _ _ _ __ ~ 4hourD 24 hour D Other: _ _ _~--'-..,...---- 8hourD Sampling start: Date: 612812011 Time: 9i>~ Gauge read: Sampling End: Date: 6128{2011 Time: OCil3S Gauge read: Vi~yl D Any tubing used on the sampling train? Tubing type: Tygon D Teflon 0 NO~ Tubing use(j from th-e sampling point to canister. PJe all parts of ~ampling D One hallf Yes '2$.5 \ \-. 5 12 hour inch. Hg inch. Hg D' . If yes, fill the information below: PVC o Length: Other: _ _ _ _ _ _ __ inch 10 inch yO NO Train tested in the lab before sampling? Comments: L'I'J~ ~ ~ '/II\\..\... BE. ~) Weather -"-=~ture: Wind: O F lKJ CD D Mild D Sunshine D D Cloudy DRain D :po:in:t~:_::~~=::::~:===::::::::==:::::",,_~;:::::_----- At the samplingg_ Comments: Field Duplicate Y 0 N j If Yes, fill in the blanks blow: Describe the duplicate sample site position and fill separate AASP' Form: Sampling site Inspection Note: 4620 E. Elwood Street, Suite 13, Phoenix, AZ 85040 • Phone:480·968·5888 • Fax: 480·966·1888 • yshi@azairlab.com Page7of11 ~ ( c Airtech Environmental Laboratories (AEL) - AZ 0740 Date: July 11, 2011 c c ( c ( Client: Company: Address: Andrew J. MacHugh SYNERGY Environmental, LLC 10645 N. Tatum Blvd. Suite 200-437 Phoenix, AZ 85028 Work Order #: Project Name: Project Number: Received Date: 1106114 RID 802.10 6/29/2011 ( ( C C C C Dear Client: ( Airtech Environmental Laboratories received nine (9) samples for analysis. All analyses met laboratory QAlQC with any exceptions addressed in the Case Narrative. C ( C ( If you have any questions or concerns regarding your samples analysis, please contact the laboratory at 480-968-5888 c ( ( ( ( Sincerely, C ( C C Yu Min Shi ( ADHS License No. AZ0740 ( ( ( C C C ( C C ( Page 1 of 27 C ( ( '( '. ( ( ' ( ',I '( '( \[ \( \( \( \( H ' ( ) ! H , ) ( ) ( i ( i ( ; ( ' ( ) ( ' ) ( ' ( l ( i ! I ( , ( i ! ) f , r i ' \ ' \ ' i ' ) fiJ Airtech Environmental Laboratories (AEL) - AZ 0740 Client: Company: Address: Andrew J. MacHugh SYNERGY Environmental, LLC 10645 N. Tatum Blvd. Suite 200-437 Phoenix, AZ 85028 July ii, 2011 Date: Work Order#: Project Name: Project Number: Received Date: 1106114 RID 802.10 6/29/2011 SAMPLE SUMMARY One Hour Sampling Start LABID 1106114-02 1106114-03 1106114-04 1106114-05 One Hour Sampling End Start Stop 6/29/2011 TIME 0852 0851 0853 0855 28.1 28.0 28.7 28.0 10.8 10.8 10.5 9.8 28.0 28.2 9.3 9.3 28.2 9.2 10.0 9.8 CLIENT ID METHOD DATE TIME DATE A3 A5 A6 A7 TO-15 SIM RID-3 TO-15 SIM RID-3 6/29/2011 6/29/2011 6/29/2011 6/29/2011 0752 0751 0753 0755 6/29/2011 6/29/2011 6/29/2011 1106114-06 A8 TO-15 SIM RID-3 TO-15 SIM RID-3 TO-15 SIM RID-3 6/29/2011 0754 6/29/2011 0854 1106114-08 1106114-09 A16 TO-15 SIM RID-3 6/29/2011 6/29/2011 A13 A19 A23 TO-15 SIM RID-3 TO-15 SIM RID-3 TO-15 SIM RID-3 6/29/2011 0750 0750 6/29/2011 0850 0850 1035 1035 6/29/2011 6/29/2011 1135 1135 1106114-13 1106114-14 6/29/2011 6/29/2011 Page 2 of27 Gauge Reading (in. Hg) 28.5 28.2 ,",'\' "( C ( Airtech Environmental Laboratories (AEL) - AZ 0740 Date: July 11, 2011 ( ( ( ( , Client: Andrew J. MacHugh Company: SYNERGY Environmental, LLC Address: 10645 N. Tatum Blvd. Suite 200-437 Phoenix, AZ 85028 Work Order #: Project Name: Project Number: Received Date: 1106114 RID 802.10 6/29/2011 Case Narrative All samples and QC associated with your samples met the quality control objectives. Data qualifiers in this report are in accordance with ADEQ Data Qualifiers. ( ( ( ( C ( ( ( ( ( C C C ( c ( C ( ( Page 3 of 27 C ( ( " I \( '.( "( ',r -,( \( ~r 'I( \( \( I( 'I( ')( 1( l( ,I( i ( ) ( i( \( ')( Iii' Airtech Environmental Laboratories (AEL) - AZ 0740 Client: Project: Lab Order: LablD: SYNERGY Environmental, LLC RID j( i( , ( ~('i( if 1( 1( j ( l ' \ . ' ) : \' 1106114 Sampling Kits QC Cal. Flow Rate 4620 EElwood Street, Suite 13, Phoenix f\Z. 85040 Flow Rate Phone: 480-968-5888, Fax: 480-966-1888 Page 4 of 27 i " i ' Jil Airtech Environmental Laboratories (AEL) - AZ 0740 Client: Project: Lab Order: Lab 10: SYNERGY Environmental, LLC RID 1106114 Sampling Kits QC CONC. 1 Stock S-1 00927-02 ..."'""'"""..""'"...''''..".''"..".. .. ~ ;tra Gases 272227 ''''' S-101104-01 1 Stock TO-15 25 Analytes ...,.........,,...,,..............._.....TO-1 "",,,,.. ,,.. ,, ... ,,....,,.,, ...".."""....""".."......_" 1.0 ppmv 9/21/2011 .:!:,5% :,:5% , 9/17/2011 ".....ij- ......""... """.........""',,....,,...... 5% 50 ppbv 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 i 9/23/2011 :,:5% 9/29/2011 5% 1 Phone: 480-968-5888, Fax: 480-966-1888 Page 5 of 27 .~ /--...., I r....' ~, I.r"\ , r·,I I "' , ' "I .:~ I r ' , ,~ ':, ! I ,r---.,_ ,,"\ r i, ' ~ /'\ ~ ~ ,--.. I" I ,~ I /""' ~~~~~ ' I ~"''''~~~~ I I I' I ~ ~~~~~~(• " I" ' • ( '. ( '( ',( \ 1 '( \ ( \ ( , ( \ 1 1( \ ( \ ( 1( 11 ) ( H ( rc I ( H ]( 11 ,( I 1 I ( I ( I ( 1( 1 ( I ( ) ! I ( I ( 1 ( \ ' \ ' \ Airtech Environmental Laboratories (AEL) - AZ 0740 Date: Client: Project: Lab Order: LablD: July 11, 2011 SYNERGY Environmental, LLC RID 1106114 LCS/LCSD LCS Result Analyses ppbv VOLA TILE ORGANICS IN AIR 3 LCSD Result LCSD %REC 3 T.V. ppbv ugIM 0,50 100 96,0 1,98 2,69 102 3.39 %RPD OM 1.62 2,63 82.0 98,0 OA8 1.98 2,58 0.53 3.59 106 0.51 3A6 0.41 Trichloroethene Tetrachloroethene 106 70~130% LCS Pass/fail LCSD RPD 70-130% 70-130% <25% Date Analyzed ppbv TO 15 SIM 1,1·Dichloroethene Surr: 4·Bromofluorobenzene ug/M LCS %REC 19,8 2.1 3.8 Analyst: JJ 6/2912011 6/2912011 6/2912011 96 70~130% 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Phone: 480-968-5888, Fax: 480-966-1888 Page 6 of27 I' \' ,f rc Airtech Environmental Laboratories (AEL) - AZ. 0740 July 11,2011 Date: Client: Project: Lab Order: LablD: SYNERGY Environmental, LLC RID 1106114 LCS/LCSD LCS Result Analyses ppbv VOLATILE ORGANICS IN AIR ugIM LCS %REC 3 LCSD Result ppbv LCSD %REC ugIM 3 T.V. 0.54 0.48 0.45 1,1-Dichloroethene Surr: 4-Bromofluorobenzene 2.14 2.58 3.05 108 96.0 90.0 0.57 0.50 0.46 Pass/fail LCSD RPD 70-130% 70-130% <25% Date Analyzed ppbv TO 15 SIM Trichloroethene Tetrachloroethene LCS %RPD 2.26 2.69 3.12 114 100 92.0 1.98 2.69 3.39 Analyst: JJ 5.4 4.1 2.2 6/30/2011 6/30/2011 6/30/2011 84 80 70-130% 70-130% Phone: 480-968-5888, Fax: 480-966-1888 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Page 7 0127 ~. /""' (~,~, '~I (---\ "'-"'1 -, ,~: I~ 0 . L'~ ,~:, ,--..." , . ' \ ~ '--"1 !~ ".-,., ~. ~ ,~ ,----- ~, ""-'1 <-...-..., (I (~ .~, , ~ ~ -)~' I~ ,,r-. I/""'\ /~\~, r Airtech Environmental Laboratories (AEL) - AZ 0740 Date: Client: Project: Lab Order: Lab 10: July 11, 2011 SYNERGY Environmental, LLC RID 1106114 Blank Analyses Result Result uglM' Limit Qual TO·15 SIM VOLATILE ORGANICS IN AIR 0.04 1,1-Dichloroethene < Trichloroethene < 0.04 Tetrachloroethene < 0.04 Surr: 4-Bromofluorobenzene ppbv Limit 128 OF Date Analyzed Analyst: 0.04 0.04 0.04 < 0.16 0.16 0.21 0.27 < 0.21 < 0.27 70·130 6/29/2011 6/29/2011 6/29/2011 %REC ~.' 4620 E.Elwood Street, Suite 13, Phoenix flZ 85040 Phone: 480·968·5888, Fax: 480·966·1888 Page 8 of 27 JJ l. C C Airtech Environmental Laboratories (AEL) - AZ 0740 (, Date: Client: Project: Lab Order: Lab 10: July 11, 2011 ( SYNERGY Environmental, LLC RID ( 1106114 Blank Analyses VOLATILE ORGANICS IN AIR ppbv Limit Result 3 ( ugIM Result Limit Qual TO-1S SIM OF Date Analyzed Analyst: 1,1-Dichloroethene < 0.04 0.04 < 0.16 0.16 6/30/2011 Trichloroethene < 0.04 < 0.21 < 0.04 0.21 0.27 6/30/2011 Tetrachloroethene 0.04 0.04 Surr: 4-Bromofluorobenzene 88 < 0.27 70-130 6/30/2011 %REC JJ ( l_ ( C C C ( ( ( ( ( ( ( ( ( ( ( C ( ( ( C C C C ( ( C ( ( C 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Phone: 480-968-5888, Fax: 480-966-1888 Page 9 of27 ( ( ( ( Airtech Environmental Laboratories (AEL) - AZ 0740 Date: Client: Project: Lab Order: Lab 10: SYNERGY Environmental, LLC RID 1106114 02 Analyses VOLATILE ORGANICS IN AIR 1,1-Dichloroethene Trichloroethene Tetrachloroethene Surr. 4-Bromofluorobenzene ~ Client Sample 10: A3 Project Number: 802.10 Collection: 6/29/2011 Matrix: Ambient Air ppbv Result Limit ugIM3 Result Limit Qual 0.87 7.52 0.95 0.04 0.04 0.04 90 70-130 OF Date Analyzed Analyst: TO·15 SIM 0.22 1.4 0.14 July 11, 2011 0.16 0.21 6/29/2011 0.27 6/29/2011 6/29/2011 %REC .. ro 4620 E.Elwood Street, Suite 13, Phoenix {l;Z 85040 Phone: 480-968-5888, Fax: 480-966-1888 Page 10 of 27 JJ L ( '- C Airtech Environmental Laboratories (AEL) " AZ 0740 ( Date: Client: Project: Lab Order: LablD: SYNERGY Environmental, LLC RID 1106114 VOLATILE ORGANICS IN AIR ppbv Result Limit 0.17 0.04 Trichloroethene Tetrachloroethene 1.2 0.13 0.04 0.04 Surr: 4-Bromofluorobenzene 92 ( Result Limit Qual C DF 0.16 0.21 0.27 C Date Analyzed Analyst: 0.67 6.44 0.88 70·130 C ugIM3 TO·1S SIM 1, 1~Dichloroethene C Client Sample ID: A5 Project Number: 802.10 Collection: 6/29/2011 Matrix: Ambient Air 03 Analyses July 11, 2011 JJ C 612912011 C 612912011 612912011 C %REC C C C ( ( ( ( ( ( "- ( ( ( ( l ( ( C C C C C C C C ( C C C 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Phone: 480·968·5888, Fax: 480·966·1888 Page 11 of 27 ( ( ( ( Airtech Environmental Laboratories (AEL) - AZ 0740 Date: Client: Project: Lab Order: Lab 10: SYNERGY Environmental, LLC RID 1106114 04 Analyses ~. VOLATILE ORGANICS IN AIR 1,1-Dichloroethene Trichloroethene Tetrachloroethene Surr: 4-Bromofluorobenzene Result Client Sample 10: A6 Project Number: 802.10 Collection: 6/29/2011 Ambient Air Matrix: ppbv Limit Result uglM' Limit Qual TO·t5 SIM 0.17 1.2 0.14 0.04 0.04 0.67 70-130 OF Date Analyzed Analyst: 0.16 0.21 0.27 6.44 0.95 0.Q4 80 July 11, 2011 6/29/2011 6/29/2011 6/29/2011 %REC 4620 E.Elwood Street, Suite 13, Phoenix {l;Z 85040 Phone: 480·968·5888, Fax: 480-966-1888 Page 12 of 27 JJ ".( ( Airtech Environmental Laboratories (AEL) - AZ 0740 ( Date: Client: Project: Lab Order: Lab 10: SYNERGY Environmental, LLC RID 1106114 VOLATILE ORGANICS IN AIR 1,1-Dichloroethene ppbv Result Limit uglM' Result Limit Qual Trichloroethene 0.08 0.08 Tetrachloroethene 0.16 0.08 ( C ( OF Date Analyzed 2 2 6/30/2011 2 6/30/2011 TO·15SIM 0.30 1.9 C Client Sam pte 10: A7 Project Number: 802.10 Collection: 6/29/2011 Matrix: Ambient Air 05 Analyses July 11,2011 Analyst: 0.32 1.19 10.2 1.08 0.43 0.54 6/30/2011 C JJ C C ( ( Surr: 4-Bromofluorobenzene 78 70·130 %REC ( ( ( C ( C ( ( ( ( ( C ( C ( C ( ( ( C ( ( C C ( C ( 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Phone: 480·968·5888, Fax: 480·966·1888 Page 13 of 27 ( ( ( ( Airtech Environmental Laboratories (AEL) • AZ 0740 Date: Client: Project: Lab Order: Lab 10: SYNERGY Environmental, LLC RID Client Sample 10: A8 Project Number: 802.10 Collection: 6/29/2011 Matrix: Ambient Air 1106114 06 Analyses VOLATILE ORGANICS IN AIR 1, 1~Dichloroethene Trichloroethene Tetrachloroethene Surr: 4-Bromofluorobenzene Result ppbv Limit ugJM' Result Limit Qual TO·15sIM 0.27 2.0 0.18 0.04 0.04 0.04 98 July 11, 2011 Date Analyzed Analyst: 1.07 10.7. 1.22 70,130 OF 0.16 0.21 0.27 6/30/2011 6/30/2011 6/30/2011 %REC r' 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Phone: 480-968-5888, Fax: 480-966-1888 Page 14 of 27 JJ ~ ( ( Airtech Environmental Laboratories (AEL) - AZ 0740 ( Date: Client: Project: Lab Order: Lab ID: SYNERGY Environmental, LLC RID VOLATILE ORGANICS IN AIR ppbv Result Limit ( ( 3 Result Limit Qual DF TO·15SIM C Date Analyzed Analyst: 1,1 Dichloroethene 0.99 0.04 3.92 5.4 0.60 0.40 0.04 29.0 4.07 Tetrachloroethene ( ugIM Trichloroethene w ( Client Sample ID: A16 Project Number: 802.10 Collection: 6/29/2011 Matrix: Ambient Air 1106114 08 Analyses July 11, 2011 0.16 2.15 0.27 1 6/30/2011 10 6/30/2011 6/30/2011 JJ ( C ( ( Surr: 4-Bromofluorobenzene 102 70·130 %REC ( C ( C ( ( ( ( ( ( ( C C C ( C ( ( ( ( ( ( ( ( ( C 4620 E.Elwood Street, Suite 13, Phoenix AI. 85040 Phone: 480·968·5888, Fax: 480·966·1888 Page 15 of 27 ( ( C ( ( Airtech Environmental Laboratories (AEL) - AZ 0740 Date: Client: Project: Lab Order: LablD: Client Sample ID: A13 Project Number: 802.10 6/29/2011 Collection: Matrix: Ambient Air SYNERGY Environmental, LLC RID 1106114 09 Analyses VOLATILE ORGANICS IN AIR ppbv Result Limit 1,1-Dichloroethene < 0.04 < 0.04 Tetrachloroethene < 0.04 Surr: 4-Bromofluorobenzene U9IM Result 3 Limit Qual 100 < 0.16 0.04 0.04 0.04 < 0.21 < 0.27 70·130 DF Date Analyzed Analyst: TO-15 SIM Trichloroethene July 11, 2011 0.16 0.21 6/30/2011 0.27 6/30/2011 6/30/2011 %REC ~. 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Phone: 480-968-5888, Fax: 480-966-1888 Page 16 of 27 JJ l ( C Airtech Environmental Laboratories (AEL) - AZ 0740 ( Date: Client: Project: Lab Order: Lab 10: SYNERGY Environmental, LLC RID 13 VOLATILE ORGANICS IN AIR 1,1-Dichloroethene ppbv Result Limit Trich[oroethene Tetrachloroethene 0.75 Surr. 4-Bromofluorobenzene ugIM3 Result Limit Qual 0.20 0.20 0.20 116 C 70·130 ( ( OF Date Analyzed 5 5 6/30/2011 5 6/30/2011 TO-15SIM 0.55 3.3 ( Client Sample 10: A19 Project Number: 802.10 Collection: 6/29/2011 Matrix: Ambient Air 1106114 Analyses July 11,2011 Analyst: 2.18 0.79 17.7 5.09 1.07 1.36 6/30/2011 %REC C JJ C C ( ( ( C C C ( C ( C ( C ( C C C ( ( ( ( ( C C C ( C C ( ( 4620 E.Elwood Street, Suite 13, Phoenix fl:Z. 85040 Phone: 480·968-5888, Fax: 480-966-1888 Page 17 of 27 ( ( ( ( r Airtech Environmental Laboratories (AEL) - AZ 0740 r Date: Client: Project: Lab Order: Lab 10: Client Sample ID: A23 Project Number: 802.10 6/29/2011 Collection: Ambient Air Matrix: SYNERGY Environmental, LLC RID 1106114 14 Analyses VOLATILE ORGANICS IN AIR Result ppbv Limit 0.20 1.2 0.20 0.20 Tetrachloroethene 0.25 0.20 Surr: 4-Bromofluorobenzene ug/M' Result Limit Qual DF 110 0.79 6.44 1.70 70-130 Date Analyzed Analyst: TO·15 SIM Trichloroethene 1,1·Dichloroethene July ii, 2011 0.79 1.07 1.36 5 5 5 6/30/2011 6/30/2011 6/30/2011 %REC 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Phone: 480-968-5888, Fax: 480·966·1888 Page 18 of 27 JJ I '-----' ( Airtech Environmental Laboratories (AEL) - AZ 0740 ( ( Canister Cleaning Certificate Canister size: 1.0LD 6.0L~ Other: Serial Number: _..c14::::4"'4'--_ _ __ AEL Canister Clean Batch#: ....;1'-'1.::.05=..-..:.15=--_ _ _ _ _ __ Comments: Analytical Method: T015 SIM Comments: c This canister has been cleaned and has been individually analyzed to certify the analytes in the box are below the Report Limits. ( C ( Report Limits Analyte ppbv 1 ,1:P.i9~lgE9",t~",neL~! ( i i ugIM i 3 C 0.04 ( Ir!£h.19E9",!~",n<:'.. ... !~I.g:g~ Tetrachloroethene "'!t:l"!n"'.. __ I_:: c Comments: Chemist: Yu Min Shi Date: 6/27/2011 4620 E.Elwood Street, Suite 13, Phoenix AZ. 85040 Phone: 480-968-5888, Fax: 480-966-1888 Page 24 0127 ,,~ ( Airtech Environmental Laboratories (AEL) - AZ 0740 c ( ( Canister Cleaning Certificate Canister size: 1.0LD 6.0L~ Other: Serial Number: _..:;14"'5"'9_ _ _ __ ( c ( AEL Canister Clean Batch#: ----'1--=-1"'05=---.:.15=--_ _ _ _ _ __ C Comments: ( Analytical Method: l T015 SIM ( Comments: C This canister has been cleaned and has been individually analyzed to certify the analytes in the box are below the Report Limits. ( c ( Report Limits .. 1I..' . :..·:.c~:h.:.:I.o";r:.."o."e.t.:.:h. : .e".:n.:. e::......................_.......... ,_........:., .......0.04 .....,........~L 0.21 .,,?g.~,,!.9.E.9_~,!.b~D.e~ ........................i /~I (~,,~: -,,~ (--\ /--'-1 ; ' \ ""----": ,'----', ,~\ ~ /"'1 ( ' . ,~" ~ ~I ~ ,/"""'"\, ~ /~I / \ ,~. /-' (' (~ 00~0~)0~ . ! \' , /--, ~ I ' ' --'' ' ' ""\ '\.' ~ r t ,- Airtech Environmental Laboratories (AEL) - AZ. 0740 Date: Client: Project: Lab Order: Lab 10: SYNERGY Environmental, LLC RID 1106114 Blank Analyses Result ppbv Limit ugIM3 Result Limit Qual TO-1S VOLATILE ORGANICS IN AIR '- July 12, 2011 DF Date Analyzed Analyst: 1,1-Dichloroethene < 0.10 0.40 7/4/2011 < 0.10 0.10 0.10 < 0.40 Trichloroethene < 0.54 7/4/2011 Tetrachloroethene < 0.10 0.10 < 0.68 0.54 0.68 Surr: 4-Bromofluorobenzene 89 70-130 7/4/2011 %REC 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Phone: 480-968-5888, Fax: 480-966-1888 Page 7 of 17 JJ Airtech Environmental Laboratories (AEL) - AZ 0740 Date: Client: Project: Lab Order: Lab 10: SYNERGY Environmental, LLC RID Client Sample 10: AI Project Number: 802.10 Collection: 6/29/2011 Matrix: Ambient Air 1106114 01 Analyses ppbv Result Limit 1,1-Dichloroethene 350 2.0 Trichloroethene 760 17 2.0 2.0 SUrr. 4-Bromofluorobenzene ug/M3 Limit Qual Result 84 ( (" OF TO-15 VOLATILE ORGANICS IN AIR Tetrachloroethane July 12, 2011 Date Analyzed Analyst: 70-130 1,390 4,080 7.92 10.7 115 13.6 20 20 20 7/5/2011 7/5/2011 7/5/2011 %REC JJ ( l ( C C ( ( ( ( ( C C ( ( ( ( ( ( ( C ( c C C l ( c 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Phone: 480-968-5888, Fax: 480-966-1888 Page 8 of 17 ( C Airtech Environmental Laboratories (AEL) • AZ 0740 Date: Client: Project: Lab Order: Lab 10: SYNERGY Environmental, LLC RID 1106114 Client Sample 10: A15 Project Number: 802.10 6/29/2011 Collection: Ambient Air Matrix: 07 3 ppbv Analyses Result Trichloroethene 410 580 Tetrachloroethene 5.2 Surr: 4-Bromofluorobenzene ugIM Limit Result Limit Qual OF TO·1S VOLATILE ORGANICS IN AIR 1,1-Dichloroethene July 12, 2011 83 Date Analyzed Analyst: 2.0 2.0 2.0 1.620 3,110 35.3 70·130 7.92 10.7 13.6 20 20 20 7/5/2011 7/5/2011 7/5/2011 %REC '--" 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Phone: 480·968·5888. Fax: 480·966·1888 Page 9 of 17 JJ ~ ( ( Airtech Environmental Laboratories (AEL) - AZ 0740 ( Date: Client: Project: Lab Order: LablD: ppbv Result Limit VOLATILE ORGANICS IN AIR 1,1-Dichloroethene Trichloroethene Tetrachloroethene Surr: 4-Bromofluorobenzene ugIM3 Result Limit Qual DF 90 ( ( 20 20 20 70-130 2,570 79.2 17.700 1,020 107 136 ( Date Analyzed Analyst: TO-15 650 3,300 150 ( ( Client Sample ID: A17 802.10 Project Number: Collection: 6/29/2011 Matrix: Ambient Air SYNERGY Environmental, LLC RID 1106114 10 Analyses July 12,2011 200 200 7/5/2011 7/5/2011 200 7/5/2011 %REC JJ ( C ( ( ( ( ( C ( ( ( ( ( C ( C ( C ( r ( c c ( ( C ( C ( C ( 4620 E.Elwood Street, Suite 13, Phoenix AZ. 85040 Phone: 480-968-5888, Fax: 480-966-1888 Page 10 of 17 C ( ( ( Airtech Environmental Laboratories (AEL) " AZ 0740 Date: Client: Project: Lab Order: Lab 10: SYNERGY Environmental, LLC RID 1106114 11 Client Sample ID: A18 Project Number: 802.10 Collection: 6/29/2011 Matrix: Ambient Air uglMJ ppbv Analyses Result Limit 1,1-Dichloroethene 1.3 0.10 Trichloroethene 4.7 0.72 0.10 0.10 Tetrachloroethene Surr: 4-Bromofluorobenzene Result Limit Qual TO·15 VOLATILE ORGANICS IN AIR 83 July 12, 2011 DF Date Analyzed Analyst: 70·130 5.15 25.2 0.40 0.54 7/5/2011 4.88 0.68 7/5/2011 7/5/2011 %REC 4620 E.Elwood Street, Suite 13, Phoenix fl:Z. 85040 Phone: 480·968·5888, Fax: 480·966·1888 Page 11 of 17 JJ ~. ( ( ( Airtech Environmental Laboratories (AEL) - AZ. 0740 Date: Client: Project: Lab Order: Lab 10: SYNERGY Environmental, LLC RID 1106114 12 Analyses 1,1-Dichloroethene Trichloroethene Tetrachloroethane Surf: 4-Bromofluorobenzene U9IM Result C ( Limit Qual OF 5.94 26.9 7.46 70-130 0.40 0.54 0.68 C Date Analyzed Analyst: 0.10 0.10 0.10 83 ( 3 TO·15 1.5 5.0 1.1 ( Client Sample 10: Duplicate 0 Project Number: 802.10 Collection: 6/29/2011 Matrix: Ambient Air ppbv Result Limit VOLATILE ORGANICS IN AIR July12,2011 7/5/2011 7/5/2011 7/5/2011 %REC JJ ( c c ( ( C ( C ( ( ( ( ( C ( ( ( ( ( C ( ( C ( ( C C C C C ( 4620 E.Elwood Street, Suite 13, Phoenix p;z 85040 Phone: 480·968·5888, Fax: 480-966·1888 Page 120117 ( ( ( ( Airtech Environmental Laboratories (AEL) - AZ 0740 Canister Cleaning Certificate 1.0L~ Canister size: AEL Canister Clean Batch#: 6.0LD Other: Serial Number:_-'1::,8"'67'--_ _ __ --'1-'1~0"'6-="0~1_ _ _ _ _ _ __ Comments: Analytical Method: T015 Comments: This canister has been cleaned and has been individually analyzed to certify the analytes in the box are below the Report Limits. Report Limits ~.' ppbv !,1:!?!~~.I'?Eg_~th~D.E'.._._.I....~:.,. . . . ,.:0.10 . ,.".-.. . I,. . _. <:.,. . . . .,0".;40. •.1._ .. . .". . . ". "". . """". . ". ,. ". "'."". . ". . ". .". Trichloroethene ~ ~ ~ ~ ~ 0.10 < . . · "·. ··"l-.! . _. ·'·. ·. · 0.54 !'~.!~§!.~b.!'?fg.~.!~~n~.........g:~S."i_.... ,...."....... _..... _... _............ ".......1.... ...._.._.."......._..........."......- ........_......_...__."..........,.......__.....i _......._....... ! ! ...._.. _.........._........._......._..........._....._....._............L....__ . .~._.......".,..... Comments: Chemist: Yu Min Shi Date: 6/27/2011 4620 E.Elwood Street, Suite 13, Phoenix AZ 85040 Phone: 480-968-5888, Fax: 480-966-1888 Page 13 of 17 \. ( Airtech Environmental Laboratories (AEL) - AZ. 0740 C ( ( Canister Cleaning Certificate Canister size: 1.0LG] 6.oLD Serial Number: _-"18::.:7..=6_ _ _ __ Other: AEL Canister Clean Batch#: --,1,-,1",06"--,,,,0-,-1_ _ _ _ _ _ __ ( C C C ( Comments: Analytical Method: ( ( ...:T..=O:..:1.;::5_ _ _ _ __ Comments: C This canister has been cleaned and has been individually analyzed to certify the analytes in the box are below the Report Limits. ( C ( Report Limits ppbv 1 Analyte 3 ugIM ( i C yO ( ( inch CommentS: Miid' "D ( : 127153 D Ves Vinyl D Tubing used from the sampling point to canister: Olhe" _ _ _ _ _-'-_ __ Five min 4 hourD 8 hourD 12 ,hour 0 Other. _ _ _ _ _ _ _ _ _ __ Gaugeread:2V=b inch.Hg Gauge(ead: Inch. Hg I/J. 32 If yes, fill the Information below: PVC D length: Other: _ _ _ _ _ _ _ __ inch Are ali parts of Sampling Train tested in the lab before sampling? Y ID inch 0N D Comments: L'N~ez. ~6N,. ~ IN~\..L 9C: Weather F" ~ Temp' D Middle At the sampling point Upwind Wind: Mild CO D Sunshine 0 trong D D Cloudy useu) DRain D Downwind Comments: Field Duplicate NJ8:r YD IIYes. flU in the blanks blow: Describe the duplicate sample site position and fill separate AASP Form: Sampling site Inspection Note: (\...lcll \ , - " - I r '.. _--=v"--.!-'ft,2:z;\,=",,t\\--,E-£""",\,,,,-,-,,=,~::!..g=:s::t'9=-==-\'V-,-,,-....:..N \-1'\ ''''C. ~, 4620 E. Elwood Street, Suite 13, Phoenix, AZ 85040 • Phone:480·968-5888 • F~ 48046~-1888 • yshi@azairlab.com age 0 14 ~ ~. ", 8: oi 7-P.;;:r 3 8, 1 :s d' '1.1 )j' :}? H') %: t.\'J If\} \~,y ~ \10 .1 -:::::- Page 4 of 14 l. ( c ( ( ( ( #: A7 " S\!rnpling Co. Date: ' :. 612912011 C6!llpany--~~me: ""s",yn"e",rgy!l!I~Ai!!!rte~ch:!!'_ _~_.,-_sampler'S Name: !:A\!l'nd~r~ew!!.lY~u!.!M~in~.~_~~~-,.:.:- Cons!!)lin9 Firm: " Company Name: Synergy ". PrQj~Manager: ~ ;: '"" ( ( samllling,Slie's Information Location.: .!OR",iD",~A0!7_ _~""","~_~--,,~~-,.,.~_ ( ( Addre~:~' ':-,,"~~~""'-.c..,.~""'-~~-~..,.,-­ Descri9~ the site locatio'l): san!~ling Train ¢:r7C?auge read: D 12 8hourD Qlhei: !?Is;; r,es, Othe.r: ~~~~--'..,.,-'-'-__ ~ ,4~ourD O!! 'il 0 ( N Are alr~arts of Sampling Train tested I'n the, iab before sampling? /'.,' '."., ',', W~.athe~. C ( " . ""'-""'>.~,. \ Ot<\";' ~ ~\' >. ( ( inch VI]]ND At the ~nipllng poInt Mi ' { Upwind . Strong 0 ( ( ( ( ( ( ( ( C'«~~~ D~ 'N\U:;~t~ F"~. C'O. Sunshine 0 Cloudy 0 Rain 0 Mild ( ( ( ( 0 Downwind ( Field. Duplicate yO N~ If Yes. flll in the blanks blow: ( '[j~:~ribe tjie, duplicate sampl~,~ifi,' position'\~:n~ fill separate AASP Form: s~mD.iin.g·SitelnsDeCtio. II Note: ..." • ., . /. It. r:::.,,'.,.,. .• '",,' . . ... : . '1\... \l)"') ( . .. ,~\\. ~\:.\bD'>i~E ::x.21~ C C ( ( ( C ( "-- ( Page 5 of 14 ( C ( ,r ,r r AlnachEnl.renmalllllaboratorlas,llC ,r r ,- \£\4~ll~L-14~ . ,r Ambient Air Sampling Plan (AASP) #: A8 Sampling Co. Date: 6/29/2011 Company NamE:!:: "S"'vn"e"m"'vi,,"'' '·rt'' ec'' h'-_ _ _ _ _ Sampler's Name: "An"d"'r."'wIY=u,.,M"I,,"_ _ _ _ _ _ _...; Cons.ulting Firm: Company Name: .::s"'yn::e~m~y--=,....---.,__--Project Name; 3c:e,\..:.'~ Project Manager. RJD Project Number: Sampling Site's Information Location: .:;R:::ID,,·A,,8"-_ _~--------~­ Address: Describe the site location: Sampling Train Capister: 1.0 L Grab,Sampler: o 6.0L0 Onemin 0 Silanlzed: Two min· 0 O~er. Five min ________ ~ ________ One min =,Taking one minute toflll one liter canister. nmelntegratedSampler~Samplingduration: One hour ~ 4hourD 8hourD D Samplingstert Date: 6/2912011 Sampling End: Date: 6/29/2011 TygonO Time: N~ TeflonO 0 Vinyl 28_£1 ~ Yes' Tubing used from the sampling point to canister. 0 PVC Gauge read: ,q~ "3 inch, Hg If yes, fin the ii1fortnation below: 0 Length: Other: _ _ _ _ _ _ __ inch Are all parts of SampnngTraintestedinthelab'beforesampnng? ,'-- D 24 hour Other. - - - - r ; n - : : - - - - TIme: O;;Zi;q Gauger.ad: Inch,Hg Any tubing used on the sampling train? Tubing type; 12hour 10 _ _ inch Y [R] NO Comments: (~~E;';1-~~ ~ "'-l~LL·~ Weather . ~. Wind: Miid At the sampling point F"IK] CO Mid e Upwind 0 Sunshine 0 trong 0 0 v-sro). 0 Clo~dy Rain 0 Downwind Comments: Field Duplicate YON!;if If Yes. fill in the blanks blow: Describe the duplicate sample site position and fill separate AASP Form: Sampling site Inspection Note: (\.. I. 'n \\ _\0-,-,'1/::::'-..:LB~z,o""MD....IC;~:w~~""D~.$J~)OGI::::!:.I<~=W..\"'-.!..:.:::1 ~, 4620 E. Elwood street, Suite 13. Phoenix, AZ 85040 o Phone:480·968·5888 0 F",: 480·966't888 0 ysbi@azairtab.com page 60f 14 ~- ~ I',,.J S'I>1 ~ I~ I~ &:tI'-J ~- Page 6 of 14 "-. c c f " ( ( ( AinechE....romu.ntalllllb..'atories.llC Ambient Air Sampling Plarl(AASP) ( -- #: A13 c Sampling Co. Date: 6129120,11 Company Nanfe: ~S"-)m",e,"rguy!!:IA",irt",e,,,Ch,----~_ _ _ _ Sampler's Name: "A"'"d"re"'w"N.!.!u'"'M!!ti!!!n_ _ _ _ _-'-~_ C,onsultingFirm: Company Name: ,S"yn"e"'rg"y-'-_=---"O,--i-;-_-,---_ _ Project Name: . Project Manager. ~ :::I~\... ~ Project Number. RID _*_'_-..:'<:C2-==_'..:L::..'U=+._~_ Sampling Site's 1I1formaiion . . . . Location: .cR"'I()"'~~A"--1,,·3'___ _~_ _ _ _ _- - - - - A\i», Describe the site la,cation: • ·~·.O L Canister':" D 6.0 ~~.[R] CJ D Grab sampler. One IT!in Two min One min =-Taking one minute to.,fill6ne liter canister. Time Int~wated Sampler [&r~'~~p;ing duration: Five min' . One hour 24hbur SarrfpIr~g' sia:rt: Date: S~mpliri~ ~nd: D~le: Anytubil)9 used on the D ( [J Ofuer. ____________- - - - 4 hourD 12'hour o At the samplklg />T~ ( ( Downwind Comments: Field Duplicate C ?5il.. inch, Hg F' 0 ( Gauge read: ,()N~~~~ ~ IN~\.C ~0-SE:\)). Mild" C CJ"feff? Tempera Wind: 8 hourD Ofuer: _ _ _ _ _"'-_"'-_ __ Are aU parts of, $arriRli,QgJrain tes~ed in theJab befqre sampling? Weather ( ( Time: : Tubfng used from t~e ,s~mpling point to canister: C<:lmmentS: C 6/2912011 Tygon [J Tubing type: ~ C C NO Silanized: l ( CUent's 1D:, RID-Ba,round 6,29-11 Address: SampUngTrain ( l '\C) b~:NQce,NxfMQ'?IP ' page70f 4 "\W88 ~ C ( l C ( C c Page 7 of 14 ( ( ( ( r ,r Alnech EnvironmentallaboralOrias, lle Amoient Air Sampling Plan (AASP) #: A15 Sampling Co. Date: -,..,...::6",/2",9,,,20,,,1-'.1~_ Company N:ame: ~Syn=e"rg..y,"lftj.::·rt"e"ch,,--_ _ _ _ _ _ Samprer's Name: ::.A"nd"'r"ew"'N""u.::M"'in-'-_ _ _ _ _ _ __ Consulting Firm: Company Name: ~S'f.yn~e~rg ..y'---_=____---,_ _ _ project ::rO&\..- ?:<"S~'2S=>:,i Project Manager: Sampling Name: RIO' Project Number: _;:j\:_'O_b_Z_"_t'-:o=--____ Site's~lnfoi"mation Location: .cR"'ID"'·"A,,1S"--_ _ _ _ _ _ _ _ _ _ _ _ __ Client's 10: HeadS ace in RID-114 Address: /1<.1 Diversion Box Describe -the site loCation: Sampling Train Canjster: 1.0 L 0 6.0 L 0 0 NO Silanized: 0 Grab Sampler: One min Two min One min = Taking one minute to fill one liter canister. Time Integrated Sampler ~samp[ing duration: Five min One hour 24 hour r D Samplingstart: Date: 612912011 Time: O'1S\ Sampling End: Date: 6/2912011 Time: O'OS \ Any tubing used on the sampling train? '-- - ~ Tubing type: Tygon 0 Teflon 0 NoD Tubing used from the sampling point to canister: Vinyl 'Yes ~ 0 PVC Length: o Other. _ _ _ _ _ _ __ 4 hourD Gauge read: eather Temperatur . 12 hour D Gauge read: 1../ inch, Hg .-Lq inch, Hg If yes, fi[[ the information below: o Other. _ _ _ _ _ __ _ _ inch Me all parts of Sampling Train tested in the lab before sampling? Comments: 8 hourD Other: _ _ _--;;;:=,--____ 10 ~inch Y0 NO J L'N~~ ~o,..j D~ v:>\u... ~ <.A.S8) ~ lKJ Co D Sunshine D Cloudy DRain D '--- Describe the d,uplicate sample site position and fill separate AASP Fonn: Sampling site Inspection Note: 4620 E. Elwood Street, Suite 13, Phoenix, AZ 85040 . • Phone:480-968-5888 _ F~: 480-966-1888. yshi@azairlab.com page Bof14 Page 8 of 14 l~ ( ( ID ( Airt8Ch!~;;~ronqa8ntal18bOrat.rI.~{;IlC . ... ... l\I"('lD!!lnMir Sampling Plan (MSP) Sanipling Co. Date: ~ #: A16 . ( ( 6/29/2011 Compa[!Y,'f\J,ame:' ",S",yn",e"rg",yf!!:A~irt~echo:!!..._ _ _ _ _ _ Sampler's Name: !:.A"nd",re",w"!!N"u"M"!!!!.!ln_ _-,~_ _ __ Con§l'!!i))g Firm:. Coni~~iiY'Name: "S'Eyn=e"rgu.Y_'-~"""'--7;-,-_--;-~_Project Name: pr6j~Manager:--r00\.-.~ ( !:.R7.ID~.,-~_ _ _ _ __ d;\'~, \.1£) Project Numbei: C Sainplin~:Site'slnformation ( Location:· ;.R",fb.,,,,"A,,1,,6,---,-~_ _ _ _~_ _ _ _ __ Client's ID:.:B"'Z==~="'-'!\~'-"'''--_ Address":>".~·_ _ _.,--_ _ _..-_....,."""_.,....,_ __ ( Describ6:the sJte [oeatto:n: ( Sambling Train Gi~i~ter: 1.0 L D "G~rab'Sampler: 6.0 L D On~min_ W Silanized: Y 0 TwomJn W Fivemin ( N D 0 Other. _ _ _ _ _ _ _ __ Ohe min = Taking one minJ!!e to fi!l-one liter canister. ,'Time lrit!3:~rated samPle;,[]samPling duratIon:, Dai~::" 6/29/2011 Anyrubing 4~d o~"tfie '~~lTlplin'g train? Sampling End:', Tubing Tygon:D 2::J!.oli[,oD Vin~ TeHonD tis~:d' from th~ s~'mpling point t~ canis!er., Are all',Plfts of comfu9'~ts: ~ 12 hour ( o \ ( Other: ~.,-_ _ _--,.._ _~_ _ p PVC D ( ( ( Other: _ _ _ _ _ _ __ Length: inch samQ,~'rgTraintes'tedintheI13:6'before,sampling? , ' 8 hourD 4 houry Time~~ Q ._~ G-~~cie read: 2~ .'l--Inch. Hg Time: ci S?i) Gauge read: q. S i~chi Hg NO,g Yes D If ~es, fill the information beloW:, Sarripl.irig start: Date:- _ 6/29/2011 Tubing typO: One,hour Y ID ( inch 00 NO ',,' , C '" C w;ai~~.~(~~\~~~oN.~~ 'N\\A- ~.~J. 'eratl!t~: O F IKJ Wind:"~ild Co D Sunshine S!(ong D D Cloudy 0 Rain ( 0 C ( ( Eieici'Ouplicate yD' tI ( If Yes, fin in the blanks blow: De~'Cribe tl!~Jju~licate' sample site positio'n and fill separate AASP Form: ( Samplinf:1site Inspection Note:",. ('~.ii:.II. ..•.. . . ..... . •. ' . • ""<'0.: ~E ~ G\)e-'Ps6F .............. oQ~ ~k3-J.,,\£. Qcl\.sW. JO . 4620E,~1.w0od Street, Suite 13, Phoenix, AZ 85040 ~' o~ • Phone:480-968-5888 • Fax: 480-966.-1888. YShi@azair1ab.com- ...._..... /'.(". _ ~ Page 9 of 14 ~ ~ . ( . \...,\...~ "t>'I~~IQo..\, ( ~ 'S'¥- C C C ( ( Page 9 of 14 ( ( ( Ain8ch Environmental Labo,ato,les,UC Ambient Air Sampling Plan (AASP) #: A17 Sampling Co. Date: _---"6~/2,,9~/2"'01.!c1~_ Company Name:' -"S!lyn~e:!Jrgi!ly,"/A"irt~e",ch,,--_ _ _ _ _ _ Sampler's Name: !A~n~dr!-,e,!!w!2lY~uC!M!!!in~_ _ _ _ _ __ Consulting Finn: Company Name: -"S!lyn~e:!Jrgi!ly,-~_ _ _ _ _ _~_ _ Project Name: ::IO'€:L~ru Project Manager: RID Project Number: Sampling Site"s Information Location: lR~IDe:-~Ac!.17,- _ _ _ _ _ _ _ _ _ _ _ _ __ Client's lO: HeadS. pace in Salt Cajl Manhole (I?e the'site location: '.j( I DN 't ) Clienrs 10: '12v'PI-\~ b (- '-- r '- Sambling Train Canister: " 1.0 L 1iU~.0 L g Silanizel Project Manager. .!:Re:ID~._ _ _~_ _ __ Name,: 4li'6:YZ. . l a Project Number. Sampling Site's Information Location: .!:R",ID",-"A2=:3~ _ _ _ _ _ _ _ _ _ _ _ _ __ ~ '" Clienfs ID: Surface of Main Canal @ Address: Sat! Canal Dlscarge (AP-3) Describe the siteJocation: Sampling Train Canister: 1.0 L 0, 6.0 L 0 Silanlzed: 0 0 Grab Sampler: One min Two min bne min = Taking one minute to fill one liter canister. Time Integrated Sampler 0sampling duration: Five min One hour ~ 24 hour D Sampling start: Date: 612912011 11me: lO?S Samplin9 End: Date: .612912011 11me: N'oD Any tUQing used on the sampling train? J81 0 Tygon 0 1ZJ PVC 8hourD 12 hour Ofuer. __________________ Gauge read: F' m erature: Wind: Mild idd[e IK] C' 0 0 Strong 0 0 'I.. 8' inell, Hg Ofuer: _ _ _ _ _ __ inch [D y0 Dffi""A Sunshine "'I\\J..Cloudy inch NO J ~VlSE:U 0 Rain 0 samplin:g~pO:i:nt~.~~u:p;W:in:d;~~~:~~~~=;=::::::::::=_~=:::::::=- At tQe Comments: _ Field Duplicate Y·O __ If yes, fill the information below: o Length: ().,N~E;\2... ~~ Weather D ~ Gauge read: 'Z.'S ,~ inell, Hg Are' all parts of Sampling Train tested in the lab before sampling? Comments: Other: _~_ _ _ __ 4hourD t \~ Yes Tefton Vin~ Tubing used ftom the sampling point 10 canister: Tubing type: oNO __ N}?( If Yes, fill in fue blanks blow: Describe the duplicate sample site position and fill separate MSP Form: Sampling site Inspection Note: \ I\.... :ro " -'2., _ _ _ _ _ _ _ _ _ _ _ ___ ~ -SO~1>o.4:: Df \Nks9'2.. )~~:tV ~ G!\:AISTf.,!2.. . , 4620 E. Elwood Stree4 Suite 13, Phoenix, AZ 85040 I' 'Phon,,480·968·S888 'Fax: 480-966·1888, yshi@azairtab.com \.-St:.e ~ Page 13 of 14 fv~ ~~ C2. 5~\ Wf'\L \ \)\s;.C~ J Page 14 of 14 L ( C ( ( ( ( ( ( ( - l~ ( C ( ( ( l ( ( . ( ( ( C ( ( ( C ( ( ( ( ( C ( ( ( ( ( C ( '- ( ( ( ( (3w SYNERGY ENVIRONMENTAL, LLC APPENDIX COPIES OF SYNERGY ENVIRONMENTAL WATER SAMPLING FIELD DATA SHEETS I ( '( '( i( ' ( '( 'f '( \( 1( H 1(]( 1 ( ) ( ) ( ) ( 1( H H)( ,f H)~:r II II I ' , I , ' 1 ' , ' ) ( I r \, r \,' FIELD DATA SHEET FOR GROUNDWATER SAMPLING prOject~BYz. .\ 0 SAMPLE ID tS-\ RID Well/canal Site: £;'0- \ SAMPLE DATE 'fz7!\1 TEMP (OC) TIME db'2.6 ----- --- ----- \l'-1-3 ~ ~l'\)\oS (~\'\)\05 pH (S.U.) On-Site: E.C. (uS) - --............. t---- - - ---- ---------- \o7::.";f- /'" \O~ '2..?Co «'.q'b Q.) \'2...'l. '" \oa.\ Z4.~ (:03 '2..) \4b I 'ot\-3 '24-4 1·05 \~ page_I_OfS ANALYSIS 'Bt.~t'5. COMMENTS/NOTES FG'/\l,\~&aT %lJ' <1''2.7h \ ~ 050 FIELD METER - - --- ) Off-Site: \ - "2.J ~ ~\C.b... ifi;r ~~a.\Nt< I't' ~"'~ SNoJ\?\.6~.i CDu..e.cntJG> IN 12-1w.~ ~~ 'W ~\2S0. ~~ t>~i..J~-N ---..., ~~'W~~~ ? ~flo..",", V'I ~ ""i ~ "'" ~ 1,2-~ ~ w' Ie ~~ ~. "'_T~~ 7\,· V~'qq\~\ ~ no - ~? (A'/tii!. 1.---- _ _ _ _ _ _ _ _ _ - - - - - - - - - - - - GPQ\A~G\\' ---- ---- --- - ---- -- - - - - - - - - - - - - - - f(:~ -..;,-~~ Y,SYNERGY ENVIRONMENTAL. LLC If PrOject~' FIELD DATA SHEET FOR GROUNDWATER SAMPLING \ 0 RID Well/Canal - - --- SAMPLE ID - SAMPLE DATE w-4 0/1.-1 I \ \ @~\t:>\C \\0'3, v:z.:, .C) '·n \\04' \,~ \ \\"2-5 1-\5 - 2.4.0 - - - ANALYSIS \\~~~- COMMENTS/NOTES ?v..~ \N\:n~ ~ '*~Nt\ ~~Co\\~~~ '?v.~ :t~\~_ ~ I7.OD \/\'2t-\ 1AA 1.1'0 24.1... 1.\\ V\\~ \\'7..-:/ ~ \\'7Jb 'b'UPJ~ ~~G:>\\ -\ j . «", f ::i ~ ,---., ~ r--- ~,~: r., ~: (.-. " ' ' -' ' , i~ f ' \ "~, ~\ ~, ' ) ~, I~' (' ,f""', ~ . ( ' I ~ ~, ~ ---1 ~ ,"'--"" ~: (-\, !,-...", r;, i~ .r';: ;~ G.~!" S YN1\., R",. EHvmo ;~,: ~ (.--.. . . LLC ~ ~, ,~, ,:~ ~, (- "( . ( '( '( '( \ ( • ( '( ',( ',( '( \ ( 1 ( \ ( ) ( 1 ( 1 ( '( 1 ( 1 ( ) ( 1 ( ) ( 1 r 1 ( 1 r '\ ( 1 ( ') ( '\ ( 1 r \ ~. \ 0 SAMPLE ID RID Well/canal Site: ¥t\t>~\c6,1\O, \\').on-Site: SAMPLE DATE cq-z;-, ~~t>\OJ /' ~-, '" 4;(1..-'7 W~ ~\U'D\'O /' \ ~ l- ~\2..\C>\Q.. 111...1- .I TIME \\ H<:::ft., \\S~ \'2.0 \ II \~9-, \'2.\0, \'1.2-\ ~ - 'V5:~ pH (S.U.) 1. \'0 r '\ r '\ ' " ,r " '£A.L\- l· '1- - - E.C. (uS) FIELD METER ANALYSIS COMMENTS/NOTES ~ \1 \ 1f>.,;'7j, _"t! l1'~ \f\~ . ~CP'3:> - ~.Cc -r .\0 \Jq~ V5:~ .., .\0 \)q5\ (#,d\<;, \~ t£(e~ l.CO '2..,02k. \V\S ~:~ ,,0\ - ~M ,""'-. \.J h.. I'" VltOo 1:-1.\ !_\~..IL Page~OfS Off-Slte: _ _ __ \""'\lA .. \)' '1,\2- L'Y\~ \"1-"2..:'3. '2--5.0 1 .\1).. /f " \24-\ '" TEMP (OC) \'2..a:> "l4.~ ~ .lId '\ FIELD DATA SHEET FOR GROUNDWATER SAMPLING .~ Project: r - I~u.-. \t-.\\-n~~ ..... ~ ~IhoB ).\tI,. '. ~\eG>~\ede~ . i{l.. a ~cJ.\ecl n. ~M/ /, ~~\-flM~ '"4OZS ~o~\ ~~~ I~de C,l\echl (~SYNER~Y " lH I EHVIROHNEHTA L. LLC r 'I r ' Project:~. I'D SAMPLE SAMPLE DATE 10 I"1'Z.1\ \\ ~~\t:>l\~I. C \N- \ \ ~ \J'J-2'2- FIELD DATA SHEET FOR GROUNDWATER SAMPLING \ZID-IY~ I"\c, '+IE!;., 0" ~~, TEMP \~OS \ ~~'l'Ill <: V\r'C"' .. IA.rI_ 'N-\O) pageiOf Off-Site:._ _ __ S E.C. (uS) FlELD METER ''''1~ ~ ... ANALYSIS COMMENTS/NOTES I?I,)..~ Tl'\.-I\i~ \~04 1?iJ·'d.., 1I!:f~~~~C:L-IJ pH (S.U.) On-Site: \?O~I - ~I\;\C t...N~Ll~ 1\40\ cR~t 1'2.., \\3 I 'ZIb." ( . \'1 1'2-, \2.>7 '30:0 ~t!t:s. ~III I\t;-1--~ 1 - ~\.l~ ~r-tl~. "SS LSD2 I )403 rzA.?'" l--"Zl 'l-ttl:1 to~ 1'Se.v.~e. G:,\\ec.-le.d _ (.Co\ lLS\S \)5\ \ ~ 1~~_G::;ll~~ 1- 1- ~~~;J /' h4~ I'Z---:I:l 11·'2x:; hm4 rr Of>6-J~J '" 1\4-7:;.1- I Uo:1 11-'0 12,m5 ~~l\ ~~ \j.\'\-n~ O I\N :-~1~L~ I \4"h4 I %. \ 11.?;S 1'2-,d\:~ ~ ~n\e eoUee-bJ 11'6\ bJ~L\C~~ I..L<; ~~to'\e~tI rr' l'ri ~ 01:" \f\I~. ,~. ~.,. ;'ij 1SYNERGY £HVIlIOH!II:.TAL. LLC ~~~~0~~~n~n~0n~~~nn0~n~~I~r,~nr~~nrnnn~~~~~nnr '( ,,( '( '( ' ( ' ( ,( '( '( 1 ( ' ( ) ( ) ( ) ( ) ( ) ( .' ( ) ( ) ( ) ( ) ( 1 (1 ( 1 ( 1( 1( ) ( 1 ( ) ( 1 ( 1 ( '( '\ ( )' '} l ' 1 ' '\ ( FIELD DATA SHEET FOR GROUNDWATER SAMPLING prOject:~'Z..' \ Q SAMPLE ID \N-\'2~~l~ SAMPLE DATE RID Well/canal Site: TIME ~'\H )'SR] (' '"V ~ @\ t:>~ TEMP (OC) pH (S.U.) On-S"e: E.C. (uS) - \<50<6 2<0:2 ,.\'2.. Lq'U::, \'5\'0 -1..-'3.'2. 1.\"\ \lqGo~ 1'5\2.. '2t\.'S 1·\6 lPIC\3 Off-Site: _ _ _ __ FIELD METER , ...... ANALYSIS \I\', ::".C- pageS of 5" COMMENTS/NOTES ?~~ T~-\-ti~ cc,~ I~ .,.--\ , e Gd\~~. - %f~ SYNERGY )1 E.VlIlOHM!:"TA!.. LL C Integrity: (Check) analyses performed ·'on c., )-z'R-'.! , '1 ,-"-, /--." ) :--. ,~~ ,i ,~ , ,'" ,~ "' " /-.., ~, ~ ~"~ ~ ,r--., ~ . ',~ , ~\ ,~,(..- ,( · ( \ ( '. ( \ ( ',r 4~, \'0 _ -==--____ Project: SAMPLE ID SAMPLE DATE '.( i( \,~ '.( I( If)r i( RID Well/canal Site: ~'i pH TEMP (OC) TIME I_ (S.U.) I_ \\ \2.\~~ On-Site: E.C. (uS) 1_ ~~ '2.S\~ 1, \,-1'6-) o::33d.- f2A-.~ '1.0') \;'113 0?3i\- '1A-A- I. Ct: 'I( Ie ~(.)C .Jf I( I( ~(,\/ 1( I f 'It!().r)')( ):' l' Page_\_Of3 Off-Site: _ _ _ __ ANAl YC:IC: FIELD METER ,I). I~~ \~\,\\~, .... ~.) --- - -_.- \N-~ )()()( FIELD DATA SHEET FOR GROUNDWATER SAMPLING '51.5: 't'-J-\"? ~\2-'tJt9) 1( o:.:,.~ \,* .- a;..,~ "lPJ-O 1·\3 \)lo2fc:, cr.:Ac\ ~.'t; -?q \,1&3 ~3 ~"2.k>o'-:> D I~~r1 , - - ---g I~'""'''''''''''''' ± ~\?\.A~ I~~ \~\-n~. , ;.S I( I-\ 1...1,~ ll~3 \,\~l l\~"3. ")...0.C, (.o~ I) \<=)0 (' (" COMMENTS/NOTES t'1.lVG£: \~~~ .-. ~~ ·t\~~ '3 ~~e. GA\ec-\ec\.. ,. . "'/'l,' ..t"> ;;) l'1. E?d'ec~~ ?..;:,~ \~\,,~ 4!.CO.~ \202... - \"Z..o; ~;l - - 1l0~ \J"LS1.. \~ '(...S :~ .,30 \i7..::1S \2-0, V\,~ /.?P \i1..~ Page~of3 Off-Slte: _ _ __ FIELD METER ANALYSIS ?~\N\'\\~ l"'-W~ h. I~ ,.,,~ COMMENTSINOTES -"" ~"'-~ ~c\ed I~"""'L~ ~~,~~ ~ ~B. I ~Jurl,e Co~\eC\e~ ~!""SYNER~\ ' Jl / ENVlIIOHMEHTA LLC r '\ r \ >~-' Date/Time: 2. rt~1 f..- ( Time: (Check) I2rD .~-,;: normal - By: ,to: D8v'for the,servlces' requested on thi:h::l1ain .. of custody form and "any additlonal ,analys~s'performed'on, this project. ','" .lnvoice-. Samplo(s) wlllbedlsPOSeaol "ne' aoo,ys. '",,' - ': -, -' ,~ ---' ,,..-, -~, ,.....:..., ,\ ' , ' '---- ,", _~ r' ~ ,( "'--"',~ _,~, ',', .' ~ I , _____ " ~ _~ 0---, ' i:'-'- ;---', -~i ,,~ f'. ~ -""""", A -'~: ,-.., I~ (~'. --<:~\ :-" r '( '( ',( '( '( \ ( \ ( ; ( '( \ ( '( 1 ( ) r. ,r 1( ) ( ) ( ) ( 1 ( ; ( ,( ) ( ! ( ) ( ,r 1 r 1 ( 1 ( 1 ( I ( 1 ( 1 r ! r ,r 1 " 1 " " " FIELD DATA SHEET FOR GROUNDWATER SAMPLING Project~' \ 0 SAMPLE ID ~-\ SAMPLE DATE TIME 1a.~T\\I~\ ~~\\:)\\Arl(' ) ~ 'N-\'b M M~g@..9kt....'"'~\)...'- RID Well/canal Site: i;c{2.-\ 11\' b On-Site: TEMP pH (OC) (S.U.) - E.e. (uS) ~~~~I C~S>144 \ Off-Site' _ _ __ "O~~I ~% G::.\\ecW'. I~\" ~~m' <."t. ~ ~~\.E ~\e~ t)1kD!:> I It--ic..\.-. ~?~~ b:.- &.(~SYNERGY ~I '" ! EHVIBOHNtHTAL, LLC , ( . TIme: (Check) ~.-X (Check) .' on iCe form arid any addltionai analyses performed on this/p'r~jEu:ii> ~,-.\ I /-----" r~ (~'I~ /-- '-,r--.: r'\ r .~. r ~\,"'--'" /". ,r-., ( ~ I I ,r. ." ~ ~ ~ ~ r· ~ n 9P(~ .~ t; ~ ( SYNEBGY ENVIRONMENTAL, LLC APPENDIX COPY OF TESTAMERICAFINAL ANALYTICAL REPORTS \r r ( TestAmerica n-lE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 LABORATORY REPORT Prepared For: ,- Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Project: PO #802.10 June 2011 Sampled: 06127111 Received: 06/27/11 Issued: 07/05/11 13: 17 NELAP #01l09CA Arizona DHS#AZ0728 The results listed within this Laboratory Report pertain only to the samples tested in the laboratolY. The analyses contained in this report were peiformed in accordance with the applicable certifications as noted All soil samples are reported on a lVet weight basis unless othenvise noted in the report. This Labora/ory Report is confidential and is intended/or the sole lise ofTestAmerica and its client. This report shall not be reproduced, except in/Ill!, without written permissionjrom TestAmerica. The Chain o/Custody, 1 page, is included and is 011 integral part of this report. This entire report was reviewed and approved/or release. CASE NARRATIVE LABORATORYID CLIENTID MATRIX PUF1584-01 TB PUF1584-02 PUF1584-03 PUF I 584-04 PUF1584-0S PUFlS84-06 PUFlS84-07 PUF1584-08 PUFlS84-09 PUFlS84-1O PUFlS84-11 PUF1584-12 PUF1584-13 PUFlS84-14 EB-l Water Water Water Water Water Water Water Water Water Water Water Water Water Water W-3 W-4 W-S W-6 W-7 W-8 W-IO W-ll W-22 W-19 W-12 Duplicate A TestAmerica Phoenix Carlene McCutcheon Project Manager PUF1584 TestAmerica THE LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Report Number: PUFI584 Sampled: 06/27/11 Received: 06/27111 SAMPLE RECEIPT: Samples were received intact, at 3°e, on ice and with chain of custody documentation. HOLDING TIMES: All samples were analyzed within prescribed holding times and/or in accordance with the TestAmerica Sample Acceptance Policy unless otherwise noted in the report PRESERVATION: Samples requiring preservation were verified prior to sample analysis. QA/QC CRITERIA: All analyses met method criteria, except as noted in the report with data qualifiers. ( ( ,~ ( C L3 EPA 8260B:LaboratOlY Control Sample andlor Laboratory Control Sample Duplicate recovery was above the acceptance limits. Analyte not detected, data not impacted. RI EPA 8260B:The RPD exceeded the acceptance limit. ( COMMENTS: No significant observations were made. ( SUBCONTRACTED: No analyses were subcontracted to an outside laboratory. ( C ( C ( C ( ( ( ( ( C ( C ( ( C C ( C Reviewed By: C C C C TestAmerica Phoenix ( Carlene McCutcheon Project Manager C The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except infull, without wrilten permissionjrom TestAmerica. PUFl584 ( ( ( l ( ( \ r TestAmerica 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437·3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Batch Reporting Limit IIFI075 IIFI075 11FI075 11FI075 IIFI075 11FI075 11FI075 11F1075 IIFI075 I1FI075 11F1075 IIFI075 IIFI075 IIF1075 11FI075 IIFI075 11F1075 IIFI075 I1FI075 IIF1075 IIF1075 11FI075 11FI075 IIF1075 I1FI075 IIFI075 IIF1075 IIF1075 11FI075 IIFI075 IIF1075 IIF1075 IIFI075 IIFI075 11FI075 IIF1075 11F1075 11FI075 11FI075 IIFI075 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 '- ,,,... ,'- '-... Sampled: 06/27II I Received: 06/27II I Report Number: PUFI584 VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) ,- , Project!D: PO #802.10 June 2011 Analyte Method Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers Sample !D: PUF1584-01 (TB - Water) Reporting Units: ug/l Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene '-- ~ r. '-' sec-Butylbenzene rtert-Butylbenzene '-- Carbon disulfide ,.. . Carbon tetrachloride r-- _ Chlorobenzene "-.-/ Chloroethane r- - Chloroform Chloromethane 2-Chlorotoluene ---- 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane ,,-, l,2-Dibrornoethane (EDB) ___ J Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1A-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane l,2-Dichloroethane 1,1-Dichloroethene cis-l,2-Dichloroethene trans-l,2-Dichloroethene l,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene cis-l,3-Dichloropropene trans-l ,3 -Dichloropropene Ethylbenzene Hexachlorobutadiene EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B . EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/201 I 6/29/2011 6/29/20 II 612912011 6/29/20 II 6/29/2011 612912011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/20 II 6/29/2011 6129/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/20 II 6/29/2011 6/29/2011 6/29/2011 6/29/201 I 6/29/2011 612912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 612912011 6/2912011 612912011 6/29/201 I 612912011 6/29/2011 6/29/20 II 6/29/2011 6/29/20 II 6/29/2011 6/29/201 I 6/29/2011 612912011 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples rested in the laboratory. This report shalll/ot be reproduced. except injull. without writtel/permissionjrom TestAmerica. PUFI584 "-. ( TestAmerica ( THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200·437 Phoenix, AZ 85028 Attention: Joel Peterson ( I, VOLATILE ORGANICS BY GCIMS (EPA S030B/S260B) Analyte Method Batch Reporting Limit 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 Sample Dilution Date Result Factor Extracted Date Analyzed 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 612912011 6/2912011 6/2912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 612912011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 Data Qualifiers Sample ID: PUF1584·01 (TB - Water) - cont. Reporting Units: ugll 2-Hexanone Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride 4-Methyl·2·pentanone (MIBK) Methy1-tert-buty1 Ether (MTBE) Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND C \. ( Sampled: 06/27/11 Received: 06127111 Report Number: PUF1584 ( ( l ( C ( C ( C ( ( ( ( ( ( ( ( ( ( 108% ( 102% 100% ( C l C C ( ( C C TestAmerica Phoenix ( " Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report sila/lnot be reproduced, except inJull, without wriltcnpcrmissionJrom TestAmerica. PUF1584 ( ( l > TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/27111 Received: 06/27111 Report Number: PUFI584 VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Method Analyte '-, '- , '-r '-- "'r '--- r '- . r ~.~ r, ,"--r" '-. ...... _/ r, \,._/ r' 1.. •. -' r-' '-r '-r-' ,--/ '-'-...-- '-'-..._ '-~. '-'- Sample!D: PUF1584-02 (EB-I- Water) Reporting Units: ugll Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1.2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-l,2-Dichloroethene trans-l,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-l,3-Dichloropropene trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B Batch Reporting Limit IIFI075 IIFI075 IIFI075 IIFI075 IIFI075 IIFI075 IIFI075 IIFI075 IIFlO75 IIFI075 IIFI075 IIFlO75 IIFI075 IIFI075 IIFlO75 IIFI075 IIFI075 IIFI075 11FI075 11FI075 IIFlO75 11FI075 11FI075 11FI075 IIFI075 11FI075 IIFI075 IIFI075 IIFI075 11FI075 IIFI075 IIFI075 IIFI075 11FI075 11FI075 IIFI075 IIFI075 IIFI075 11FI075 11FI075 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 Sample Dilution Date Result Factor Extracted ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 6/2912011 6/29/2011 612912011 6129/2011 6/29/20 II 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6/29/2011 Date Analyzed Data Qualifiers 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/20 II 6/29/2011 612912011 6/29/20 II 6/29/2011 612912011 6/29/2011 6/29/2011 6/2912011 6/2912011 6/2912011 612912011 6/29/2011 6/2912011 6/2912011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 612912011 6/29/2011 612912011 6/29/2011 612912011 6/29/2011 612912011 6/29/2011 612912011 6129/2011 6/29/2011 6/29/2011 6/29/2011 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced. except inJII/l, without writlenpermissiolljrolll TestAmerica. PUFl584 ( TestAmerica ( THE LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 10645 N. Tatum Blvd .• Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Sampled: 06/27/11 Received: 06/27111 Report Number: PUF1584 ( C ( VOLATILE ORGANICS BY GCIMS (EPA S030B/8260B) Analyte Method Sample ID: PUF1584-02 (EB-I- Water) - cont. Reporting Units! ug/l EPA 8260B 2-Hexanone EPA 8260B Iodomethane EPA 8260B Isopropylbenzene EPA 8260B p-Isopropyltoluene EPA 8260B Methylene Chloride EPA 8260B 4-Methyl-2-pentanone (MIBK) EPA 8260B Methyl-tert-butyl Ether (MTBE) EPA 8260B Naphthalene EPA 8260B n-Propylbenzene EPA 8260B Styrene EPA 8260B 1,1,1,2-Tetrachloroethane EPA 8260B 1,1,2,2-Tetrachloroethane EPA 8260B Tetrachloroethene EPA 8260B Toluene EPA 8260B 1,2,3-Trichlorobenzene EPA 8260B 1,2,4-Trichlorobenzene EPA 8260B 1,1,1-Trichloroethane EPA 8260B 1,1,2-Trichloroethane EPA 8260B Trichloroethene EPA 8260B Trichlorofluoromethane EPA 8260B 1,2,3-Trichloropropane EPA 8260B 1,2,4-Trimethylbenzene EPA 8260B 1,3,5-Trimethylbenzene EPA 8260B Vinyl Acetate EPA 8260B Vinyl chloride EPA 8260B Xylenes, Total Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) Batch Reporting Limit Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers ( 11F1075 11F1075 11F1075 l1F1075 11F1075 11F1075 11F1075 11F1075 11F1075 11F1075 l1F1075 11F1075 11F1075 11F1075 11F1075 11F1075 l1F1075 11F1075 11F1075 l1F1075 l1Fl075 11F1075 llF1075 11Fl075 11F1075 11F1075 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 107% 101 % 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 612912011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/2912011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 612912011 6/29/2011 6/2912011 6/29/2011 612912011 612912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6129/2011 C ( C ( ( ( ( ( ( ( ( ( ( ( C ( r "( 96% TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall/lOt be reproduced, except infull. wi/houtwrilten permissionji'Om Tes/America. PUFl584 <.Page 6 of 62> c c ( ( l ,r , \ TestAmerica THE LEADER IN ENVIRONMENTAL TESTING ,~ Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson , 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Pax:(602) 454-9303 VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Batch Reporting Limit IIFI075 IIFI075 11FI075 IIFI075 11FI075 11FI075 11FI075 11FI075 11FI075 IIF1075 11F1075 IIF1075 IIFI075 IIFI075 IIFI075 IIFI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 IIFI075 IIFI075 IIFI075 IIFI075 IIFI075 IIFI075 11FI075 IIF1075 11FI075 IIFI075 11FI075 11FI075 11FI075 11FI075 11FI075 I1FI075 11FI075 11FI075 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 '-- r '-- Sampled: 06/27111 Received: 06/27111 Report Number: PUFI584 Method Analyte Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers r Sample!D: PUF1584-03 (W-3 - Water) Reporting Units: ugll Acetone Benzene Bromobenzene "'-- Bromochloromethane r Bromodichloromethane '--, Bromofonn '--' Bromomethane r-\ 2-Butanone (MEK) .....- n-Butylbenzene sec-Butylbenzene r-·, tert-Butylbenzene Carbon disulfide rCarbon tetrachloride " ' ..j EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 Chlorobenzene '--..-/ Chloroethane r Chlorofonn EPA 82608 Chloromethane ,----" 2-Chlorotoluene ...---- 4-Chlorotoluene '-- Dibromochloromethane 1,2-Dibromo-3-chloropropane ,.- l,2-Dibromoethane (EDB) EPA 82608 Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-l,2-Dichloroethene trans-I,2-Dichloroethene 1,2-Dichloropropane l,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-l,3-Dichloropropene trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene EPA 82608 r EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.68 ND ND ND ND ND ND ND ND ND ND 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/2912011 6/2912011 6/2912011 6/29/2011 6/2912011 6/2912011 6/29/2011 6/2912011 612912011 6/2912011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 612912011 6/2912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except injull, withoutwril1enpermissionjrom TcstAmerica. PUF1584 TestAmerica THE LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 Sampled: 06/27111 Received: 06/27111 Report Number: PUF1584 VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Analyte Method Sample ill: PUF1584-03 (W-3 - Water) - cont. Reporting Units: ug/l EPA 8260B 2-Hexanone EPA 8260B Iodomethane EPA 8260B Isopropylbenzene EPA 8260B p-Isopropyltoluene EPA 8260B Methylene Chloride EPA 8260B 4-Methyl-2-pentanone (MlBK) EPA 8260B Methyl-tert-butyl Ether (MTBE) EPA 8260B Naphthalene EPA 8260B n-Propylbenzene EPA 8260B Styrene EPA 8260B 1,1,1,2-Tetrachloroethane EPA 8260B 1,1,2,2-Tetrachloroethane EPA 8260B TetrachIoroethene EPA 8260B Toluene EPA 8260B 1,2,3-Trichlorobenzene EPA 8260B 1,2,4-Trichlorobenzene EPA 8260B 1,1,1-Trichloroethane EPA 8260B 1,1,2-Trichloroethane EPA 8260B Trichloroethene EPA 8260B Trichlorofluoromethane EPA 8260B 1,2,3-Trichloropropane EPA 8260B 1,2,4-Trimethylbenzene EPA 8260B 1,3,5-Trimethylbenzene EPA 8260B Vinyl Acetate EPA 8260B Vinyl chloride EPA 8260B Xylenes, Total Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-dB (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) Batch Reporting Limit l1Fl075 l1Fl075 l1Fl075 11Fl075 11Fl075 11Fl075 l1Fl075 l1Fl075 l1Fl075 l1Fl075 11Fl075 11Fl075 l1F1075 11Fl075 l1Fl075 l1F1075 11Fl075 11Fl075 l1F1075 l1Fl075 l1F1075 l1F1075 11Fl075 11Fl075 11Fl075 l1Fl075 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 Sample Dilution Date Result Factor Extracted Date Analyzed 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/2912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/2912011 6/2912011 6/29/2011 612912011 6/2912011 6129/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 ND ND ND ND ND ND ND ND ND ND ND ND 3.5 ND ND ND ND ND 0.58 ND ND ND ND ND ND ND 110% Data Qualifiers ( \ ( ( ( ( ( ( ( ( ( ( C ( , ( 103% ( 98% ( ( C C , ( TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. 11,;s report shall not be reproduced, except in/uti, without written permission/rom TestAmerica. PUF1584 ( ( ( l r,- TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189. Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/27/11 Received: 06/27/11 Report Number: PUF1584 VOLATILE ORGANICS BY GC/MS (EPA 5030B/S260B) Method Analyte 'r Reporting Units: ugll Acetone r Benzene ~. Bromobenzene Bromochloromethane r Bromodichloromethane '-- Bromofonn r ...... _ Bromomethane 2-But.none (MEK) "--..---/ n-Butylbenzene r" sec-Butylbenzene ~~ tert-Butylbenzene -------- Carbon disulfide r Carbon tetrachloride ~. ,.--', Chlorobenzene '----...-' Chloroethane r', Chloroform u r- Reporting Limit Sample Dilution Date Result Factor Extracted Date Analyzed 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6129/2011 6129/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/2912011 6/29/2011 Data Qualifiers Sample ID: PUF1584-04 (W-4 - Water) '---- r, Batch Chloromethane 2-Chlorotoluene 4-Chlorotoluene ::'-- Dibromochloromethane l,2-Dibromo-3-chloropropane 1,2-Dibromoeth.ne (EDB) "---~ Dibromomethane 1,2-Dichlorobenzene ~" 1,3-Dichlorobenzene l,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane l,l-Dichloroethene cis-l,2-Dichloroethene trans-l,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene cis-l,3-Dichloropropene trans-l ,3 -Dichloropropene Ethylbenzene Hexachlorobutadiene EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B 11 F 1075 11Fl075 l1Fl075 l1F1075 l1Fl075 l1Fl075 l1F1075 l1Fl075 11Fl075 l1Fl075 l1Fl075 11Fl075 l1Fl075 l1Fl075 l1Fl075 l1F1075 11Fl075 11Fl075 11Fl075 11Fl075 11Fl075 11Fl075 11Fl075 11Fl075 11Fl075 11Fl075 11Fl075 11Fl075 11Fl075 l1F1075 l1Fl075 11Fl075 11Fl075 11Fl075 11Fl075 11Fl075 l1Fl075 11Fl075 11Fl075 l1Fl075 10 0.50 0.50 0.50 0.50 LO LO 2.5 0.50 0.50 0.50 0.50 0.50 0.50 LO 0.50 LO 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 LO 0.50 0.50 0.50 0.50 LO ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.9 ND ND ND ND ND ND ND ND ND ND ND ND ND 4_9 1.3 ND ND ND ND ND ND ND ND ND TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only 10 the samples lested in Ihe labora/ory. This report shallllot be reproduced, except illfull, wilhout wrillenpermission/i'om TestAmerica. PUF1584 ( TestAmerica ( THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.1 0 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterspn Sampled: 06/27/11 Received: 06/27/11 Report Number: PUFI584 ( ( ( ( C (' VOLA TILE ORGANICS BY GCIMS (EPA 5030B/8260B) Reporting Method Analyte Batch Limit Date Factor Extracted Sample Dilution Result Date Analyzed Data Qualifiers Sample ID: PUF1584-04 (W-4 - Water) - cont. Reporting Units: ugll 2-Hexanone EPA 8260B IIF1075 Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride EPA 8260B 11FI075 11 F 1075 11FI075 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl Ether (MTBE) EPA 8260B Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane EPA 8260B TetrachIoroethene EPA 8260B Toluene EPA 8260B 1,2,3-Trichlorobenzene EPA 8260B 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene EPA 8260B EPA 8260B 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride EPA 8260B Xylenes, Total EPA 8260B EPA 8260B EPA 8260B Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-dB (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) IIFI075 IIFI075 IIFI075 IIFI075 IIFI075 11F1075 11 F 1075 IIFI075 IIF1075 11FI075 IIFI075 IIFI075 IIFI075 IIFI075 IIFI075 IIFI075 IIFI075 IIFI075 IIF1075 IIFI075 IIFI075 11FI075 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 ND ND ND ND ND ND ND ND ND ND ND ND 25 ND ND ND ND ND 9.0 0.93 ND ND ND ND ND ND 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6129/2011 6129/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/2912011 612912011 6/2912011 6/2912011 6/29/2011 612912011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 111% 105% 96% ( ( ( (' ( ( ( ~ , ( ( ( C ( C ( ( ( C ( ( ( ( \ ( ( ( ,- c c ( c ( TestAmerica Phoenix Carlene McCutcheon Project Manager The resulfs pertain only to fhe samples tested in the laboratory. This report shall not be reproduced, except in/ul!, withoutwritlenpermissionjrom TestAmerica. PUFI584 ( ( ( ( l ( , ( ,- TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/27111 Received: 06/27111 Report Number: PUFI584 VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Method ,- Sample ID: PUFIS84-0S (W-S - Water) , Reporting Units: ugll Acetone Benzene r Bromobenzene Bromochloromethane Bromodichloromethane ,---. Bromofonn ("0 EPA 8260B Batch EPA 8260B IIFI075 IIFI075 EPA 8260B 11FI075 EPA 8260B IIFI075 EPA 8260B IIFI075 llFI075 EPA 8260B Bromomethane EPA 8260B IIFI075 2-Butanone (MEK) EPA 8260B llFI075 llFI075 '--- n-Butylbenzene r'o ,,--_,' sec-Butylbenzene c tert-Butylbenzene '------- Carbon disulfide c ' Carbon tetrachloride c-, Chlorobenzene . . _' Chloroethane Chloroform Chloromethane "--- 2-Chlorotoluene r-' 4-Chlorotoluene "--- Dibromochloromethane 1,2-Dibromo-3-chloropropane EPA 8260B ~- 1,2-Dibromoethane (EDB) EPA 8260B IIFI075 '----, Dibromomethane "--_ 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-l,2-Dichloroethene trans-l,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene cis-l,3-Dichloropropene trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene EPA 8260B llFI075 IIFI075 IIFI075 IIFI075 IIF1075 IIFI075 IIFI075 IIFI075 11FI075 IIF1075 IIFI075 IIFI075 IIF1075 IIFI075 11 F 1075 IIFI075 llFI075 11FI075 ~~ EPA 8260B IIFI075 IIFI075 EPA 8260B llFI075 EPA 8260B EPA 8260B IIFI075 EPA 8260B 11FI075 EPA 8260B IIFI075 EPA 8260B IIFI075 llFI075 llFI075 IIFI075 11FI075 IIFI075 EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B Reporting Limit 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 Sample Dilution Date Result Factor Extracted Date Analyzed 6/29120 II 6/2912011 6/29/2011 612912011 6/2912011 6/29/2011 6/29120 II 6/2912011 6/29/2011 6/29/2011 612912011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/20 II 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/2912011 6/2912011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/20 II 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/20 II 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/20 II 6/29/20 II 6/29/2011 6/29/2011 6129120 II 6/29/2011 612912011 612912011 6/29/2011 612912011 6/2912011 6/29/20 II 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.5 ND ND ND ND ND ND ND ND ND ND 0.65 ND ND 2.9 ND ND ND ND ND ND ND ND ND ND Data Qualifiers TestAmerica Phoenix Carlene McCutcheon Project Manager Tile results pertain only to 'he samples rested in the laboratory. This report shalll/ot be reproduced. except in/ul!. without wriltenpermissionjrom TestAmerica. PUFl584 "-~ ( TestAmerica C THE LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 ( Sampled: 06/27111 Received: 06/27111 Report Number: PUFI584 C ( C VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte ( ( Method Sample !D: PUF1584-05 (W-5 - Water) - cont. Reporting Units: ugll EPA 8260B 2-Hexanone EPA 8260B Iodomethane EPA 8260B Isopropylbenzene EPA 8260B p-Isopropyltoluene EPA 8260B Methylene Chloride EPA 8260B 4-Methyl-2-pentanone (MIBK) EPA 8260B Methyl-tert-butyl Ether (MTBE) EPA 8260B Naphthalene EPA 8260B n-Propylbenzene EPA 8260B Styrene EPA 8260B 1,1,1,2-Tetrachloroethane EPA 8260B 1,1,2,2-Tetrachloroethane EPA 8260B Tetrachloroethene EPA 8260B Toluene EPA 8260B 1,2,3-Trichlorobenzene EPA 8260B 1,2,4-Trichlorobenzene EPA 8260B 1,1,1-Trichloroethane EPA 8260B I, I ,2-Trichloroethane EPA 8260B Trichloroethene EPA 8260B Trichlorofluoromethane EPA 8260B 1,2,3-Trichloropropane EPA 8260B 1,2,4-Trimethylbenzene EPA 8260B 1,3,5-Trimethylbenzene EPA 8260B Vinyl Acetate EPA 8260B Vinyl chloride EPA 8260B Xylenes, Total Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) Batch Reporting Limit IIFI075 IIFI075 IIFI075 11FI075 IIFI075 11FI075 IIFI075 11FI075 IIFI075 IIFI075 IIFI075 11FI075 11FI075 11FI075 11FI075 IIFI075 IIFI075 IlFI075 11FI075 IIFI075 JlFI075 IIFI075 IIFI075 IIFI075 IIFI075 11FI075 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 Date Sample Dilution Result Factor Extracted Date Analyzed Data Qualifiers ( ( ( ND ND ND ND ND ND ND ND ND ND ND ND 8.8 ND ND ND ND ND 8.5 0.80 ND ND ND ND ND ND 112% 102% 98% 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6129/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/2912011 ( ( ( ( ( ( ( ( ( ( ( ( ( ( ( ( r ( l c c c c c c ( TestAmerica Phoenix ( Carlene McCutcheon Project Manager C The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except injull, withoutwrittenpermission!rom TestAmerica. PUFl584 ( ( ( l , ( r~ TestAmerica THE LEADER IN ENVIRONMENTAL TESTING Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 ;-'- 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Sampled: 06/27/11 Received: 06/27/11 Report Number: PUFI584 Attention: Joel Peterson ,VOLATILE ORGANICS BY GCIMS (EPA S030B/8260B) '-- ,- Batch Reporting Limit 11FI075 IIFI075 11FI075 IIFI075 11 F 1075 11FI075 11FI075 11FI075 IIFI075 11FI075 11FI075 11FI075 11FI075 IIFI075 11FI075 11FI075 11FI075 11FI075 IIFI075 11FI075 11FI075 IIFI075 IIF1075 IIFI075 11FI075 11FI075 IIFI075 11FI075 11FI075 IIFI075 IIFI075 11FI075 11FI075 11FI075 11FI075 IIFI075 IIFI075 11FI075 11FI075 11FI075 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 ',-~ '- ,.-~ r~ '( 1..... r '--_ r 1........ ('-. Analyte Method Sample Dilution Date Result Factor Extracted Date Analyzed 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 612912011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/20 II 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/20 II 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 Data Qualifiers Sample ID: PUF1584-06 (W-6 - Water) Reporting Units: ugll Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform '-- / Bromomethane ,-. 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide r', Carbon tetrachloride Chlorobenzene Chloroethane Chloroform '-/ " Chloromethane "---' 2-Chlorotoluene 4-Chlorotoluene r Dibromochloromethane "---/ 1,2-Dibromo-3-chloropropane r". 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene l,3-Dichlorobenzene ::-- l,4-Dichlorobenzene '-- Dichlorodifluoromethane ,,- l, l-Dichloroethane '-----" l,2-Dichloroethane ~, r~ '-- l,l-Dichloroethene cis-} ,2-Dichloroethene '--' trans-l,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene cis-l,3-Dichloropropene ______ trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.2 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.76 ND ND ND ND ND ND ND ND ND ND TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain Dilly 10 rhe samples rested in the laboratory. This report shall not be reproduced, except ;njull. without writfenpermissionjrom TestAmerico. PUFl584 ~... ( TestAmerica C THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix. AZ 85040 (602) 437~3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200·437 Phoenix, AZ 85028 Attention: Joel Peterson ( ( Sampled: 06/27111 Received: 06/27/11 Report Number: PUFI584 ( ( ( C VOLATILE ORGANICS BY GCrMS (EPA 5030B/8260B) Method Analyte Batch Reporting Limit 11FI075 IIFI075 IIFI075 IIFI075 IIFI075 11FI075 IIFI075 11FI075 11FI075 IIFI075 11FI075 IIFI075 IIFI075 IIFI075 IIF1075 11FI075 11FI075 IIFI075 IIF1075 llFI075 IIFI075 IIF1075 IIF1075 IIFI075 IIFI075 11FI075 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 Sample Dilution Date Result Factor Extracted Date Analyzed 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 612912011 6129/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 Data Qualifiers Sample!D: PUF1584-06 (W-6 - Water) - cont. Reporting Units: ugll 2RHexanone Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl Ether (MTBE) Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) ( C C EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND 2.7 ND ND ND ND ND 7.5 ND ND ND ND ND 2.8 ND ND ND ND ND ND ND 6129/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 109% 104% 94% C ( C ( C ( ( ( ( ( C ( C C ( ( C ( C ( C ( C ( C ( C C TestAmerica Phoenix Carlene McCutcheon Project Manager ( The results perlain only to Ihe samples fested in fhe laboratory. This report shall not be reproduced, except inJull, without writtenpermissionJrom TesrAmerica. PUF1584 C ( ( ,, (' "- TestAmerica 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437~3340 Fllx:(602) 454-9303 Tf-IE LEADER IN ENVIRONMENTAL TESTING , ,,r- Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/27111 Received: 06/27111 Report Number: PUFI584 VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) ,Analyte Method r Sample ID: PUF1584-07 (yI'-7 - Water) "-_ r Acetone EPA 8260B Benzene Bromobenzene EPA 8260B Batch Reporting Limit IIFI075 IIF1075 11FI075 IIFI075 IIFI075 IIFI075 IIFI075 IIFI075 IIFI075 IIFI075 IIFI075 IIFI075 IIFI075 11FI075 IIFI075 IIFI075 11FI075 11FI075 11FI075 11FI075 IIFI075 11FI075 IIFI075 11FI075 11FI075 IIFI075 IIFI075 11FI075 11FI075 IIFI075 11FI075 IIFI075 11FI075 IIFI075 IIFI075 11FI075 IIFI075 11FI075 11FI075 IIFI075 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers Reporting Units: ugll '-.. r ,"--'- / EPA 8260B EPA 8260B Bromochloromethane Bromodichloromethane EPA 8260B Bromoform EPA 8260B Bromomethane r . 2-Butanone (MEK) EPA 8260B '--, n-Butylbenzene r'. '-" sec-Butylbenzene EPA 8260B ,. tert-Butylbenzene EPA 8260B '-..j Carbon disulfide EPA 8260B ,r-- Carbon tetrachloride '-...- ,- Chlorobenzene "---/ Chloroethane EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ,---" Chloroform EPA 8260B ::=:.: EPA 8260B '-' ,~/ . . . . . _, ~-, '-/ Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane l,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane '-_" 1,2-Dichlorobenzene 1,3-Dichlorobenzene '--" 1,4-Dichlorobenzene ,. Dichlorodifluoromethane l,l-Dichloroethane 1,2-Dichloroethane '-_ l,l-Dichloroethene cis-l ,2-Dichloroethene '--" trans-I,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane _______ 2,2-Dichloropropane 1,1-Dichloropropene cis-I,3-Dichloropropene trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.8 ND ND ND ND ND ND ND ND ND ND 1.0 ND ND 2.5 ND ND ND ND ND ND ND ND ND ND 6/2912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/2912011 6/2912011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/20 II 6/29/2011 6/29/20 II 612912011 6/29/2011 6/29/20 II 6/29/2011 6129/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/20 II 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/20 II 6/2912011 6/29/2011 6/2912011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6129/2011 6/29/2011 6/29/2011 6/2912011 612912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 TestAmerica Phoenix Carlene McCutcheon Project Manager The resulls perlain only 10 Ihe samples fesfed in fhe laboratory. This report shall nol be reproduced, excepf infulI, wilhoulwriffell permission/rom TestAmerica. PUFl584 ~ ( TestAmerica THE LEAOERIN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454·9303 Project ID: PO #802.1 0 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson . ( Sampled: 06/27111 Received: 06/27/11 Report Number: PUFI584 C C' C C C ( VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Method Analyte Batch Reporting Limit IIFI075 11F1075 11FI075 IIFI075 IIFI075 11FI075 11FI075 IIFI075 IIF1075 11F1075 11FI075 IIFI075 11F1075 IIFI075 IIFI075 IIFI075 11FI075 IIF1075 IIFI075 11FI075 IIFI075 IIFI075 11F1075 11FI075 11FI075 IIF1075 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 Sample Dilution Date Result Factor Extracted Date Analyzed 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 Data Qualifiers Sample!D: PUF1584-07 (11'-7 - Water) - cont. Reporting Units: ugll 2-Hexanone Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl Ether (MTBE) Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane ( C C EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B Tetrachloroethene EPA 8260B Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane EPA 8260B Trichloroethene EPA 8260B Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromofluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND 6.3 ND ND ND ND ND 7.0 ND ND ND ND ND ND ND 112% 103% 96% C ( C ( ( ( C ( ( ( ( ( C (. ( ( C ( ( C ( C ( ( C C ( TestAmerica Phoenix C Carlene McCutcheon Project Manager C The results pertain only 10 the samples tested in the laboratory. This report shall not be reproduced, except in/ul!, without written permissionjrom Tes/America. PUF1584 C ( ( TestAmerica 4625 East Cotton Center Blvd. SIc 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING , '- Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson ,'""- VOLATILE ORGANICS BY GC/MS (EPA S030Bf8260B) Batch Reporting Limit 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 I1FI075 11F1075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11FI075 11F1075 11FI075 11 F1075 11FI075 I1F1075 11 F 1075 I1FI075 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 "" Sampled: 06/27/11 Received: 06/27111 Report Number: PUF1584 Method Analyte Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers '-- Sample ID: PUF1584-08 (W-8 - Water) Reporting Units: ugll Acetone "'" Benzene '. Bromobenzene Bromochloromethane ', Bromodichloromethane "---- Bromoform r Bromomethane r 2-Butanone (MEK) '--- / n-Butylbenzene '- / sec-Butylbenzene r-' tert-Butylbenzene ,----. Carbon disulfide r- Carbon tetrachloride ,. r '---'-./ ,-----, '----.r'-~ "--r· ::< "-..- ~ Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane l,2-Dibromoethane CEDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane l,l-Dichloroethene cis-l,2-Dichloroethene trans-l,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene cis-l,3-Dichloropropene trans-l ,3 -Dichloropropene Ethylbenzene Hexachlorobutadiene EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3.7 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 6/29/2011 6129/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6129/2011 6129/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/2912011 6/29/2011 612912011 6/2912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/2912011 6/2912011 6/2912011 612912011 6/2912011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 612912011 6/29/2011 612912011 6129/2011 6/29/2011 612912011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 612912011 6/29/2011 6129/2011 6/29/2011 612912011 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall nat be reproduced, except infull, without written permissionjrom TestAmerica. PUF1584 \. ( TestAmerica ( THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson C ( Sampled: 06/27111 Received: 06/27/11 Report Number: PUF1584 ( C ( ( VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Analyte Method Batch Reporting Limit 11Fl075 11Fl075 l1Fl075 l1F1075 l1F1075 l1Fl075 l1Fl075 llFl075 llFl075 llFl075 l1Fl075 11F1075 l1Fl075 l1Fl075 l1Fl075 llFl075 llFl075 llFl075 l1Fl075 l1Fl075 l1Fl075 l1Fl075 llFl075 llFl075 llFl075 l1Fl075 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 Sample Dilution Date Result Factor Extracted Date Analyzed 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/2912011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6129/2011 6129/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 612912011 6/2912011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 612912011 6/2912011 6/29/2011 6/29/2011 Data Qualifiers Sample ID: PUFI5S4-0S (W-S - Water) - cont. Reporting Units: ugll 2-Hexanone Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MlBK) Methyl-tert-butyl Ether (MTBE) Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xyienes, Total Surrogate: Dibromofluoromethane (70-130%) Surrogate: Toluene-dB (70-130%) Surrogate: 4-Bromofluorobenzene (70-130%) ( C ( EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B NO NO NO NO NO NO NO NO NO NO NO NO 7.3 NO NO NO NO NO 1.4 NO NO NO NO NO NO NO 112% 105% 95% ( ( C ( C ( C ( C ( ( ( C C C ( ( ( ( ( C C C C C C C C C TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shallllot be reproduced, except inJull, without wriltenpermissionjrom TestAmerica. PUF1584 ( ( ( r , TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Sampled: 06/27111 Received: 06/27111 Report Number: PUF1584 Attention: Joel Peterson VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Method Analyte Batch Reporting Limit IIFI075 IIFI075 llFI075 IIFI075 IIFI075 llFI075 llFI075 llFI075 llFI075 I1FI075 llFI075 llFI075 I1FI075 I1FI075 I1FI075 IIF1075 IIFI075 I1FI075 llF1075 IIF1075 I1FI075 I1F1075 IIF1075 I1FI075 11 F 1075 llFI075 I1FI075 I1F1075 IIFI075 llFI075 llFI075 I1F1075 IIFI075 llFI075 IIF1075 I1FI075 I1F1075 I1FI075 llFI075 llFI075 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers '-- ,- ,r ,- Sample!D: PUFIS84-09 (W-IO - Water) Reporting Units: ugll Acetone Benzene Bromobenzene Bromochloromethane r- Bromodichloromethane "-.. ~ Bromofonn Bromomethane 2-Butanone (MEK) "---- n-Butylbenzene sec-Butylbenzene r tert-Butylbenzene Carbon disulfide Carbon tetrachloride '-Chlorobenzene '--- / Chloroethane EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ".-. Chloroform EPA 8260B :::: "-~ / r, ::- / "---,-, "--/ Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochlorornethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane EPA 8260B '---" ,.- 1,2-Dichlorobenzene 1,3-Dichlorobenzene l,4-Dichlorobenzene Dichlorodifluoromethane 1, I-Dichloroethane 1,2-Dichloroethane EPA 8260B l,l-Dichloroethene cis-l ,2-Dichloroethene EPA 8260B trans l,2-Dichloroethene 1,2-Dichloropropane l,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene cis-l,3-Dichloropropene trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene EPA 8260B r ..../ M "---- EPA 8260B EPA 8260B EPA 8260B . EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3.8 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.62 2.0 ND ND ND ND ND ND ND ND ND 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/2912011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/20 II 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/20 II 6/29/2011 6/29/2011 6/29/20 II 6/29/2011 6/29/20 II 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29120 II 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29120 II 6/29/2011 6/29/2011 6/29/20 II 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/20 II 6/29/2011 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall/lOt be reproduced, except infilll, Wilhout written permissionjrom Tes/America. PUF1584 \,~ ( TestAmerica C THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project JD: PO #802.1 0 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson ( ( Sampled: 06/27/11 Received: 06127111 Report Number: PUFI584 ( C ( C VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Method Analyte Batch Reporting Limit I1FI075 11FI075 11FI075 11FI075 I1FI075 I1FI075 I1FI075 11FI075 11FI075 11FI075 11FI075 I1FI075 11F1075 11FI075 I1FI075 IIFI075 IIFI075 I1FI075 I1F1075 11FI075 I1FI075 I1FI075 I1FI075 I1FI075 11FI075 11FI075 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 Sample Dilution Date Result Factor Extracted Date Analyzed 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/2912011 6129/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 612912011 6/29/2011 Data Qualifiers Sample JD: PUF1584-09 (W-IO - Water) - cont. Reporting Units: ugll 2-Hexanone Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl Ether (MTBE) Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene I, 1,1-Trichloroethane 1,1,2-Trichloroethane TrichIoroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromofluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 82608 EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 82608 EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 82608 EPA 8260B EPA 8260B EPA 8260B ( C ( ND ND ND ND ND ND ND ND ND ND ND ND 3.6 ND ND ND ND ND 14 ND ND ND ND ND ND ND 113% 104% 101 % C ( C ( ( ( C ( C C C ( ( l C C C C ( C C C C C ( ( C C C TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except in/ull, without written permissionjrom TestAlllerica. PUF1584 C ( ( , r r- TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.1 0 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/27111 Received: 06/27111 Report Number: PUF1584 VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Method Analyte r Sample ID: PUF1584-10 (W-ll- Water) Reporting Units: ugIJ Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane '-- Bromoform r ,.r EPA 8260B 1,1-Dichloroethane EPA 8260B l,2-Dichloroethane EPA 8260B I1Fl075 I1Fl075 I1Fl075 l1Fl075 I1Fl075 I1Fl075 I1Fl075 I1Fl075 I1Fl075 I1Fl075 I1Fl075 I1FI075 I1Fl075 IIF1075 l1Fl075 11FI075 I1Fl075 I1FI075 I1Fl075 I1Fl075 11FI075 I1Fl075 I1Fl075 I1FI075 l1Fl075 I1Fl075 I1FI075 l1FI075 I1Fl075 1,1-Dichloroethene cis-l,2-Dichloroethene EPA 8260B 11 F 1075 EPA 8260B trans-l,2-Dichloroethene l,2-Dichloropropane EPA 8260B 1~3-Dichloropropane EPA 8260B 2,2-Dichloropropane' l,l-Dichloropropene cis-l,3-Dichloropropene trans-I,3 -Dichloropropene Ethylbenzene Hexachlorobutadiene EPA 8260B l1FI075 l1Fl075 I1Fl075 I1Fl075 l1Fl075 l1FI075 I1FI075 l1Fl075 I1Fl075 l1F1075 EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B Bromomethane r ' 2-Butanone (MEK) ,--. n-Butylbenzene EPA 8260B "--' sec-Butylbenzene r-' tert-Butylbenzene '-.....-/ Carbon disulfide r Carbon tetrachloride r-· Chlorobenzene "-..--,' Chloroethane EPA 8260B ~- r. EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ~/ r, Batch Chloroform ::_: Chloromethane 2-Chlorotoluene r , 4-Chlorotoluene "- / Dibromochloromethane 1,2-Dibromo-3-chloropropane ~. 1,2-Dibromoethane (EDB) '-......--' Dibromomethane 1,2-Dichlorobenzene '1,3-Dichlorobenzene 1A-Dichlorobenzene Dichlorodifluoromethane EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B Reporting Limit 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 Sample Dilution Date Result Factor Extracted ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.9 ND ND ND ND ND ND ND ND ND ND ND 1.1 ND 2.2 4.4 ND ND ND ND ND ND ND ND ND 6/2912011 6/29/2011 6/29/2011 6/29120 II 6129/2011 612912011 6/2912011 6/29/2011 612912011 6/2912011 612912011 612912011 6/2912011 612912011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/201 I 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 Date Analyzed Data Qualifiers 6129/2011 6/29/2011 6/29/2011 6129120 I 1 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/201 I 6/2912011 6/2912011 612912011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 612912011 612912011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertahl only to the samples tested in the laboratory. This report shall not be reproduc~d, except inJull, withol/twrillen pennissionji"om TestAmerica. PUF1584 \~~ ( TestAmerica ( THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437~3340 Fax:(602) 454-9303 Project 1D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson C VOLATILE ORGANICS BY GCIMS (EPA 5030Bf8260B) Analyte Method Batch Reporting Limit IIFI075 IIF1075 IIFI075 11FI075 11FI075 11FI075 IIFI075 IIF1075 IIFI075 IIFI075 11FI075 11FI075 IIF1075 11FI075 IIFI075 IIFI075 IIF1075 11FI075 11FI075 IIFI075 IIFI075 IIFI075 IIFI075 IIF1075 IIFI075 11FI075 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 Date Sample Dilution Result Factor Extracted Date Analyzed 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6/2912011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 Data Qualifiers Sample ID: PUF1584-10 (W-ll- Water) - cont. Reporting Units: ugll 2-Hexanone Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl Ether (MTBE) Naphthalene n-Propylbenzene Styrene l,l,l,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,S-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromofluoromethane (70-130%) Surrogate: Toluene-dS (70-130%) Surrogate: 4-Bromofluorobenzene (70-130%) EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 82608 EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ( ( ( ( Sampled: 06/27111 Received: 06/27111 Report Number: PUFI584 C C C ( ND ND ND ND ND ND ND ND ND ND ND ND 3.2 ND ND ND ND ND 27 ND ND ND ND ND ND ND 113% 101 % 97% ( ( C ( ( ( ( ',-- ( C ( C ( C ( C ( C ( ( ( C C C C C C C TestAmerica Phoenix ~ \. c Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except inJull, withoutwrittenpermissionjrom TestAmerica. PUFI584 ( ( ( r TestAmerica 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/27/11 Received: 06/27111 Report Number: PUFI584 VOLATILE ORGANICS BY GC/MS (EPA 5030B/S260B) Reporting Method Analyte r Benzene Bromobenzene Bromochloromethane EPA 8260B EPA 8260B EPA 8260B EPA 8260B r Bromodichloromethane EPA 8260B '- ~ EPA 8260B ,----' Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane r-, Chloroform EPA 8260B :::~ Chloromethane '--' 2-Chlorotoluene 4-Chlorotoluene EPA 8260B r '---r. '-' -------,,---- EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ,---" Dibromochloromethane EPA 8260B ,,---' 1,2-Dibromo-3-chloropropane 1,2-0ibromoethane (EOB) ,--/ Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,I-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene EPA 8260B .... , Limit 11F1112 11F1112 11FI112 11F1112 11Fl112 11F1112 11F1112 11F1112 11F1112 11F1112 11FI112 llFll12 11F1112 llF1112 11F1112 11F1112 11F1112 llFI112 11F1112 11F1112 11F1112 11F1112 11F1112 11FlI12 11FlI12 11FI112 11F1112 11F1112 lIFI112 I1FlI12 lIFll12 11F1112 11FlI12 11F1112 11F1112 11F1112 11F1112 11F1112 11FI112 11F1112 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers Sample ID: PUF1584-1l (W-22 - Water) Reporting Units: ugll Acetone r. Batch EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B cis-l,2-Dichloroethene EPA 8260B trans-l,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-l,3-Dichloropropene trans-I,3-Dichloropropene Ethylbenzene Hexachlorobutadiene EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B NO NO NO NO 1.7 NO NO NO NO NO NO NO NO NO NO 3.0 NO NO NO 0.70 NO NO NO NO NO NO NO NO NO NO 0_74 NO NO NO NO NO NO NO NO NO 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shal/ll01 be reproduced, except infull, wirhoutwrillenpermission!i"om TestAmerica. PUF1584 TestAmerica ( THE LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project 10: PO #802.10 June 2011 Sampled: 06/27/11 Received: 06/27/11 Report Number: PUFI584 ( ( ( VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Method Sample ID: PUFIS84-1l (W-22 - Water) - cont. Reporting Units: ugll EPA 8260B 2-Hexanone EPA 8260B Iodomethane EPA 8260B Isopropylbenzene EPA 8260B p-Isopropyltoluene EPA 8260B Methylene Chloride EPA 8260B 4-Methyl-2-pentanone (MIBK) EPA 8260B Methyl-tert-butyl Ether (MTBE) EPA 8260B Naphthalene EPA 8260B n-Propylbenzene EPA 8260B Styrene EPA 8260B 1,1,1,2-Tetrachloroethane EPA 8260B 1,1,2,2-Tetrachloroethane EPA 8260B Tetrachloroethene EPA 8260B Toluene EPA 8260B 1,2,3-Trichlorobenzene EPA 8260B 1,2,4~ Trichlorobenzene EPA 8260B 1,1, 1~Trichloroethane EPA 8260B 1,1 ,2~Trichloroethane EPA 8260B Trichloroethene EPA 8260B Trichlorofluoromethane EPA 8260B 1,2,3-Trichloropropane EPA 8260B 1,2,4-Trimethylbenzene EPA 8260B 1,3,5-Trimethylbenzene EPA 8260B Vinyl Acetate EPA 8260B Vinyl chloride EPA 8260B Xylenes, Total Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-dB (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) Batch Reporting Limit c c c Date Sample Dilution Result Factor Extracted Date Analyzed Data Qualifiers ( ( '-- ( IIFII12 11FIII2 11F1112 11Fl112 IIFl112 IIFl112 IIFl112 11Fl112 11F11I2 IIFIl12 IIFII12 IIFII12 IIFII12 IIFl112 IIFII12 IIFI1I2 IIFI112 IIFII12 IIFII12 IIFII12 IIFII12 IIFIII2 IIFIII2 IIFI1I2 IIFI1I2 llFII12 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 ND ND ND ND ND ND ND ND ND ND ND ND 1.9 ND ND ND ND ND 4.2 ND ND ND ND ND ND ND 110% 103% 101 % I I 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 C ( C ( ( ( ( ( ( ( ( M2 ( ( ( ( ( C ( ( C ( C C C ( ( ( TestAmerica Phoenix ( Carlene McCutcheon Project Manager C The results pertain only /0 the samples tested in the laboratory. This report shallllot be reproduced, except illfull, without writtenpermissiolljrol1l TestAmerica. PUFl584 ( ( ( TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. SIc 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/27/11 Received: 06/27/11 Report Number: PUFI584 VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte r ..-- ,-- Method Reporting Limit Sample Dilution Date Result Factor Extracted Date Analyzed 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 Data Qualifiers Sample ID: PUF1584-12 (W-19 - Water) Reporting Units: ugll Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromofonn EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ,---' Bromomethane r . 2-Butanone (MEK) n-Butylbenzene EPA 8260B "---' sec-Butylbenzene tert-Butylbenzene Carbon disulfide r ' Carbon tetrachloride EPA 8260B ,- Chlorobenzene '-.--/ Chloroethane ,'. Chloroform EPA 8260B r. v EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B Chloromethane 2-Chlorotoluene ..--. 4-Chlorotoluene '-- / Dibromochloromethane EPA 8260B 1,2-Dibromo-3-chloropropane ~. 1,2-Dibromoethane (EDB) ,--" Dibromomethane EPA 8260B 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane EPA 8260B r--, ...../ Batch EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B l,l-Dichloroethane EPA 8260B 1,2-Dichloroethane EPA 8260B l,l-Dichloroethene cis-l,2-Dichloroethene EPA 8260B trans-I,2-Dichloroethene l,2-Dichloropropane l,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene cis-l,3-Dichloropropene trans-l ,3-Dichloropropene Ethylbenzene Hexachlorobutadiene EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B 11F1112 11F1112 11F1112 IIFII12 11F1112 IIF1112 IIFII12 IIF1112 IIFI112 IIF1112 IIFI112 11F1112 11F1112 11F1112 11F1112 IIFI112 11F1112 11F1112 11F1112 11F1112 IIFII12 11F1112 11F1112 IIF1112 IIF1112 IIFII12 IIF1112 11F1ll2 IIF1112 11F1112 11F1112 IIFII12 IIF1112 11F1112 IIF1112 IIFI112 IIFII12 IIF1112 IIFII12 IIFII12 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.2 ND ND ND ND ND ND ND ND ND ND ND 0.62 ND 1.5 2.2 ND ND ND ND ND ND ND ND ND TestAmerica Phoenix Carlene McCutcheon Project Manager The resul/s pertain only /0 the samples tested in the laboratory. This repor' shall I/ot be reproduced, except in/ull, without wrillenpermissionjrom TestAmerico. PUF1584 \.. ( TestAmerica C THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437·3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/27111 Received: 06/27111 Report Number: PUF1584 C c c c c ( VOLATILE ORGANICS BY GC/MS (EPA 5030B/S260B) Method Analyte Sample ID: PUFI584-12 (W-19 - Water) - cont. Reporting Units: ug/l EPA 8260B 2-Hexanone EPA 8260B Iodomethane EPA 8260B Isopropylbenzene EPA 8260B p-Isopropyltoluene EPA 8260B Methylene Chloride EPA 8260B 4-Methyl-2-pentanone (MIBK) EPA 8260B Methyl-tert-butyl Ether (MTBE) EPA 8260B Naphthalene EPA 8260B n-Propylbenzene EPA 8260B Styrene EPA 8260B 1,1,1,2-Tetrachloroethane EPA 8260B 1,1,2,2-Tetrachloroethane Tetrachloroethene EPA 8260B Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene l,l,l-Trichloroethane I, I ,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) EPA 8260B EPA 8260B EPA 8260B EPA 82608 EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 82608 Batch Reporting Limit l1F1112 11FI112 11F1112 11Fl112 llFl112 11F1112 l1F1112 l1F1112 l1FI112 11F1112 llF1112 llFl112 l1F1112 llF1112 l1F1112 l1F1112 l1FI112 llFI112 llFII12 llFl112 l1F1112 l1F1112 11F1112 l1F1112 llFI112 llFI112 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 Sample Dilution Date Result Factor Extracted Date Analyzed 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/3012011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 ND ND ND ND ND ND ND ND ND ND ND ND 5.9 ND ND ND ND ND 14 ND ND ND ND ND ND ND Data Qualifiers 111% 105% 98% c c c c ( c ( ( ( ( ( C ( C ( ( C ( ( r ( c c c c c c c c c c TestAmerica Phoenix Carlene McCutcheon ( Project Manager The results pertain only to the samples tested in the laboratOJY. This report shall not be reproduced, except infull, without writtenpermissionji-om TestAmerica. PUFl584 ( C ( r TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 1064S N. Tatum Blvd., Suite 200-437 Phoenix, AZ 8S028 Attention: Joel Peterson Sampled: 06/27111 Received: 06/27111 Report Number: PUF1S84 VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Method Analyte r Batch Reporting Limit Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers Sample!D: PUF1584-13 (W-12 - Water) Reporting Units: ugll '-__ Acetone r 'r '-r. ... -~ r, Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone CMEK) n-Butylbenzene '--. sec-Butylbenzene r-·, tert-Butylbenzene ,--/ Carbon disulfide .-- Carbon tetrachloride Chlorohenzene Chloroethane r-, Chloroform ~ Chloromethane 2-Chlorotoluene 4-Chlorotoluene "---' Dibromochloromethane '. 1,2-Di bromo-3-chloropropane 1,2-Dibromoethane CEDB) ,,-/ Dibromomethane "- ~ 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane l,l-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene ~ cis-I,2-Dichloroethene trans-I,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene cis-l,3-Dichloropropene trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B 11Fl0S0 l1Fl0S0 l1Fl0S0 11Fl0S0 l1Fl0S0 l1Fl0S0 11Fl0S0 11Fl0S0 l1Fl0S0 11Fl0S0 11Fl0S0 11Fl0S0 11Fl0S0 11Fl0S0 l1Fl0S0 l1F1OS0 11Fl0S0 11Fl0S0 11Fl0S0 11Fl0S0 11Fl0S0 l1Fl0S0 11Fl0S0 11Fl0S0 l1Fl0S0 11Fl0S0 l1Fl0S0 llFIOSO l1Fl0S0 11Fl0S0 l1Fl0S0 l1F1OS0 l1Fl0S0 l1F1OS0 l1Fl0S0 l1Fl0S0 11Fl0S0 11Fl0S0 11Fl0S0 11Fl0S0 10 O.SO O.SO O.SO O.SO 1.0 1.0 2.S O.SO O.SO O.SO O.SO O.SO O.SO 1.0 O.SO 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 O.SO 0.50 O.SO O.SO O.SO O.SO O.SO O.SO 1.0 0.50 0.50 0.50 0.50 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.61 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.88 ND ND ND ND ND ND ND ND ND ND 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/20 II 6/29/2011' 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 L3 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except inJull, withoutwrittenpennissionji"om TestAmerica. PUFI584 ~. C TestAmerica C 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 1064S N. Tatum Blvd., Suite 200-437 Phoenix, AZ 8S028 Attention: Joel Peterson Sampled: 06/27/11 Received: 06/27111 Report Number: PUF1S84 ( C C C c ( VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Method Batch Reporting Limit 11F10S0 11F10S0 2.S 2.S 11F10S0 11F10S0 11F10S0 11F10S0 0.50 0.50 1.0 2.5 11F10S0 11F10S0 11F10S0 O.SO 2.S O.SO 11F10S0 11FlOS0 11F10S0 11F10S0 O.SO O.SO O.SO O.SO 11FlOS0 11F10S0 0.50 1.0 11F10S0 11F10S0 11F10S0 11F10S0 1.0 O.SO O.SO Date Date Sample Dilution Result Factor Extracted Analyzed 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6129/2011 612912011 612912011 6/29/2011 6/2912011 6/2912011 612912011 6/29/2011 612912011 6/29/2011 6/29/2011 6/2912011 6/2912011 6/29/2011 Data Qualifiers Samp1e!D: PUF1584-13 (W-12 - Water) - cont. Reporting Units: ugll 2-Hexanone EPA 8260B EPA 8260B EPA 8260B Iodomethane Isopropylbenzene p-Isopropyltoluene EPA 8260B EPA 8260B Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methy1-tert-buty1 Ether (MTBE) Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 82608 Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) EPA 82608 EPA 8260B EPA 8260B EPA 82608 EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 82608 EPA 8260B EPA 8260B EPA 8260B EPA 8260B ( C ( 11F10S0 11FlOS0 11FlOS0 11F10S0 11F10S0 llF10S0 11F10S0 O.SO O.SO 1.0 0.50 0.50 1.0 O.SO 1.5 ND ND ND ND ND ND ND ND ND ND ND ND 9.7 ND ND ND ND ND 1.4 ND ND ND ND ND ND ND ( ( C ( ( ( ( ( C ( C ( C ( C ( C 102% , 98% 96% c c c c ( c ( ( ( C TestAmerica Phoenix C Carlene McCutcheon ( Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except injull, without writlenpermissionjrom TestAmerica. PUF1584 ( ( ( r TestAmerica THE LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Sampled: 06/27111 Received: 06/27111 Report Number: PUF1584 VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Method Batch Reporting Limit llFl050 l1Fl050 llF1050 l1Fl050 11Fl050 llFl050 llFl050 llFl050 11F1050 l1Fl050 l1F1050 11F1050 11F1050 l1Fl050 11F1050 11Fl050 l1F1050 l1Fl050 l1Fl050 l1F1050 l1Fl050 l1F1050 l1Fl050 l1F1050 l1F1050 l1F1050 l1Fl050 11Fl050 l1Fl050 11Fl050 11F1050 l1F1050 l1F1050 11F1050 l1F1050 11Fl050 l1F1050 l1Fl050 l1F1050 l1F1050 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 Sample Dilution Date Result Factor Extracted Date Analyzed 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 612912011 6/29/2011 6/29/2011 612912011 612912011 6/29/2011 612912011 612912011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 612912011 6/29/2011 612912011 6/29/2011 6/29/2011 612912011 612912011 6/29/2011 612912011 612912011 6/29/2011 612912011 6/29/2011 6/2912011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6129/2011 6/29/2011 612912011 6/29/2011 Data Qualifiers '- '- ~' ---/ r. ---./ ~ ..---~, '--, '--., Sample ID: PUF1S84-14 (Duplicate A - Water) Reporting Units: ug/l EPA 8260B Acetone EPA 8260B Benzene EPA 8260B Bromobenzene EPA 8260B Bromochloromethane EPA 8260B Bromodichloromethane EPA 8260B Bromoform EPA 8260B Brornomethane EPA 8260B 2-Butanone (MEK) EPA 8260B n-Butylbenzene EPA 8260B sec-Butylbenzene EPA 8260B tert-Butylbenzene EPA 8260B Carbon disulfide EPA 8260B Carbon tetrachloride EPA 8260B Chlorobenzene EPA 8260B Chloroethane Chloroform EPA 8260B ~ '--, Chloromethane ,_j 2-Chlorotoluene '--, 4-Chlorotoluene '- / Dibromochloromethane ___ .' 1,2-Dibromo-3-chloropfopane r,. 1,2-Dibromoethane (EDB) ---/ Dibromomethane r, 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1A-Dichlorobenzene Dichlorodifluoromethane l,l-Dichloroethane 1,2-Dichloroethane l,l-Dichloroethene cis-l,2-Dichloroethene --_/ trans-I,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene cis-l,3-Dichloropropene trans-l ,3-Dichloropropene Ethylbenzene Hexachlorobutadiene EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.2 ND ND ND ND ND ND ND ND ND ND ND 0.63 ND 1.7 2.4 ND ND ND ND ND ND ND ND ND L3 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertaill olily to the samples tested in the laboratory. This report shallllot be reproduced, except iliJull, without wrilten permission!rom TestAmerica. PUFl584 ~ ( ( TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 ProjectlD: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 8S028 Attention: Joel Peterson ... ( ( Sampled: 06/27111 Received: 06/27111 Report Number: PUFI584 ( ( ( C VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Method Analyte Batch Reporting Limit 11FI050 11FIOSO IIF\050 IIF\050 IIFI050 IIFIOSO IIFIOSO 11FIOSO 11F\050 IIF\050 IIFI050 IIFI050 IIFI050 IIFIOSO 11FIOSO IIF\050 IIF\050 11FI050 IIF\050 IIFlO50 IIFIOSO IIFI050 IIFI050 11FI050 11FIOSO IIFIOSO 2.S 2.5 0.50 0.50 1.0 2.S 0.50 2.5 0.50 0.50 0.50 O.SO O.SO O.SO 1.0 1.0 0.50 0.50 O.SO 0.50 1.0 0.50 0.50 1.0 O.SO I.S Sample Dilution Date Result Factor Extracted Date Analyzed 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6129/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/2912011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/29/2011 612912011 6/29/2011 6/29/2011 6/2912011 6/2912011 6/29/2011 6129/2011 Data Qualifiers Sample ID: PUF1584-14 (Duplicate A - Water) - cont. Reporting Units: ug/l 2-Hexanone Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl Ether (MTBE) Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND 6.0 ND ND ND ND ND 14 ND ND ND ND ND ND ND 104% 98% 93% ( ( ( C ( C ( ( ( C ( ( ( ( ( C C C C C ( C ( ( ( C ( C C ( TestAmerica Phoenix ( Carlene McCutcheon ( Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except infull, without wrillen permission/rom TestAmerica. PUF1584 ( ( ( , TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/27111 Received: 06/27111 Report Number: PUFI584 METHOD BLANKlQC DATA , VOLATILE ORGANICS BY GCIMS (EPA S030B/8260B) . Analyte Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: 11FI050 Extracted: 06/29/11 Blank Analyzed: 06/29/2011 (I1FI050-BLKl) NO Acetone ND Benzene ND Bromobenzene NO Bromochloromethane ND Bromodichloromethane Bromoform ND Bromomethane NO 2-Butanone (MEK) ND n-Butylbenzene ND sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride NO ND ND ND Chlorobenzene ND Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane l,2-Dichlorobenzene 1,3-Dichlorobenzene NO NO 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1, J-Dichloroethene cis-l,2-Dichloroethene trans- I ,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane ND NO NO ND NO NO ND NO ND ND NO ND NO ND NO NO NO ND NO 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll TestAmerica Phoenix Carlene McCutcheon Project Manager The res/llts pertain only (0 the samples tested;n the laboratory. This reporl shallllot be reproduced, except infull. without writtenpermission!ram TestAmerica. PUFl584 \. C C TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson C ( Sampled: 06/27111 Received: 06/27111 Report Number: PUF1584 ( C ( C MEitb'n BLA~KlQC DATA ( ( VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC ( %REC Limits RPD RPD Limit Data Qualifiers Batch: IIFIOSO Extracted: 06/29/11 ( ( Blank Analyzed: 06/29/2011 (llFIOSO-BLKl) l,l-Dichloropropcnc ND 0.50 cis-J ,3-Dichloropropene trans-l ,3-Dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone Iodomethane Isopropy Ibenzene p-Isopropyltoluene ND 0.50 ND 0.50 ND ND 0.50 ND 2.5 1.0 ND 2.5 ND ND 0.50 0.50 Methylene Chloride ND 1.0 4-Methyl-2-pentanone (MIBK) ND 2.5 Methyl-tert-butyl Ether (MTBE) ND 0.50 Naphthalene ND 2.5 n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trich loropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total ND ND 0.50 0.50 ND 0.50 ND 0.50 ND ND 0.50 ND 1.0 ND 1.0 ND 0.50 ND 0.50 ND ND 0.50 ND 1.0 0.50 0.50 ND 0.50 ND 0.50 ND 1.0 ND 0.50 ND 1.5 ( ( ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ( ( C ( C ( ( ( ( C C ( ( ( C C C C ( Surrogate: Dibromojluoromethane 23.9 ugll 25.0 96 70-130 Surrogate: Toluene-dB 24.8 ugll 25.0 99 70-130 Surrogate: 4-Bromojluorobenzene 24.4 ugll 25.0 98 70-130 ( ( C C TestAmerica Phoenix ( Carlene McCutcheon ( Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except infull, without writlenpennissionFom restAmerica. PUF1584 ( ( ( l , TestAmerica THE LEADER IN ENVIRONMENTAL TESTING Project!D: PO #802.10 June 2011 Synergy Environmental, LLC " 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437·3340 Fax:(602) 454-9303 10645 N. Tatum Blvd., Suite 200-437 Sampled: 06/27111 Phoenix, AZ 85028 Report Number: PUFI584 Received: 06/27111 Attention: Joel Peterson METHOD BLANKlQC DATA VOLATILE ORGANICS BY GCfMS (EPA 5030B/8260B) Analyte Result " Batch: 11FI050 Extracted: 06/29/11 r '-. LCS Analyzed: 06/29/2011 (l1FI050-BSl) r' Acetone ,--,' Benzene r', Bromobenzene "-----Bromochloromethane ~ '-_/ Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene Reporting Limit 32.4 10 24.8 0.50 23.2 0.50 25.0 Spike Units Level Source Result %REC %REC Limits RPD 25.0 130 30-150 25.0 99 70-130 25.0 93 70-130 0.50 ugll ugll ugll ugll 25.0 100 70·130 26.0 0.50 ugll 25.0 104 70-130 23.0 1.0 ugll 25.0 92 67-122 25.0 101 64-132 25.0 125 48-150 25.2 1.0 31.3 2.5 29.0 0.50 ugll ugll ugll 25.0 116 70-130 28.0 0.50 ugll 25.0 112 70-130 26.4 0.50 25.0 106 70-130 30.6 0.50 25.0 122 61-126 25.0 106 70-130 25.0 97 70-130 105 69-128 '--- Carbon tetrachloride 26.4 0.50 r Chlorobenzene Chloroethane 24.3 0.50 ugll ugll ugll ugll 26.1 1.0 ugll 25.0 "-- - Chlorofonn 24.6 0.50 ugll 25.0 98 70-130 Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane "- l,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane '----- 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane I,l-Dichloroethane 1,2-Dichloroethane '---~ I,l-Dichloroethene cis-l,2-Dichloroethene trans-l,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 26.2 1.0 ugll 25.0 105 56-131 70-130 '- tert-Butylbenzene .--, Carbon disulfide r 24.8 0.50 ugll 25.0 99 25.7 0.50 ugll 25.0 103 70-130 26.4 0.50 25.0 105 70-130 25.8 2.5 ugll ugll 25.0 103 63-129 24.7 0.50 ugll 25.0 99 70-130 25.2 0.50 25.0 101 70-130 25.5 0.50 25.0 102 70-130 24.6 0.50 25.0 98 70-130 24.8 0.50 25.0 99 70-130 27.5 0.50 25.0 110 42-150 24.8 0.50 25.0 99 70-130 25.8 0.50 25.0 103 72-133 26.1 0.50 25.0 104 70-130 24.6 0.50 25.0 98 70-130 25.0 0.50 25.0 100 70-130 23.6 0.50 25.0 94 70-130 22.9 0.50 25.0 92 70-130 26.5 1.0 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 25.0 106 70-130 RPD Limit Data Qualifiers TestAmerica Phoenix Carlene McCutcheon Project Manager The resulJs pertain ollly to the samples tested in the laboratory. This report shallllot be reproduced. except infull, withour wrirtell permission from TestAmerica. PUFl584 \ ( TestAmerica TI-IE LEADER ( IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 10645 N. Tatum Blvd., Suite 200-437 Report Number: PUFI584 ( Received: 06127111 Attention: Joel Peterson ( --- - C --~'1!8: ~:);HOD BLANKlQC DATA:ki8' ( C VOLATILE ORGANICS BY GelMS (EPA 5030B/8260B) Result Analyte Reporting Limit Units Spike Level Source Result %REC ( %REC Limits RPD RPD Limit Data Qualifiers Batch: llFI050 Extracted: 06/29/11 C ( C LCS Analyzed: 06/29/2011 (l1FI050-BSI) 1,1-Dichloropropene cis-} ,3-Dichloropropene 24.9 0.50 ugll 25.0 100 70-130 26.6 0.50 ugll 2S.0 107 70-130 trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene 27.2 0.50 ugll 25.0 109 70-130 27.7 0.50 ugll 25.0 111 70-130 26.4 1.0 ugll 25.0 106 70-130 31.9 2.5 ugll 2S.0 128 44-1 SO 28.8 2.5 ugll 2S.0 lIS 58-138 26.9 O.SO ugll 25.0 108 70-130 p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl Ether (MTBE) Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1, 1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trich lorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trich loroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total 28.9 0.50 ugll 2S.0 116 70-130 70-130 Surrogate: Dibromojluoromethane 24.9 Surrogate: Toluene-dB Surrogate: 4-Bromojluorobenzene 2-Hexanone Iodomethane Isopropylbenzene ( ( Sampled: 06/27111 Phoenix, AZ 85028 ( ( C ( ( ( C ( 24.8 1.0 ugll 2S.0 99 30.3 2.S ugll 25.0 121 61-142 22.2 0.50 ugll 25.0 89 70-130 27.6 2.5 ugll 25.0 110 65-129 ( 27.8 O.SO ugll 25.0 III 70-130 27.4 O.SO ugll 25.0 110 70-130 24.6 0.50 ugll 2S.0 98 70-130 19.8 0.50 ugll 2S.0 79 70-130 24.5 0.50 ugll 25.0 98 70-130 C C C 26.4 0.50 ugll 2S.0 106 70-130 ( 28.S 1.0 ugll 25.0 114 70-130 27.2 1.0 ugll 25.0 109 70-130 C 25.6 0.50 ugll 2S.0 102 70-130 ( 25.0 0.50 ugll 2S.0 100 70-130 25.0 O.SO ugll 25.0 100 70-130 ( 29.2 0.50 ugll 25.0 117 78-149 ( 22.6 1.0 ugll 25.0 90 70-130 28.0 0.50 ugll 25.0 112 70-130 C 27.3 0.50 ugll 25.0 109 70-130 ( 24.1 1.0 ugll 25.0 96 57-149 28.1 0.50 ugll 2S.0 112 66-134 54.3 I.S ugll 50.0 109 70-130 ugll 25.0 100 70-130 25.6 ugll 25.0 102 70-130 26.8 ugll 25.0 107 70-130 ( ( C ( C C TestAmerica Phoenix C Carlene McCutcheon Project Manager ( The results pertain only to the samples tested in the laboratory. This report shallllot be reproduced, except illfull, withoul writlenpermissiollfrom TestAmerica. PUF1584 ( ( ( ( TestAmerica THE LEADER IN ENVIRONMENTAL TESTING Project ID: PO #802.10 June 2011 Synergy Environmental, LLC ( 10645 N. Tatum Blvd., Suite 200-437 \ Phoenix, AZ 85028 ( Attention: Joel Peterson 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Sampled: 06127111 Received: 06/27111 Report Number: PUF1584 ( METHOD BLANKlQC DATA VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Analyte , Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: 11F1050 Extracted: 06/29/11 LCS Dup Analyzed: 06/29/2011 (l1FI050-BSDI) , , '- , ,- Acetone 33.4 10 ugll 25.0 134 30-150 3 35 Benzene 25.4 0.50 ugll 25.0 102 70-130 3 20 Bromobenzene Bromochloromethane 23.8 0.50 25.0 95 70-130 3 20 24.5 0.50 ugll ugll 25.0 98 70-130 2 20 Bromodichloromethane 26.1 0.50 ugll 25.0 104 70-130 0.4 20 Bromoform Bromomethane 23.1 1.0 25.0 92 67-122 0.7 20 26.0 1.0 25.0 104 64-132 3 20 2-Butanone (MEK) 30.9 2.5 25.0 123 48-150 I 33 n-Butylbenzene 28.2 0.50 25.0 113 70-130 2 20 20 sec-Butylbenzene 28.1 0.50 ugll ugll ugll ugll ugll 25.0 112 70-130 0.4 tert-Butylbenzene 26.5 0.50 ugll 25.0 106 70-130 0.3 20 Carbon disulfide 32.8 0.50 ugll 25.0 131 61-126 7 20 Carbon tetrachloride 27.1 0.50 ugll 25.0 108 70-130 2 20 3 20 Chlorobenzene 25.1 0.50 ugll 25.0 100 70-130 Chloroethane 26.4 1.0 ugll 25.0 106 69-128 20 Chloroform 24.9 0.50 ugll 25.0 100 70-130 20 Chloromethane 25.8 1.0 ugll 25.0 56-13 I 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane I ,2-Dibromo-3-chloropropane 25.7 0.50 ugll 25.0 103 103 70-130 4 20 26.6 0.50 ugll 25.0 106 70-130 3 20 26.4 0.50 ugll 25.0 105 70-130 o 20 2.5 ugll 25.0 99 63-129 5 25 0.50 ugll 25.0 98 70-130 0.9 20 Dibromomethane 24.6 24.5 24.3 0.50 ugll 25.0 97 70-130 4 20 1,2-Dichlorobenzene 25.5 0.50 25.0 102 70-130 0.1 20 1,3-Dichlorobenzene 25.0 0.50 25.0 100 70-130 2 20 1,4-Dichlorobenzene 25.0 0.50 25.0 100 70-130 Dichlorodifluoromethane 27.9 0.50 25.0 112 42-150 I 20 l,l-Dichloroethane 25.4 0.50 25.0 102 70-130 2 20 1,2-Dichloroethane 25.0 0.50 25.0 100 72-133 3 20 l,l-Dichloroethene 26.6 0.50 25.0 106 70-130 2 cis-l,2-Dichloroethene 24.9 0.50 ugll ugll ugll ugll ugll ugll ugll ugll 25.0 99 70-130 I 20 20 trans-l,2-Dichloroethene 25.9 0.50 ugll 25.0 103 70-130 3 20 1,2-Dichloropropanc 23.5 0.50 ugll 25.0 94 70-130 0.3 20 1,3-Dichloropropane 22.7 0.50 ugll 25.0 91 70-130 I 2,2-Dichloropropane 26.6 1.0 ugll 25.0 106 70-130 0.1 20 20 1,2-Dibromoethane (EDB) L3 20 20 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shalf not be reproduced, except inflllf, without wrilfen permissionjiYJm TesrAmerica. PUF1584 \_. ( TestAmerica THE LEADER ( ',", IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Synergy Environmental, LLC Project!D: PO #802.\0 June 2011 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 c Attention: Joel Peterson ( c METHOD B~~l#Q0J)ATA A, " ' " , ' ; j ,0>::~, / ," G',"'>:;0b, __"0~b~~~~00 ___ ( . c VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC ( %REC Limits RPD RPD Limit Data Qualifiers Batch: llFlOSO Extracted: 06/29/11 Les Dup Analyzed: 06/29/2011 (l1FI050-BSDl) l,l-Dichloropropene cis-J ,3-Dichloropropene trans-],3 -Dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone Iodomethane Isopropylbenzene p·Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl Ether (MTBE) Naphthalene n-Propylbenzene Styrene I, I, 1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromojluoromethane Surrogate: Toluene-d8 Surrogate: 4-Bromojluorobenzene ( ( Sampled: 06/27/11 Received: 06/27111 Report Number: PUFI584 c 25.7 26.4 26.2 28.4 26.4 32.6 29.0 27.9 28.8 25.1 27.9 20.0 25.1 28.5 26.8 25.3 19.5 25.5 26.6 26.7 26.0 26.1 23.9 25.8 30.4 21.8 28.1 27.7 21.7 28.3 54.9 0.50 0.50 0.50 0.50 1.0 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil 24.7 ugll 25.3 ugll 26.4 ugll 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 50.0 25.0 25.0 25.0 103 106 105 114 105 130 116 112 115 100 III 80 101 114 70-130 70-130 70-130 70-130 70-130 44-150 58-138 70-130 70-130 70-130 61-142 70-130 65-129 70-130 107 70-130 101 78 102 106 107 104 104 96 103 122 87 113 III 87 113 110 99 101 106 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 78-149 70-130 70-130 70-130 57-149 66-134 70-130 70-130 70-130 70-130 0.7 4 0.5 0.9 20 20 20 20 20 31 25 20 20 20 8 22 II 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 21 20 20 3 0.9 4 3 0.3 2 9 2 2 3 2 4 0.7 6 5 2 4 3 4 4 0.7 II 0.8 c ( ( ( c ( c ( ( ( ( ( c c c ( c ( ( ( ( ( ( c c c c c TestAmerica Phoenix Carlene McCutcheon Project Manager l1,e results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except inJull, wilhoutwrittenpermissionJrom TestAmerica. PUFl584 ( ( ( ( TestAmerica ,- THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC Sampled: 06/27111 Received: 06/27111 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 ," Report Number: PUFI584 Attention: Joel Peterson r '- r METHOD BLANKlQC DATA ,\.. VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) 'r ,'-'-( '- Result Analyte Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers , - Batch: IIF10SO Extracted: 06/29/11 ,-c... '-- Matrix Spike Analyzed: 06/29/2011 (llFIOSO-MSl) 17.8 Source: PUFlS7S-11 ND 71 10-150 ~~. Benzene 25.4 0.50 ugll ugll 25.0 ND 101 70-130 r". 8romobenzene 24.2 0.50 ugll 25.0 ND 97 70-130 1......../ Bromochloromethane r-" 24.2 0.50 25.0 ND 97 70-130 L" Bromodichloromethane 25.1 0.50 ugll ugll 25.0 ND 100 70-130 Bromoform L- Bromomethane ,.-- 20.S 1.0 ugll 25.0 ND 83 62-126 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 25.0 ND 104 55-136 25.0 ND 93 22-150 25.0 ND liS 70-130 25.0 ND 119 70-130 25.0 ND 112 70-130 25.0 ND 86 56-132 25.0 ND 108 76-131 25.0 ND 99 70-130 25.0 ND 105 67-134 25.0 0.220 99 70-130 25.0 ND 101 50-135 25.0 ND 103 70-130 25.0 ND 107 70-130 25.0 ND 97 70-130 25.0 ND 94 60-135 25.0 ND 94 70-130 25.0 ND 95 70-130 25.0 ND 102 70-130 25.0 ND 101 70-130 25.0 ND 100 70-130 25.0 ND 112 36-150 25.0 ND 102 70-130 25.0 ND 98 68-143 25.0 ND 106 70-130 25.0 ND 100 70-130 25.0 ND 103 70-130 25.0 ND 93 70-130 25.0 ND 88 70-130 25.0 ND 112 66-130 (_ Acetone r 10 26.0 1.0 L 2-Butanone (MEK) 23.3 2.5 ,-- n-Butylbenzene 29.6 0.50 sec-Butylbenzene 29.7 0.50 ....._./ tert-Butylbenzene 27.9 0.50 r- Carbon disulfide 21.4 0.50 ,,----.- Carbon tetrachloride 26.9 0.50 r'-.r Chlorobenzene 24.8 0.50 Chloroethane 26.3 1.0 '-- Chloroform 25.0 0.50 r- Chloromethane 25.3 1.0 r 2-Chlorotoluene 25.9 0.50 I....... 4-Chlorotoluene 26.9 0.50 Dibromochloromethane 24.2 0.50 1,2-Dibromo-3-chloropropane 23.4 2.5 1,2~Dibromoelhane '-.-. '-.._ ",'- 23.6 0.50 Dibromomethane 23.7 0.50 '-... 1,2~Dichlorobenzene 25.6 0.50 '-- 1,3~Dichlorobenzene 25.2 0.50 1,4~Dichlorobenzene 25.0 0.50 Dichlorodifluoromethane 28.1 0.50 1,I ~Dichloroethane 25.4 0.50 1,2~Dichloroethane 24.5 0.50 '-... 1,1~Dichloroethene 26.5 0.50 '-....... cis~I,2~Dichloroethene 24.9 0.50 trans~ 1,2~Dichloroethene 25.S 0.50 1,2~Dichloropropane 23.4 0.50 1,3~Dichloropropane 22.0 0.50 2,2~Dichloropropane 27.9 1.0 ,--. (EDB) 25.0 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the somples tested in the laboratory. This report shalll/ot be reprodllced. except in/IIII, withoutwritlenpermissionji"om TestAmerica. PUF1584 \- ( TestAmerica C THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Stc 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06127/11 Received: 06/27/11 Report Number: PUF1584 C ( C VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Result Reporting Limit Units Spike Level Source Result %REC ( %REC Limits RPD RPD Limit Data Qualifiers Batch: IIFIOSO Extracted: 06/29/11 cis-l,3-Dichloropropene trans-I,3-Dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tett-butyl Ether (MTBE) Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1, I-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total 26.3 25.4 0.50 0.50 ugll 25.0 ugll 25.3 28.3 28.0 24.0 0.50 0.50 1.0 2.5 2.5 ugll ugll ugll ugll ugll ugll ugll 25.0 25.0 25.0 25.0 29.0 28.9 30.0 24.5 26.7 19.8 25.8 29.4 22.9 24.5 19.4 25.8 26.7 27.2 26.4 26.3 23.4 30.7 30.8 21.4 26.3 28.5 24.6 29.5 54.9 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 ugll 25.0 25.0 25.0 ugll ugll ugll 25.0 25.0 25.0 ugll 25.0 25.0 25.0 ugll ugll ugll 0.50 0.50 ugll 1.0 1.0 0.50 ugll ugll ugll ugll ugll ugll 0.50 0.50 0.50 1.0 25.0 25.0 25.0 25.0 ugll ugll ND ND ND ND ND ND 0.910 ND ND ND ND ND ND 25.0 25.0 ND 5.38 25.0 25.0 25.0 25.0 ND ND ND ND ND 1.0 0.50 ugll ugll ugll 25.0 ND 25.0 50.0 ND 24.7 ug/! 25.0 Surrogate: Toluene-dB 25.4 ug/! 25.0 Surrogate: 4-Bromojluorobenzene 26.4 ug/! 25.0 66-129 18-150 47-141 ( ( 78-137 70-130 74-132 56-145 C 113 112 98 107 79 25.0 25.0 25.0 25.0 Surrogate: Dibromojluoromethane C ND ugll 1.5 70-130 71-132 70-130 120 0.50 0.50 ugll 102 101 ND ND ND ND ND ( 70-130 ND ND ( 105 96 116 116 ND C C Source: PUF1575-11 Matrix Spike Analyzed: 06/29/2011 (l1F10SO-MS1) 1,1-Dichloropropene C C C ( METHODBLANKfQCVA;~~1;; Analyte ( 99 118 92 ( ( C 67-138 54-135 70-130 98 78 51-123 70-130 69-133 103 107 109 106 70-130 70-130 70-130 66-126 105 93 76-132 70-130 101 123 86 70-130 74-150 70-130 105 114 99 70-130 61-138 50-150 118 110 58-139 70-130 99 102 106 70-130 70-130 70-130 ( C C C ( ( ( ( ( C C C ( C C C TestAmerica Phoenix ( Carlene McCutcheon Project Manager C The results pertain only to the samples tested in the laboratory. This report shal!not be reprodllced, except in/Ill!, without written permission./i'om TestAmerica. PUF1584 ( ( ( TestAmerica THE LEADER IN ENVIRONMENTAL TESTING ( l 4625 East COlton Center Blvd Ste 189, Phoenix, AZ 85040 (602) 437~3340 Pax:(602) 454-9303 Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/27111 Received: 06/27111 Report Number: PUFI584 c (. ,,,'- METHOD BLANIDQC DATA VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) 'r '-r Analyte r Batch: IIFIOSO Extracted: 06/29/11 Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers L ,- Matrix Spike Dup Analyzed: 06/2912011 (llFIOSO-MSDl) '-r ' Acetone 17.6 10 '----' Benzene r-, 24.7 BrolDobenzene 23.1 ,--' Bromochloromethane 23.5 23.3 r' l_/ r Bromodichloromethane Bromoform '---- Bromomethane r 2-Butanone (MEK) (~ n-Butylbenzene "-,. L sec-Butylbenzene tert-Butylbenzene r ' Carbon disulfide 18.6 23.9 22.3 28.9 27.7 25.6 16.9 '-- / Carbon tetrachloride 25.2 Chlorobenzene 24.1 24.8 23.9 23.5 r- Chloroethane '--, Chloroform r' Chloromethane 2·Chlorotoluene 4·Chlorotoluene Dibromochloromethane ~ 1,2·Dibromo-3·chloropropane ,_, 1,2·Dibromoethane (EDB) Dibromomethane 1,2·Dichlorobenzene '-_ 1,3·Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1·Dichloroethane 1,2-Dichloroethane '-- l,t·Dichloroethene ,__ cis-J ,2-Dichloroethene 21.5 22.9 23.1 23.4 24.7 24.4 24.1 25.8 23.7 23.4 25.4 23.6 1,3-Dichloropropane 24.4 22.9 21.4 2,2-Dichloropropane 26.0 trans-I,2-Dichloroethene '-- 24.8 25.8 1,2-Dichloropropane 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ugll 25.0 25.0 25.0 25.0 25.0 25.0 Source: PUF1S7S-11 ND 70 10-150 70-130 3 ND ND ND 92 94 93 70-130 70-130 70-130 5 7 20 20 20 ND 75 96 89 116 62-126 55-136 22-150 70-130 II 8 20 24 5 2 31 20 25.0 25.0 25.0 25.0 ND 25.0 25.0 ND ND III 102 68 70-130 70-130 56-132 25.0 25.0 25.0 ND ND 101 96 ND 99 76-131 70-130 67-134 25.0 0.220 ND 95 94 ND ND ND ug/l ug/l 0.50 0.50 2.5 ug/l ug/l 0.50 0.50 0.50 ugll 0.50 0.50 ug/l ug/l ug/l ug/l 25.0 25.0 25.0 25.0 ND ugll 25.0 25.0 ND 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 ugll ugll ugll ug/l ug/l ug/l ug/l ug/l ug/l 35 20 99 0.50 1.0 0.50 ugll I ND 3 7 20 9 20 23 6 20 3 6 99 70-130 50-135 70-130 103 86 70-130 70-130 92 92 94 60-135 70-130 70-130 2 29 2 20 I 20 99 98 96 70-130 70-130 70-130 3 3 4 20 103 95 36-150 70-130 9 22 7 20 68-143 70-130 5 20 ND 93 101 4 25.0 25.0 25.0 ND ND 95 98 70-130 70-130 5 20 20 20 ND 20 ND 70-130 70-130 66-130 2 25.0 25.0 92 86 104 2 20 7 20 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 ND ND ND ND ND ND ND ND ND ND ND 5 20 7 4 20 20 4 20 12 20 6 Ri 20 20 20 20 20 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shallllot be reprodllced, e.r:cept in/ull, Wilhol/lwritlen permission/rom TestAmerica. PUFl584 ~ ( TestAmerica c THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson ( Sampled: 06/27/11 Received: 06/27II I Report Number: PUFI584 c ( c .;,,£:';i;Y,;,:,' l\'!~nOD BLANKlQC DATA ( "'~~~"/0 c VOLATILE ORGANICS BY GCIMS (EPA 5030Bf8260B) Reporting Analyte ( ( Result Limit Units Spike Level Source Result %REC ( %REC Limits RPD RPD Limit Data Qualifiers /" ... ( ( Batch: 11F10SO Extracted: 06/29/11 Matrix Spike Dup Analyzed: 06129/2011 (l1F10SO-MSDl) 1,1-Dichloropropene 25.1 0.50 cis-l,3-Dichloropropene 23.8 0.50 trans-} ,3-Dichloropropene 23.9 0.50 Ethylbenzene 27.6 0.50 l Source: PUF1S7S-11 ugil 25.0 ND 100 70-130 5 20 ugll 25.0 ND 95 70-130 7 20 25.0 ND 95 71-132 20 25.0 110 70-130 106 66-129 6 3 6 95 18-150 0.9 25 ( ~.. Hexachlorobutadiene 26.5 1.0 ugil ugil ugil 2-Hexanone 23.8 2.5 ugll 25.0 ND ND ND Iodomethane 27.3 2.5 ugll 25.0 ND 109 47-141 6 29 ( Isopropylbenzene 27.1 0.50 25.0 ND 108 78-137 7 20 ( p-Isopropyltoluene 28.8 0.50 25.0 115 70-130 4 20 1.0 94 74-132 5 20 25.0 20 21 ( ( Methylene Chloride 23.4 4-Methyl-2-pentanone (MIBK) 26.7 2.5 ugil ugil ugil ugil 25.0 ND ND ND 107 56-145 0.07 26 Methyl-tert-butyl Ether (MTBE) 18.0 0.50 ugll 25.0 ND 72 67-138 10 21 Naphthalene 26.0 2.5 25.0 0.910 100 54-135 0.8 33 n-Propylbenzene 28.3 0.50 25.0 ND 113 70-130 4 20 Styrene 24.2 0.50 25.0 97 51-123 6 21 25.0 ND ND 95 70-130 3 20 25.0 ND 75 69-133 3 20 25.0 ND 100 70-130 4 20 25.0 ND 104 70-130 2 20 ( 25.0 ND 107 70-130 20 104 66-126 2 2 ( 100 76-132 6 20 93 70-130 0.5 20 25.0 1,1,1,2-Tetrachloroethane 23.8 0.50 1, 1,2,2-Tetraehloroethane 18.8 0.50 Tetrachloroethene 24.9 0.50 Toluene 1,2,3-Trichlorobenzene 26.1 0.50 26.7 1.0 ugil ugil ugil ugil ugil ugil ugil ugil 1,2,4-Trichlorobenzene 26.0 1.0 ugll 25.0 1,1 , I-Trichloroethane 24.9 0.50 ugll 25.0 ND ND 1,1,2-Trichloroethane 23.2 0.50 ugll 25.0 ND 20 Trichloroethene 29.7 0.50 5.38 97 70-130 3 20 28.6 0.50 ugil ugil 25.0 Trichlorofluoromethane 25.0 ND 114 74-150 8 20 1,2,3-Trichloropropane 21.0 1.0 ugll 25.0 ND 84 70-130 2 1,2,4-Trimethylbenzene 26.5 0.50 ugil 25.0 ND 106 70-130 0.6 1,3,5-Trimethylbenzene 26.8 0.50 ugll 25.0 ND 107 61-138 6 Vinyl Acetate 21.4 1.0 ugll 25.0 ND 85 50-ISO 14 20 20 33 23 Vinyl chloride 27.0 0.50 25.0 ND 108 58-139 9 21 1.5 ugil ugil 50.0 ND 106 70-130 4 20 96 103 104 70-130 Xylenes, Total 53.0 Surrogate: Dibromojluoromethane 24.0 ug/J 25.0 Surrogate: Toluene-d8 25.7 ugll 25.0 Surrogate: 4-Bromojluorobenzene 26.0 ugll 25.0 70-130 70-130 ( ( ( ( ( ( ( ( C C C ( l C ( C TestAmerica Phoenix ( Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except inJull, without writlcn pcnnission!rom TesfAmerica. PUFl584 ( ( ( ( l. ( TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/27111 Received: 06/27111 Report Number: PUF1584 METHOD BLANKlQC DATA VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Reporting Analyte Result Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: 11FI075 Extracted: 06/29/11 Blank Analyzed: 06/29/2011 (l1FI075-BLKl) ND Acetone Benzene ND Bromobenzene Bromochloromethane ND ND Bromoform Bromomethane ND 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene ND ND Carbon disulfide ND ND ND ND ND ND ND Chloromethane '-- ND ND ND tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform '-~. ND Bromodichloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodif1uoromethane l,l-Dichloroethane 1,2-Dichloroethane l,l-Dichloroethene cis-} ,2-Dichloroethene tmns-I,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll TestAmerica Phoenix ,~ Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall nat be reproduced, except inJull. without wriltenpermissionjrom Tes/America. PUF1584 TestAmerica THE LEADEAIN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/27111 Received: 06/27/11 Report Number: PUF1584 ( ',--- VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC ( %REC Limits RPD RPD Limit Data Qualifiers ( ( Batch: IIFI075 Extracted: 06/29/11 ( Blank Analyzed: 06/29/2011 (IIFI075-BLKl) l,l-Dichloropropene ND cis-l,3-Dichloropropene ND trans-l,3-Dichloropropene ND Ethylbenzene ND NO Hexachlorobutadiene 2-Hexanone Iodomethane Isopropy Ibenzene ND ND Methylene Chloride ND ND ND 4-Methyl-2-pentanone (MIBK) ND Methyl-tert-butyl Ether (MTBE) ND Naphthalene ND n-Propylbenzene ND NO p-Isopropyltolucne Styrene 1, I, 1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total SWTogate: DibromojIuoromelhane ND ND NO NO ND NO ND ND NO NO ND NO ND ND ND ND 0.50 0.50 0.50 0.50 1.0 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 ( ugil ugil ugll ugil ugil ugil ugil ugil ugil ugll ugll ugil ugil ugil ugil ugll ugll ugil ugil ugil ugil ugil ugll ugil ugil ugil ugil ugil ugll ugil ugil ( ( ( ( C ( ( ( ( ( ( ( ( ( C ( ( C C ( lIgll 25.0 106 70-130 Surrogate: Toluene-d8 26.5 25.4 ugll 25.0 102 70-130 Surrogate: 4-BromojIuorobenzene 24.5 ugll 25.0 98 70-130 ( ( ( TestAmerica Phoenix C Carlene McCutcheon ( Project Manager The resulfs pertain only to fhe samples tested in the laboratory. This report sflallllot be reproduced, except infull, withoutwrittenpenllissionfrom TestAmerica. PUF1584 ( C C l ( TestAmerica 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437~3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING r Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/2711 1 Received: 06/2711 1 Report Number: PUF1584 c METHOD BLANKlQC DATA "'- VOLATILE ORGANICS BY GCIMS (EPA 5030Bf8260B) "'- C , Analyte Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers '- , . Batch: 11FI075 Extracted: 06/29/11 ',,-, LeS Analyzed: 06/29/2011 (l1Fl075-BSl) ,_. Acetone 27.5 '- Benzene r Bromobenzene "----, Bromochloromethane C r r Bromodichloromethane Bromofonn Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene 22.9 24.5 22.8 23.8 22.6 19.0 27.2 26.5 26.4 tert-Butylbenzene 25.8 Carbon disulfide 28.3 23.8 Carbon tetrachloride Chlorobenzene Chloroethane "---- Chlorofonn r- Chloromethane '-..' 2-Chlorotoluene '- 4-Chlorotoluene Dibromochloromethane '-.. ___ 1,2-Dibromo-3-chloropropane r" 24.3 21.8 22.9 24.7 25.1 25.8 24.4 24.4 1,2-Dibromoethane (EDB) Dibromomethane '-....-- 1,2-Dichlorobenzene 23.6 '-...-_ 1,3-Dichlorobenzene "- l,4-Dichlorobenzene Dichlorodifluoromethane 25.2 25.0 24.2 l,l-Dichloroethane 1,2-Dichloroethane 23.1 24.2 '---_ ~ r '-...-- l,l-Dichloroethene ,, __ . cis-l,2-Dichloroethene '-- 22.2 25.4 23.0 22.0 trans-l,2-Dichloroethene 1,2-Dichloropropane 23.1 23.0 1,3-Dichloropropane 23.6 23.2 2,2-Dichloropropane 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 25.0 110 25.0 25.0 25.0 92 25.0 25.0 25.0 25.0 98 91 95 91 76 109 30-150 70-130 70-130 70-130 70-130 67-122 64-132 48-150 25.0 25.0 25.0 106 25.0 25.0 113 ·70-130 70-130 70-130 61-126 95 97 70-130 70-130 87 92 69-128 70-130 56-131 25.0 25.0 25.0 106 103 25.0 25.0 25.0 103 25.0 25.0 25.0 98 97 94 25.0 25.0 89 102 25.0 25.0 25.0 101 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 99 101 100 97 93 97 92 70-130 70-130 70-130 63-129 70-130 70-130 70-130 70-130 70-130 42-150 70-130 72-133 88 70-130 70-130 92 92 94 70-130 70-130 70-130 93 70-130 TestAmerica Phoenix Carlene McCutcheon Project Manager Tile results pertain only to the samples tested in the laboratory. This report shall not be reproduced. except in/ull, without written permission/rom TestAmerica. PUFJ584 l." ( TestAmerica C THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Stc 189, Phoenix, AZ 85040 (602) 431-3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Sampled: 06/27111 Phoenix, AZ 85028 Report Number: PUF1584 ( ( ( ( Received: 06/27111 Attention: Joel Peterson ( ~;-F~~" .,METHOD Bb~K.!~~nATA ( C VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result ( %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: 11F1075 Extracted: 06/29/11 (- C C LCS Analyzed: 06/29/2011 (llF1075-BS1) l,l-Dichloropropene 22.9 0.50 ugll 25.0 92 70-130 ( cis-I,3-Dichloropropene 24.1 0.50 ugll 25.0 97 70-130 ( trans-l,3-Dichloropropene 23.9 0.50 ugll 25.0 96 70-130 Ethylbenzene 25.5 0.50 ugll 25.0 102 70-130 Hexachlorobutadiene 24.5 1.0 ugll 25.0 98 70-130 2-Hexanone 30.5 2.5 ugll 25.0 122 44-150 Iodomethane 27.3 2.5 ugll 25.0 109 58-138 Isopropylbenzene 27.4 0.50 ugll 25.0 110 70-130 p-Isopropyltoluene 26.1 0.50 ugll 25.0 105 70-130 Methylene Chloride 22.3 1.0 ugll 25.0 89 70-130 4-Methyl-2-pentanone (MIBK) 25.3 2.5 ugll 25.0 101 61-142 Methyl-tett-butyl Ether (MTBE) 22.8 0.50 ugll 25.0 91 70-130 Naphthalene 25.6 2.5 ugll 25.0 103 65-129 n·Propylbenzene 26.7 0.50 ugll 25.0 107 70-130 Styrene 23.8 0.50 ugll 25.0 95 70-130 1,1,1,2· Tetrachloroethane 23.6 0.50 ugll 25.0 94 70-130 1, 1,2,2·Tetrachloroethane 24.6 0.50 ugll 25.0 98 70-130 Tetrachloroethene 24.1 0.50 ugll 25.0 96 70-130 Toluene 23.6 0.50 ugll 25.0 95 70-130 I ,2,3·Trichlorobenzene 25.7 1.0 ugll 25.0 103 70-130 1,2,4·Trich lorobenzene 25.3 1.0 ugll 25.0 101 70-130 1,1, I· Trichloroethane 23.9 0.50 ugll 25.0 96 70-130 1,1,2·Trichloroethane 22.7 0.50 ugll 25.0 91 70-130 Trichloroethene 23.4 0.50 ugll 25.0 94 70-130 Trichlorofluoromethane 25.2 0.50 ugll 25.0 101 78-149 1,2,3·Trichloropropane 24.8 1.0 ugll 25.0 99 70-130 1,2,4~ Trimethylbenzene 26.3 0.50 ugll 25.0 105 70-130 1,3,5·Trimethylbenzene 26.4 0.50 ugll 25.0 106 70-130 Vinyl Acetate 21.2 1.0 ugll 25.0 85 57-149 Vinyl chloride 22.3 0.50 ugll 25.0 89 66-134 Xylenes, Total 49.7 1.5 ugll 50.0 99 70-130 Surrogate: Dibromojluoromethane 25.1 ugll 25.0 100 70-130 Surrogate: Toluene·d8 25.1 24.3 ugll 25.0 101 70-130 ugll 25.0 97 70-130 Surrogate: 4-Bromojluorobenzene ( ( ( ( ( ( ( ( C ( ( ( ( \ c ( ( C C C C C ( TestAmerica Phoenix Carlene McCutcheon Project Manager ( The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except in/ull, without written permission/rom TestAmerica. PUF1584 ( ( ( l ( TestAmerica THE LEADER IN ENVIRONMENTAL TESTING Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson r ~ 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Sampled: 06/27/11 Received: 06/27111 Report Number: PUFI584 c C METHOD BLANKlQC DATA r '- VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) c r Analyte ,. '- Batch: 11FI075 Extracted: 06/29/11 r LCS Dup Analyzed: 06/29/2011 (l1FI075-BSDl) 26.0 23.8 Benzene Bromobenzene 26.0 Bromochloromethane 24.9 24.5 Bromodichloromethane 23.5 Bromofonn Bromomethane 23.5 2-Butanone (MEK) 26.9 28.0 n-Butylbenzene sec-Butylbenzene 27.9 26.9 tert-Butylbenzene Carbon disulfide 29.6 Carbon tetrachloride 25.4 Chlorobenzene 25.5 23.8 Chloroethane Chlorofonn 24.6 Chloromethane 25.2 26.3 2-Chlorotoluene 26.7 4-Chlorotoluene Dibromochloromethane 26.1 I ,2-Dibromo-3-chloropropane 26.8 1,2-Dibromoethane (EDB) 25.3 Dibromomethane 22.9 1,2-Dichlorobenzene 26.1 1,3-Dichlorobenzene 26.1 26.2 lA-Dichlorobenzene Dichlorodifluoromethane 26.2 24.4 I,I-Dichloroethane 25.2 1,2-Dichloroethane l,l-Dichloroethene 24.7 cis-I,2-Dichloroethene 23.4 trans-I,2-Dichloroethene 24.4 1,2-Dichloropropane 23.4 1,3-Dichloropropane 25.0 2,2-Dichloropropane 23.6 '-r Acetone '---' f· L ("l~. r~ _ r-, '-......-/ r ..... j r "'---, ,- r ,. "-- ,r L' '--'-- ,'"--, '------ '--'-- Result Reporting Limit 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 Units ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll Spike Level 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 Source Result %REC 104 95 104 99 98 94 94 108 112 112 108 118 102 102 95 99 101 105 107 104 107 101 92 104 104 105 105 98 101 99 94 97 94 100 94 %REC Limits RPD 30-150 70-130 70-130 70-130 70-130 67-122 64-132 48-150 70-130 70-130 70-130 61-126 70-130 70-130 69-128 70-130 56-131 70-130 70-130 70-130 63-129 70-130 70-130 70-130 70-130 70-130 42-150 70-130 72-133 70-130 70-130 70-130 70-130 70-130 70-130 6 4 6 9 3 4 21 I 5 5 4 4 6 5 9 7 2 5 3 7 9 7 3 3 3 5 8 5 4 7 6 5 2 6 2 RPD Limit 35 20 20 20 20 20 20 Data Qualifiers R6 33 20 20 20 20 20 20 20 20 20 20 20 20 25 20 20 20 20 20 20 20 20 20 20 20 20 20 20 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain ollly to the samples tested in the laboratory. This report shall/lOt be reproduced, except infull, without written permission/rom TestAmerica. PUF1584 l_ TestAmerica ( THE LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC !O645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson 4625 East Cotton Center Blvd. Stc 189, Phoenix. AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Sampled: 06/27/11 Received: 06127111 Report Number: PUFI584 ( ( ( MEl'~q]j'BLANKlQC DATA ( ( VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Analyte ( ( ( ( Result Reporting Limit Units Spike Level Source Result %REC ( %REC Limits RPD RPD Limit Data Qualifiers Batch: llFl075 Extracted: 06/29111 LCS Dup Analyzed: 06/29/2011 (1IFl075-BSD1) l,l-Dichloropropene 23.7 0.50 cis-l,3-Dichloropropene 24.8 0.50 trans-!,3 -Dichloropropene 24.9 0.50 Ethylbenzene 26.1 0.50 ugil ugil ugil ugil 25.0 95 70-130 3 20 25.0 99 70-130 3 25.0 100 70-130 4 20 20 25.0 104 70-130 2 20 Hexachlorobutadiene 25.7 LO ugil 25.0 to3 70-130 5 2-Hexanone 28.9 2.5 ugil 25.0 t16 44-150 5 Iodomethane 30.3 2.5 25.0 121 58-138 to IsopropyJbenzene 28.2 0.50 25.0 113 70-130 3 20 31 25 20 p-Isopropyltoluene 27.5 0.50 25.0 Ito 70-130 5 20 Methylene Chloride 23.8 LO 4-Methyl-2-pentanone (MlBK) 27.7 2.5 ugil ugil ugil ugil ugil Methyl-tert-butyl Ether (MTBE) 24.7 0.50 Naphthalene 27.8 2.5 n-Propylbenzene 27.8 0.50 Styrene 24.5 0.50 25.0 95 70-130 25.0 111 61-142 6 9 20 22 ugil 25.0 70-130 8 20 25.0 99 III 65-129 25.0 lIt 70-130 8 4 20 25.0 98 70-130 3 20 1,1,1,2-Tetrachloroethane 24.4 0.50 1,1,2,2-Tetrachloroethane 25.7 0.50 Tetrachloroethene 25.4 0.50 Toluene 24.6 0.50 1,2,3-Trich lorobenzene 27.3 1,2,4-Trichlorobenzene 27.3 LO LO ugil ugil ugil ugil ugil ugil ugil ugil ugil 1, 1, I-Trichloroethane 25.2 0.50 1,1,2-Trichloroethane 24.1 0.50 20 C ( ( ( C ( ( ( ( ( , ( ( ( C 25.0 98 70-130 3 20 25.0 103 70-130 4 20 25.0 102 70-130 20 25.0 98 70-130 5 4 20 ( 25.0 109 70-130 6 25.0 109 70-130 8 20 20 ( ugit 25.0 101 70-130 5 20 ( 25.0 96 70-130 6 20 C C Trichloroethene 24.0 0.50 Trichlorofluoromethane 27.0 0.50 1,2,3-Trichloropropane 26.0 LO 1,2,4-Trimethylbenzene 27.4 0.50 1,3,5-Trimethylbenzene 27.4 0.50 ugil ugil ugil ugil ugil ugil Vinyl Acetate 23.5 LO Vinyl chloride 24.0 0.50 Xylenes, Total 5LO L5 SlI1Togate: Dibromojluoromethane ( 25.0 96 70-130 2 20 25.0 108 to4 78-149 7 20 70-130 5 20 70-130 4 20 25.0 Ito Ito 70-t30 4 20 ugil 25.0 94 57-149 t1 21 ugil ugil 25.0 96 66-134 8 20 C 50.0 102 70-130 3 20 ( 25.5 ugll 25.0 102 70-130 Surrogate: Toluene-dB 25.0 ugll 25.0 70-130 Surrogate: 4-Bromojluorobenzene 24.4 ugll 25.0 100 98 25.0 25.0 C C ( 70-130 C ( TestAmerica Phoenix Carlene McCutcheon ( Project Manager The results pertain only to the somples tested in the laboratory. This report shalf not be reproduced, e:>,:cepl inJul!, without wril1enpermissionJrom TestAmerica. PUF1584 ( (, ( ,, c TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 20 II Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/27/11 Received: 06127111 Report Number: PUFI584 METHOD BLANKIQC DATA VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) ,Analyte ,- Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: IIF1075 Extracted: 06/29/11 , Matrix Spike Analyzed: 06/29/2011 (IIF1075-MS1) Acetone 13.1 ,--. Benzene 23.9 roo '. Bromobenzene 24.8 22.8 Bromochloromethane 23.8 Bromodichloromethane r-, Bromoform 21.8 '-_/ Bromomethane 20.4 18.4 2-Butanone (MEK) , n-Butylbenzene 26.5 '-..--" sec-Butylbenzene 26.5 26.5 tert-Butylbenzene Carbon disulfide 30.4 25.5 Carbon tetrachloride 24.3 Chlorobenzene 23.2 Chloroethane 23.4 Chloroform 24.7 Chloromethane 25.8 2-Chlorotoluene 26.1 4-Chlorotoluene 24.0 Dibromochloromethane 1,2-Dibromo-3..chloropropane 23.3 23.6 1,2-Dibromoethane (EDB) 21.9 Dibromomethane 24.6 1,2·Dichlorobenzene 25.0 l,3·Dichlorobenzene 25.2 l,4·Dichlorobenzene 26.4 Dichlorodifluoromethane 23.2 l, l·Dichloroethane 22.9 l,2·Dichloroethane 25.3 l,l·Dichloroethene 22.0 cis·l,2·Dichloroethene 23.6 trans·l,2·Dichloroethene 22.2 1,2·Dichloropropane 23.1 l,3·Dichloropropane 25.1 2,2·Dichloropropane ,r- ~- 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 Source: PUF1584-03 ND 52 10-150 ND 96 70-130 ND 99 70-130 70-130 ND 91 ND 95 70-130 ND 87 62-126 ND 81 55-136 74 22-150 ND 106 70-130 ND ND 106 70-130 ND 106 70-130 122 56-132 ND 102 76-131 ND ND 97 70-130 ND 93 67-134 0.230 93 70-130 99 50-135 ND ND 103 70-130 104 70-130 ND 96 70-130 ND ND 93 60-135 ND 94 70-130 88 70-130 ND ND 99 70-130 100 70-130 ND ND 101 70-130 ND 106 36-150 93 70-130 ND ND 91 68-143 0.680 99 70-130 88 70-130 ND 94 70-130 ND 89 70-130 ND ND 92 70-130 ND 100 66-130 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested ill the laboratory. This report shall not be reproduced, excepl in/ull, without wrillellpermission/rom TestAmerica. PUFJ584 TestAmerica THE LEADeR IN ENVIRONMENTAL TESTING 4625 East Cotlon Center Blvd. $te 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 C ( Sampled: 06/27/11 Received: 06/27111 Report Nmnber: PUFI584 ( ( Attention: Joel Peterson ( ( ( C VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC ( %REC Limits RPD RPD Limit Data Qualifiers Batch: IIFI075 Extracted: 06/29/11 Matrix Spike Analyzed: 06/29/2011 (IIFI075-MSl) l,l-Dichloropropene 23.4 cis-l,3-Dichloropropene trans-} ,3-Dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl Ether (MTBE) Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene I ,1, I-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total 24.3 23.6 25.8 23.4 22.4 28.6 28.2 26.5 21.8 24.8 21.7 25.2 27.4 23.4 23.4 24.0 28.9 24.5 24.4 25.1 24.6 22.3 24.7 26.7 Surrogate: Toluene-d8 22.7 26.5 26.5 22.6 24.5 49.8 25.1 25.9 Surrogate: 4-Bromojluorobenzelle 24.3 Surrogate: Dibromojluoromethane 0.50 0.50 0.50 0.50 1.0 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 25.0 25.0 25.0 25.0 25.0 95 103 ND 93 90 115 25.0 25.0 25.0 25.0 ND 25.0 25.0 25.0 ND 25.0 25.0 25.0 ND ND ND ND ND ND ND ND 113 106 87 99 87 101 110 94 89 97 107 70-130 70-130 74-150 ND 91 106 106 70-130 70·130 61-138 25.0 ND 90 50-150 25.0 50.0 ND 98 100 100 58-139 70-130 70-130 104 97 70-130 70-130 25.0 25.0 25.0 25.0 25.0 25.0 ug/l 25.0 ugll 25.0 ug/l 25.0 ND ND ND 0.580 ND ND ND ND ( ( ( ( ( ( 54-135 70-130 51-123 70-130 70-130 66-126 76-132 ND ND ( 70·130 74-132 56-145 67-138 98 98 100 98 25.0 25.0 25.0 3.48 ( 47-141 78-137 70-130 69-133 70-130 ND ND ( 71-132 70-130 66-129 18-150 93 96 102 25.0 25.0 25.0 25.0 ( l. Source: PUF1584-03 ND 94 70-130 ND 70-130 97 ND ND ( ( ( ( ( ( C ( ( ( ( , ( ( ( ( TestAmerica Phoenix ( Carlene McCutcheon Project Manager ( The results pertain only to the samples tested in the laboratory. This report shalll/ot be reproduced, except il/jull, withoutwrittenpermissiol/jrom TestAmerica. PUF1584 ( ( ( , , , TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/27111 Received: 06/27111 Report Number: PUFI584 METHOD BLANKlQC DATA VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Analyte Result Reporting Limit ,- Batch: llFI075 Extracted: 06/29/11 , Matrix Spike Dup Analyzed: 06/29/2011 (l1FI075-MSDl) Acetone 14.4 10 ". ~.' Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) r n-Butylbenzene sec-Butylbenzene '--_~ tert-Butylbenzene r-, Carbon disulfide '---" Carbon tetrachloride Chlorobenzene Chloroethane Chloroform ,.-, Chloromethane ~. 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3 -chloropropane I,2-Dibromoethane (EDB) Dibromomethane I,2-Dichlorobenzene 1,3-Dichlorobenzene .... j 24.2 25.4 23.1 24.4 23.1 23.0 21.4 27.0 27.0 26.1 29.9 25.7 24.7 23.4 23.6 24.0 26.0 26.6 24.& 25.& 24.1 22.3 25.6 1,4-Dichlorobenzene Dichlorodifluoromethane 26.0 26.1 26.6 l,l-Dichloroethane 23.5 1,2-Dichloroethane 24.1 l,l-Dichloroethene cis-I,2-Dichloroethene trans-I,2-Dichloroethene 24.9 1,2-Dichloropropane 1,3-Dichloropropane 23.1 2,2-Dichloropropane 22.4 24.2 23.5 25.0 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Source: PUF1584-03 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 25.0 25.0 25.0 25.0 ND 57 ND NO NO 97 102 92 25.0 25.0 25.0 ND ND 25.0 25.0 25.0 ND ND NO 98 92 92 85 62-126 55-136 22-150 108 10&. 70-130 70-130 ugll 25.0 25.0 ND ND 105 119 70-130 56-132 2 25.0 25.0 25.0 25.0 ND ND NO 0.230 103 76-131 0.7 99 94 94 70-130 67-134 70-130 0.6 25.0 25.0 25.0 ND NO 96 104 107 50-135 70-130 70-130 3 0.7 2 99 103 96 70-130 60-135 70-130 3 10 2 89 103 104 70-130 70-130 70-130 2 4 20 20 20 104 106 70-130 36-150 4 3 20 20 0.7 22 94 96 70-130 68-143 5 20 20 97 90 70-130 70-130 2 2 97 92 94 70-130 70-130 70-130 2 4 20 20 20 100 66-130 2 0.2 20 20 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ND 25.0 25.0 ND ND NO 25.0 25.0 25.0 ND ND NO 25.0 25.0 ND NO ND ND ugll 25.0 25.0 25.0 ugll 25.0 ND 0.680 ugll 25.0 25.0 25.0 ND ND NO 25.0 25.0 ND NO ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 10-150 70-130 9 70-130 70-130 70-130 2 I 3 6 12 15 2 2 1 I 35 20 20 20 20 20 24 31 20 20 20 20 20 20 20 20 20 20 20 20 29 20 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain ollly to the samples tested in the laboratory. This report shallllot be reproduced, except illfull, without writlenpenllissiollji-om TestAmerica. PUF1584 ~.... TestAmerica ( ( THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.1 0 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/27/11 Received: 06/27/11 Report Number: PUFI584 ( ( ( ( ( ( ,',METHOD BLANKlQC DATA VOLATILE ORGANICS BY GC/MS (EPA S030B/S260B) Analyte c Result Reporting Limit Units Spike Level Source Result o/"REC %REC Limits RPD RPD Limit Data Qualifiers Batch: 11FI075 Extracted: 06/29/ll Matrix Spike Dup Analyzed: 06/29/2011 (l1FI075-MSDl) l,l-Dichloropropene 24.4 0.50 24.6 trans-I ,3-Dichloropropene 24.6 0.50 0.50 Ethylbenzene 25.8 Hexachlorobutadiene ( c Source: PUF1584-03 cis-I,3-Dichloropropene c ( c 25.0 NO 98 70-\30 25.0 NO 98 25.0 25.0 ND ND 98 0.50 ugll ugll ugll ugll 24.6 1.0 ugll 25.0 2-Hexanone 23.4 2.5 25.0 4 20 70-\30 I 20 71-\32 4 20 103 70-\30 0.04 20 NO 98 66-129 5 21 NO 93 18-150 4 25 25.0 ND 114 47-141 0.4 29 25.0 NO 113 78-\37 0.5 20 25.0 NO 109 70-\30 3 20 25.0 Iodomethane 28.5 2.5 Isopropy lbenzene 28.3 0.50 p-Isopropyltoluene 27.2 0.50 Methylene Chloride 22.4 1.0 ugll ugll ugll ugll ugll 74-132 3 20 26.3 2.5 ugll 25.0 ND ND 90 4-Methyl-2-pentanone (MIBK) 105 56-145 6 26 Methyl-tett-butyl Ether (MTBE) 23.4 0.50 ugll 25.0 NO 93 67-\38 7 21 Naphthalene 26.9 2.5 25.0 ND 108 54-135 7 33 n-Propylbenzene 27.7 0.50 25.0 NO III 70-\30 Styrene 23.4 0.50 ugll ugll ugll 25.0 94 51-123 0.3 21 I, I, 1,2-Tetrachloroethane 23.1 0.50 ugll 25.0 92 70-\30 I 20 1,1,2,2-Tetrachloroethane 26.0 0.50 ugll 25.0 ND ND ND 104 69-\33 20 Tetrachloroethene 28.2 0.50 ugll 25.0 3.48 99 70-130 Toluene 24.0 0.50 ugll 25.0 NO 96 70-130 8 3 2 1,2,3-Trichlorobenzene 26.5 1.0 25.0 NO 106 70-\30 26.3 1.0 25.0 NO 105 66-126 1,1,1-Trichloroethane 24.6 0.50 25.0 98 76-\32 1,1,2-Trichloroethane 22.7 0.50 ugll 25.0 ND ND 8 5 0.2 20 1,2,4-Trichlorobenzene ugll ugll ugll 91 70-\30 20 Trichloroethene 24.6 0.50 ugll 25.0 0.580 96 70-130 Trichlorofluoromethane 26.8 0.50 ugll 25.0 NO 107 74-150 2 0.3 0.2 20 1,2,3-Trichloropropane 24.8 1.0 25.0 ND 99 70-\30 9 20 1,2,4-Trimethylbenzene 26.4 0.50 25.0 NO 106 70-\30 0.3 20 1,3,5-Trimethylbenzene 26.8 0.50 ugll ugll ugll 25.0 NO 107 61-\38 I 33 Vinyl Acetate 23.9 1.0 ugll 25.0 ND 96 50-150 6 23 20 20 20 20 20 20 Vinyl chloride 25.0 0.50 ugll 25.0 NO 100 58-\39 2 21 Xylenes, Total 49.6 1.5 ugll 50.0 ND 99 70-\30 0.4 20 Surrogate: Dibromojluoromethalle 25.7 ug/l 25.0 103 70-130 Surrogate: Toluene-d8 25.5 ugll 25.0 102 70-130 Surrogate: 4-Bromojluorobellzelle 24.0 ugll 25.0 96 70-130 ( ( ( c ( ( ( ( ( c c ( ( c ( ( ( ( c c ( c c c c TestAmerica Phoenix Carlene McCutcheon Project Manager ( The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except infull, wilhoufwrittenpermissionji-om TestAmerica. PUF1584 ( ( ( , , TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.1 0 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/27111 Received: 06/27/11 Report Number: PUFI584 METHODBLANIDQCDATA VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte ~. Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: 11Fl1l2 Extracted: 06/30/11 Blank Analyzed: 06/30/2011 (l1F1112-BLKI) Acetone NO !O Benzene ND Bromobenzene ND 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 Bromochloromethane NO Bromodichloromethane ND Bromofonn ND Bromomethane NO 2-Butanone (MEK) ND n-Butylbenzene ND sec-Butylbenzene tert-Butylbenzene NO NO Carbon disulfide ND Carbon tetrachloride NO Chlorobenzene ND Chloroethane Chlorofonn NO NO Chloromethane ND 2-Chlorotoluene ND 4-Chlorotoluene ND Dibromochloromethane ND I ,2-Dihromo-3-chloropropane NO l,2-Dibromoethane (EDB) ND Dibromomethane ND l,2-Dichlorobenzene ND l,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane NO 1,1-Dichloroethane ND 1,2-Dichloroethane NO l,l-Dichloroethene ND cis-l,2-Dichloroethene ND trans-I,2-Dichloroethene 1,2-Dichloropropane NO NO J,3-Dichloropropane ND 2,2-Dichloropropane ND ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll TestAmerica Phoenix Carlene McCutcheon Project Manager The resufls pertain only to the samples tested in the laboratory. This report shall not be reprodllced, except infull, without writtenpermissionjrom TestAmerica. PUF1584 ~ ( TestAmerica ( THE LEADER IN ENVIRONMENTAL TgSTING 4625 East Colton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson ( Sampled: 06/27111 Received: 06/27111. Report Number: PUP 1584 C ( ( ( C ( ·Y>' '( ,,~ '~., ~~"';"0~ .••••. ; .••.. C VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Reporting Analyte Result Limit Units Spike Level Source Result %REC ( %REC Limits RPD RPD Data Limit Qualifiers Batch: llFl112 Extracted: 06/30/11 Blank Analyzed: 06/30/2011 (I1FI112-BLKI) 1,1-Dichloropropene ND cis-l,3-Dichloropropene ND trans-l,3-Dichloropropene ND Ethylbenzene Hexachlorobutadiene ND 2-Hexanone Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MlBK) Methyl-tert-butyl Ether (MTBE) Naphthalene n-Propylbenzene Styrene 1,1, I ,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3 -Trichloropropane ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ( C 0.50 0.50 0.50 0.50 1.0 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 ( ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll C C C ( C C ( ( C C ( C C ( ( ( ( 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene ND Vinyl Acetate ND Vinyl chloride Xylenes, Total ND Surrogate: Dibromofluoromethane 28.3 ug/l 25.0 Surrogate: Toluene-dB 25.3 ugll Surrogate: 4-Bromojluorobenzene 24.8 ugll ND C 0.50 1.0 0.50 1.5 C ( 70-130 25.0 113 101 25.0 99 70-130 ( ( 70-130 ( C TestAmerica Phoenix C Carlene McCutcheon Project Manager ( The results pertain only to the samples tested in the laboratory. This report shalll/ot be reproduced, except infull, without written permission from TestAmerica. PUF1584 ( ( ( r TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/27111 Received: 06/27111 Report Number: PUFI584 METHOD BLANKlQC DATA VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Analyte Result Reporting Limit Spike Units Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: l1FI112 Extracted: 06/30/11 LCS Analyzed: 06/30/2011 (l1F1112-BSl) Acetone 18.6 25.0 Benzene 26.5 Bromobenzene 25.2 Bromochloromethane 27.2 Bromodichloromethane 24.0 Bromofonn Bromomethane 25.9 22.3 2-Butanone (MEK) 29.8 n-Butylbenzene '-- ~ sec-Butylbenzene 29.0 28.5 ,,-/ tert-Butylbenzene '---, Carbon disulfide 29.2 "- Carbon tetrachloride 29.1 ~'. 26.5 Chlorobenzene 24.5 Chloroethane 27.6 Chlorofonn 30.4 Chloromethane 28.7 2-Chlorotoluene 4-Chlorotoluene 29.4 27.1 Dibromochloromethane '28.3 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) 25.9 25.3 Dibromomethane 1,2-Dichlorobenzene 27.8 27.9 1,3-Dichlorobenzene 27.9 1,4-Dichlorobenzene 28.4 Dichlorodifluoromethane 25.9 I,I-Dichloroethane 1,2-Dichloroethane 30.4 24.6 1,l-Dichloroethene 24.1 cis-l,2-Dichloroethene 24.0 trans-l,2-Dichloroethene 1,2-Dichloropropane 24.3 24.7 1,3-Dichloropropane 27.7 2,2-Dichloropropane 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 74 100 106 101 109 96 104 89 119 116 114 117 116 106 98 III 122 115 118 108 113 104 101 III 112 112 114 104 121 98 96 96 97 99 III 30-150 70-130 70-130 70-130 70-130 67-122 64-132 48-150 70-130 70-130 70-130 61-126 70-130 70-130 69-128 70-130 56-131 70-130 70-130 70-130 63-129 70-130 70-130 70-130 70-130 70-130 42-150 70-130 72-133 70-130 70-130 70-130 70-130 70-130 70-130 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only /0 the samples tested in the laboratory. This report shall not be reproduced. except in/Ill!. withollfwrittenpermissionji~m Tes/America. PUFl584 ~­ ( TestAmerica ( THE LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson ( ( Sampled: 06/27/11 Received: 06/27111 Report Number: PUFI584 ( ( ( C ( C VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC ( %REC Limits RPD RPD Limit Data Qualifiers Batch: 11F1112 Extracted: 06/30/11 ( ( C LCS Analyzed: 06/30/2011 (l1Fl112-BSl) l,l-Dichloropropene 25.3 0.50 ugll 25.0 101 70-130 cis-} ,3-Dichloropropene 26.3 0.50 ugll 25.0 105 70-130 trans-! ,3 -Dichloropropene 27.8 0.50 ugll 25.0 III 70-130 Ethylbenzene 27.4 0.50 ugll 25.0 110 70-130 Hexachlorobutadiene 28.0 1.0 ugll 25.0 112 70-130 2-Hexanone Iodomethane Isopropylbenzene p-Isopropyltoluene 26.0 2.5 ugl1 25.0 104 44-150 30.4 2.5 ugll 25.0 122 58-138 29.6 0.50 ugll 25.0 119 70-130 29.4 0.50 ugll 25.0 118 70-130 Methylene Chloride 24.0 1.0 ugll 25.0 96 70-130 4-Methyl-2-pentanone (MIBK) 29.3 2.5 ugll 25.0 117 61-142 Methyl-tert-butyl Ether (MTBE) Naphthalene n-Propylbcnzcne Styrene I, I, 1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethcne Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethcne Trichlorofluoromclhane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total 26.2 0.50 ugll 25.0 105 70-130 28.6 2.5 ugll 25.0 115 65-129 29.1 0.50 ugll 25.0 117 70-130 25.5 0.50 ugll 25.0 102 70-130 ( C ( ( ( ( ( ( ( 25.8 0.50 ugl1 25.0 103 70-130 25.6 0.50 ugll 25.0 102 70-130 25.6 0.50 ugll 25.0 102 70-130 ( ( ( 25.4 0.50 ugll 25.0 102 70-130 ( 29.4 1.0 ugll 25.0 117 70-130 29.2 1.0 ugll 25.0 117 70-130 C 28.9 0.50 ugll 25.0 115 70-130 ( 24.6 0.50 ugll 25.0 98 70-130 25.9 0.50 ugll 25.0 104 70-130 C 30.7 0.50 ugll 25.0 123 78-149 ( 27.6 1.0 ugll 25.0 III 70-130 30.1 0.50 ugll 25.0 120 70-130 ( 30.0 0.50 ugll 25.0 120 70-130 24.8 1.0 ugll 25.0 99 57-149 ( 26.9 0.50 ugll 25.0 108 66-134 ( 52.5 1.5 ugll 50.0 105 70-130 25.0 108 70-130 ( Surrogate: Dibromofluoromethane 26.9 ug// Surrogate: Toluene-dB 26.2 ugll 25.0 105 70-130 Surrogate: 4-Bromojluorobenzene 26.6 ug/I 25.0 106 70-130 ( ( ( TestAmerica Phoenix C Carlene McCutcheon C Project Manager The results pertain only to the samples tested in the laboratory. This report sha!l not be reproduced. except inJul!, without written permissionJrom TestAmerica. PUF1584 ( ( ( , TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/27/11 Received: 06/27/11 Report Number: PUFI584 METHOD BLANKlQC DATA VOLATILE ORGANICS BY GCIMS (EPA S030B/8260B) Analyte '. Result r Batch: l1FI112 Extracted: 06/30/11 r LCS Dup Analyzed: 06/30/2011 (IIFII12-BSDJ) ~'. Acetone Benzene Bromobenzene Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit 17.8 10 ugll 25.0 71 30-150 4 25.0 0.50 ugll 25.0 100 70-130 0.1 20 27.2 0.50 25.0 109 70-130 2 20 20 35 " 24.7 0.50 ugll ugll 25.0 99 70·130 2 Bromodichloromethane 26.9 0.50 ugll 25.0 107 70-130 I 20 r- Bromoform 23.8 1.0 25.0 95 67-122 0.9 20 '----' Bromomethane 26.4 1.0 25.0 105 64-132 2 20 ,"--. 2-Butanone (MEK) 21.8 2.5 25.0 87 48-150 2 33 --- n-Butylbenzene 29.1 0.50 25.0 116 70-130 2 20 sec-Butylbenzene 28.5 0.50 25.0 114 70-130 tert-Butylbenzene 28.1 0.50 ugll ugll ugll ugll ugll ugll 25.0 113 70-130 r ". ....... Bromochloromethane r. 20 20 Carbon disulfide 29.7 0.50 ugll 25.0 119 61-126 2 20 ..... / Carbon tetrachloride 28.6 0.50 25.0 114 70-130 2 20 Chlorobenzene 25.9 0.50 25.0 104 70-130 2 20 Chloroethane 23.8 1.0 25.0 95 69-128 3 20 26.7 0.50 25.0 107 70-130 4 20 Chloromethane 29.0 1.0 25.0 116 56-131 5 20 2-Chlorotoluene 27.9 0.50 25.0 112 70-130 3 20 4-Chlorotoluene 29.1 0.50 25.0 117 70-130 0.9 20 Dibromochloromethane 25.9 0.50 25.0 104 70-130 4 20 1,2-Dibromo-3 -chloropropane 28.1 2.5 25.0 112 63-129 0.8 I,2-Dibromoethane (EDB) 24.6 0.50 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 25.0 99 70-130 5 Dibromomethane 24.6 0.50 ugll 25.0 98 70-130 3 I,2-Dichlorobenzene 27.2 0.50 25.0 109 70-130 2 1,3-Dichlorobenzene 27.7 0.50 25.0 111 70-130 0.6 20 l,4-Dichlorobenzene 27.3 0.50 25.0 109 70-130 2 20 '--- ~ Dichlorodifluoromethane 27.2 0.50 ugll ugll ugll ugll 25 20 20 20 25.0 109 42-150 4 1,1-Dichloroethane 26.2 0.50 ugll 25.0 105 70-130 1 20 20 1,2-Dichloroethane 28.4 0.50 114 72-133 7 20 25.3 0.50 25.0 101 70-130 3 cis-l,2-Dichloroethene 24.2 0.50 25.0 97 70-130 0.4 trans-l.2-Dichloroethene 25.0 0.50 25.0 100 70-130 4 1,2-Dichloropropane 24.0 0.50 ugll ugll ugll ugll ugll 25.0 1,1-Dichloroethene 25.0 96 70-130 1 20 20 20 20 1,3-Dichloropropane 24.3 0.50 ugll 25.0 97 70-130 2 20 2,2-Dichloropropane 26.4 1.0 ugll 25.0 105 70-130 5 20 r '--.-- Chloroform Data Qualifiers , TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shallllot be reproduced, except infull, withoutwrittell permissiollfrom TestAmerica. PUF1584 TestAmerica THE LEADER IN ENVIRONMENTAL Tr:STING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 MEtH()D BL~.KlQC DATA ..•...•.• . : ~••• m _,_ b;"'.t.-••• , • VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: llF1l12 Extracted: 06/30/11 LCS Dup Analyzed: 06/30/2011 (l1Fl112-BSDl) 1,I-Dichloropropene 25.0 cis-! ,3-Dichloropropene 26.3 trans-! ,3-Dichloropropene 26.2 Ethylbenzene 27.1 Hexachlorobutadiene 28.1 2-Hexanone 24.4 Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) 30.8 30.0 28.7 24.3 27.9 Naphthalene 25.7 28.4 n-Propylbenzene 29.1 Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1, I, I-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total 25.0 Methyl-tert-butyl Ether (MTBE) 24.8 25.5 25.5 25.3 28.8 28.7 27.9 24.6 25.6 30.3 26.7 0.50 ugll 0.50 0.50 0.50 ugll ugll ugll 1.0 2.5 2.5 0.50 ugll 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 2S.0 2S.0 25.0 2S.0 25.0 2S.0 2S.0 2S.0 2S.0 2S.0 25.0 2S.0 2S.0 25.0 2S.0 2S.0 25.0 2S.0 2S.0 2S.0 25.0 2S.0 2S.0 2S.0 2S.0 2S.0 ugll 24.1 O.SO 1.0 ugll 2S.0 2S.0 2S.0 26.5 0.50 50.6 I.S ugll ugll 50.0 27.0 ugll 25.0 Surrogate: Toluene-dB 26.0 ugll 25.0 Surrogate: 4-Bromojluorobenzene 24.9 ugll 25.0 Surrogate: Dibromojluoromethane 29.0 29.1 ugll 2S.0 100 lOS lOS 109 112 98 70-130 70-130 20 0.2 70-130 70-130 70-130 44-ISO 0.04 6 123 120 lIS S8-138 70-130 70-130 2 97 III 103 70-130 61-142 70-130 I S 2 114 116 100 99 65-129 70-130 70-130 70-130 0.9 0.2 2 4 102 102 70-130 70-130 O.S 0.3 101 lIS lIS 112 70-130 70-130 70-130 70-130 0.6 2 2 3 99 102 121 70-130 70-130 78-149 0.3 107 116 116 70-130 70-130 70-130 4 4 3 96 106 S7-149 66-134 3 2 101 108 70-130 70-130 4 104 100 70-130 70-130 6 20 20 20 20 31 25 20 20 20 22 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 21 20 20 c ( c c ( ( C ( ( l ( ( C ( C ( ( ( C ( C C C C TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except injull, without written pennissionjrom TesrAmerica. PUF1584 ( ( ( ( .~ TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Sampled: 06/27/11 Received: 06/27111 Report Number: PUFI584 Attention: Joel Peterson METHOD BLANKlQC DATA VOLATILE ORGANICS BY GCIMS (EPA 5030B/S260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: IIFl1l2 Extracted: 06/30/11 r- Matrix Spike Analyzed: 06/30/2011 (llF1112-MSl) Source: PUFlS84-11 25.0 ND 47 10-150 25.0 ND 78 70-130 25.0 NO 80 70-130 25.0 ND 76 70-130 0.50 ug/l ug/l ug/l ug/l ug/l 25.0 1.66 77 70-130 1.0 ugll 25.0 0.370 66 62-126 21.7 1.0 NO 87 55-136 2.5 25.0 ND 63 22-150 21.5 0.50 25.0 ND 86 70-130 22.0 0.50 25.0 NO 88 70-130 "-..,../ tert-Butylbenzene --, Carbon disulfide ... _' Carbon tetrachloride 22.0 0.50 25.0 ND 88 70-130 25.7 0.50 25.0 ND 103 56-132 22.9 0.50 25.0 ND 91 76-131 Chlorobenzene 20.1 0.50 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 25.0 15.9 25.0 ND 80 70-130 Chloroethane Chloroform Chloromethane 19.9 1.0 ugll 25.0 NO 80 67-134 24.0 0.50 25.0 3.04 84 70-130 23.9 1.0 25.0 ND 96 50-135 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 21.1 0.50 25.0 NO 84 70-130 21.4 0.50 25.0 ND 86 70-130 19.7 0.50 ug/l ug/l ug/l ug/l ug/l 25.0 0.700 76 70-130 1,2-Dibromo-3 -chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 18.2 2.5 ugll 25.0 NO 73 60-135 18.2 0.50 ND 73 70-130 0.50 ug/l ug/l 25.0 17.8 25.0 ND 71 70-130 1,2-Dichlorobenzene 1,3-Dichlorobenzene 20.3 0.50 ugll 25.0 NO 81 70-130 20.5 0.50 25.0 ND 70-130 1,4-Dichlorobenzene Dichlorodifluoromethane _.....---" 1,1-Dichloroethane 2004 0.50 25.0 NO 82 82 22.2 0.50 25.0 ND 89 36-150 Acetone 11.8 10 ,-_' Benzene 19.6 0.50 --. Bromobenzene 20.0 0.50 Bromochloromethane '-_ Bromodichloromethane r- . Bromoform 19.0 20.9 0.50 17.0 Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene r, ~/ 21.1 0.50 ug/l ug/l ug/l ug/l 25.0 0.210 83 70-130 1,2-Dichloroethane l,l-Dichloroethene 21.2 0.50 ugll 25.0 NO 85 68-143 21.6 0.50 0.490 84 70-130 19.1 0.50 25.0 0.740 73 70-130 20.6 0.50 ug/l ug/l ug/l 25.0 cis-I,2-Dichloroethene ttans-l,2-Dichloroethene 25.0 ND 82 70-130 70-130 1,2-Dichloropropane 1,3-Dichloropropane 18.1 0.50 ugll 25.0 NO 72 70-130 17.7 0.50 25.0 ND 71 70-130 2,2-Dichloropropane 22.9 1.0 ug/l ug/l 25.0 NO 91 66-130 TestAmerica Phoenix Carlene McCutcheon Project Manager The resliits pertaill ollly to tile samples tested ill the laboratory. This reporl shall 1101 be reproduced, except ill/IIII. wilhoul writtell permissioll/rom TestAmerica. PUF1584 \ ( TestAmerica ( 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N" Tatum Blvd", Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson ( ( Sampled: 06/27111 Received: 06/27111 Report Number: PUFI584 ( ( ( ( METHOD ~LANKlQC DATA " ( ( ( TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189. Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Sampled: 06/27111 Phoenix, AZ 85028 Report Number: PUFI584 Received: 06/27/11 Attention: Joel Peterson METHOD BLANKlQC DATA VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) ,,Analyle ,.- Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Batch: llFl112 Extracted: 06/30/11 Matrix Spike Dup Analyzed: 06/30/2011 (11F1112-MSDl) Acetone 16.4 10 ,--,' Benzene 25.3 0.50 r , Bromobenzene 26.6 0.50 r- Source: PUF1584-11 25.0 ND 66 10-150 33 35 25.0 ND 101 70-130 25 20 25.0 ND 106 70-130 28 20 '-- Bromochloromethane 24.7 0.50 ugll ugll ugll ugll 25.0 ND 99 70-130 26 20 28.3 0.50 ugll 25.0 1.66 106 70-130 30 20 r', Bromodichloromethane Bromofonn 23.9 1.0 25.0 0.370 94 62-126 34 20 '0 Bromomethane 26.7 1.0 25.0 ND 107 55-136 21 24 2-Butanone (MEK) 20.0 2.5 25.0 ND 80 22-150 23 31 r-, n-Butylbenzene 28.3 0.50 25.0 ND 113 70-130 27 20 sec-Butylbenzene 28.2 0.50 ugll ugll ugll ugll ugll 25.0 ND 113 70-130 25 20 '-....- tert-Butylbenzene ---, Carbon disulfide 28.7 0.50 ND 115 70-130 26 20 0.50 ugll ugll 25.0 30.2 25.0 ND 121 56-132 16 20 ...... ' Carbon tetrachloride 28.5 0.50 25.0 76-131 22 20 26.4 0.50 ND ND 114 Chlorobenzene ugll ugll ugll 106 70-130 27 20 25.0 ND 95 67-134 17 20 ugll ugll 25.0 3.04 103 70-130 19 20 25.0 ND 115 50-135 19 20 25.0 ND 111 70-130 27 20 25.0 ND 111 70-130 26 20 r. 25.0 ..--. Chloroethane 23.7 1.0 ...... - Chlorofonn 28.9 0.50 Chloromethane 28.8 1.0 2-Chlorotoluene 27.6 0.50 4-Chlorotoluene Dibromochloromethane I ,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene IA-Dichlorobenzene '---.-/ Dichlorodifluoromethane 27.8 0.50 ugll ugll 26.7 0.50 ugll 25.0 0.700 104 70-130 30 20 26.6 2.5 ugll 25.0 ND 106 60-135 38 29 24.8 0.50 25.0 ND 99 70-130 30 20 24.1 0.50 ugll ugll 25.0 ND 96 70-130 30 20 26.6 0.50 25.0 ND 106 70-130 27 20 26.8 0.50 25.0 ND 107 70-130 26 20 26.7 0.50 25.0 ND 107 70-130 27 20 26.1 0.50 ugll ugll ugll ugll 25.0 ND 105 36-150 16 22 l,l-Dichloroethane 1,2-Dichloroethane l,l-Dichloroethene cis-l ,2-Dichloroethene trans-I,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 25.8 0.50 ugll 25.0 0.210 102 70-130 20 20 27.3 0.50 25.0 ND 109 68-143 25 20 25.4 0.50 25.0 0.490 100 70-130 16 20 23.8 0.50 25.0 0.740 92 70-130 22 20 25.5 0.50 25.0 ND 102 70-130 21 20 24.5 0.50 25.0 ND 98 70-130 30 20 24.4 0.50 25.0 70-130 31 20 1.0 ND ND 97 28.3 ugll ugll ugll ugll ugll ugll ugll 113 66-130 21 20 r' Data Qualifiers o 25.0 Ri Ri Ri Ri Ri Ri Ri Ri Ri Ri Ri Ri Ri Ri Ri Ri Ri Ri Ri Ri Ri Ri Ri Ri Ri TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced. except injull, withoutwrittenpermissiolljrol/l TestAmerica. PUFJ584 \. ( TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Synergy Environmental, LLC Project ID: PO #802.10 June 2011 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson ( Sampled: 06/27/11 Received: 06/2711 1 Report Number: PUF1584 ( ( c METHQb.llLANKlQCDATA ", ... ( c VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Result Analyte Reporting Limit Units Spike Source Level Result ( %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: 11Fl112 Extracted: 06/30/11 Matrix Spike Dup Analyzed: 06/30/2011 (l1FI112-MSDl) Source: PUFI584-11 1,1-Dichloropropene 25.7 0.50 cis-l,3-Dichloropropene trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene 25.9 27.1 0.50 0.50 0.50 25.7 1.0 26.0 ugll ugll ugll 25.0 NO 103 70-130 23 20 25.0 NO 103 70-130 20 25.0 NO 71-132 ugll 25.0 NO 104 108 ugll 25.0 NO 103 28 31 22 23 21 95 126 36 25 18 29 20 20 23.8 2.5 ugll 25.0 NO 31.5 2.5 25.0 NO 0.50 25.0 NO p-Isopropyltoluene Methylene Chloride 29.8 28.0 23.7 25.0 NO 26.4 1.0 2.5 25.0 4~Methyl~2~pentanone ugll ugll ugll ugll ugll 25.0 24.1 0.50 ugll 26.2 29.0 24.7 2.5 0.50 2-Hexanone Iodomethane Isopropy lbenzene (MIBK) Methyl~tert~butyl Ether (MTBE) Naphthalene n~Propylbenzene Styrene I, I, 1,2~ Tetrachloroethane 1,1 ,2,2~ Tetrachloroethane Tetrachloroethene Toluene I ,2,3~ Trichlorobenzene I ,2,4~ Trichlorobenzene 1,1 ,I ~ Trichloroethane 1,1 ,2~ Trichloroethane Trichloroethene Trichlorofluoromethane 0.50 70-130 66-129 18-150 47-141 20 78-137 23 70-130 25 NO 74-132 24 NO 105 56-145 25.0 NO 96 67-138 35 27 ugll 25.0 NO 105 54-135 30 25.0 25.0 25.0 25.0 NO 70-130 27 51-123 70-130 25 27 20 NO 116 99 102 99 69-133 33 20 20 26 21 33 20 21 RJ RJ RJ RJ RJ RJ RJ RJ RJ RJ RJ 25.4 0.50 24.8 0.50 27.6 0.50 ugll 25.0 1.91 103 70-130 19 20 26.1 0.50 ugll 25.0 NO 104 70-130 32 26.6 1.0 ugll 25.0 NO 106 70-130 26.7 1.0 25.0 NO 107 28.2 0.50 25.0 NO 113 66-126 76-132 20 20 20 20 23.3 30.2 28.5 0.50 ugll ugll ugll 31 31 25.0 NO 93 70-130 0.50 ugll 25.0 4.24 104 70-130 0.50 ugll 25.0 NO 114 74-150 25.6 1.0 ugll 25.0 NO 103 70-130 16 30 ugll ugll ugll ugll ugll 25.0 NO 113 70-130 25 20 RJ RJ 25.0 NO 115 61-138 26 25.0 NO 96 50-150 31 33 23 RJ 25.0 NO 107 58-139 50.0 NO 104 70-130 16 25 0.50 NO NO 28.4 0.50 0.50 Vinyl Acetate 24.1 1.0 Vinyl chloride Xylenes, Total 26.7 0.50 52.2 1.5 Surrogate: Dibromojluoromethane 25.6 ugll 25.0 103 70-130 Toluene~d8 25.6 25.0 ugll 25.0 J03 70-130 ugll 25.0 JOO 70-130 22 31 22 20 20 RJ RJ RJ RJ RJ RJ 20 20 ( ( ( c c c ( c ( c ( ( ( ( ( ( c ( 21 20 ( ( RJ RJ RJ RJ ugll ugll ugll ugll 28.9 Sun'ogate: 4-Bromojluorobenzene 20 119 112 95 I ,2,3~ Trichloropropane I ,2,4~ Trimethylbenzene I ,3,5~ Trimethylbenzene Surrogate: c c c RJ ( c ( c ( ( c TestAmerica Phoenix ( '-.,. Carlene McCutcheon ( Project Manager The results pertain only to Ihe samples lesfed in the laboratory. This report shall II0t be reproduced, except injull, without writtenpermissionjrom TestAmerica. PUF1584 C ( ( , TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix. AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.1 0 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Report Number: PUF 1584 '- Sampled: 06/27/11 Received: 06127111 DATA QUALIFIERS AND DEFINITIONS r L3 The associated blank spike recovery was above method acceptance limits. M2 Matrix spike recovery was low; the associated blank spike recovery was acceptable. Rl The RPDIRSD exceeded the method acceptance limit. R6 LFBILFBD RPD exceeded the method acceptance limit. Recovery met acceptance criteria. ND Analyte NOT DETECTED at or above the reporting limit or MDL, ifMDL is specified. RPD Relative Percent Difference TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced. except inJull, without writtenpermissionJrom res/America. PUFJ 584 ~. TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.1 0 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Report Number: PUFI584 Sampled: 06/27/11 Received: 06/27111 ( ( ( C ( C ( C C C Certification Summary TestAmerica Phoenix Method Matrix Nelac Arizona EPA 8260B Water x x ( ( ( Nevada and NELAP provide analyte specific accreditations. Analyte specific information/or TestAmerica may be obtained by contacting the laboratory or visiting our website at www.testamericainc.com ' .. C ( C C ( ( ( ( C ( ( l C ( {, ( ( ( ( C C ( C ( C TestAmerica Phoenix C Carlene McCutcheon ( Project Manager The results pertain only to the samples tested in the laboratory. This report shalll/ot be reproduced, except infull, without wri/fcnpermissionjrom Tes/Americo. PUFl584 ( ( ( TestAmerica -,usa Dsri?? 0 : ..... r e ! cOle; 8 ; 9 CHAIN OF CUSTODY FORM j II eo, Irvine, CA 92614 (949) 261-1022 FAX (949) 260-3297 , I Colton, CA 92324 (909) 370.4667 FAX (909) 370-1046 _35 SUGt" 51St St., SUllG S· 1m: PhoenIX, A2 85044 (480) 785·0043 FAX (480) 785-0851 95?? E 8 '9d MS.' as Vegas, NV 89120 (702) 798.3620 FAX (702) 798-3621 THE LEADER IN ENVIRONMENTAL TESTING Page TAl..-001S(iOO?) ProjectfPO Number: \ Of-L Analysis Required ~&::>2.., \'0 Phone Number: ._-- (ep'i)<\?>O -'2..-1rb Fax Number: . . Sample Descnptron II of Cont. Container TYp'e Special Instructions I\J\! ~~ I \ ~J.ollIl- I~ 1><1 ·If[}P \S-g'L( -c /W ~~/6 rl'L11\\~I~ I '- CfL Iw~~kl~I--;:rl\o\tl\\-i\ IYI 1 1 1 1 1 1 1 1 '" 113 l_wJ~1)1tJ '3~! 1\\c4l~XI -- o~ 1~~131\ 1\\~LMt DCI - Dr;; /W /~o~/31 \ l\tMI~A IXI b~_ I\N rwo~ 13 1 J LL'2.QLJ~Cr ~I -- o:t-i I wJ~Q"l'=J3J· 11\?..2.il1\-cA jXI~ - 0« L'liJ'~~/3 I (/\7.-¥?1 U-rA I>SI - 0:1 I~ ~rl-I?> I 'LJ\';2SI\.\G(Il':-:J~Ju I~}o / '-N ~~ 13 I J 1\4:~ I~iA I~ I - {I hi> /es-\ 't4-b 'N-4 rx. Iw 1'N... tS Iw-~ I\N -/ \N-~ \tJ--\O I\N-t\_m \/'l-'L'L Iw-\<>t_ ~_\~ bl,)~\('JJm::. A __m IW~ ( ( ( l. ~ TestAmerica THE LEADER IN ENVIRONMENTAL TESTING r-" Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ. 85028 Attention: Joel Peterson 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Report Number: PUFI619 Sampled: 06128/11 Received: 06128111 SAMPLE RECEIPT: Samples were received intact, at 2°C, on ice and with chain of custody documentation. HOLDING TIMES: All samples were analyzed within prescribed holding times and/or in accordance with the TestAmerica Sample Acceptance Policy unless otherwise noted in the report. PRESERVATION: Samples requiring preservation were verified prior to sample analysis. QA/QC CRITERIA: All analyses met method criteria, except as noted in the report with data qualifiers. Nl EPA 8260B:The RPD exceeded the acceptance limit due to sample matrix effects. RI EPA 8260B:The RPD exceeded the acceptance limit. COMMENTS: No significant observations were made. SUBCONTRACTED: No analyses were subcontracted to an outside laboratory. r '-r Reviewed By: TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shalll/ot be reproduced. except in/lIlI, without writtenpermissionji"om TestAmerica. PUF1619 TestAmerica 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Project ID: PO #802.10 June 2011 Sampled: 06/28111 Received: 06/28/11 Report Number: PUF1619 ( VOLATILE ORGANICS BY GC/MS (EPA 5030Bf8260B) Analyte Method Batch Reporting Limit llF1ll2 llFll12 llFll12 llFll12 llFll12 llF1ll2 llFll12 llFI112 11F1112 llFll12 llFll12 llFll12 llFll12 llFll12 llFll12 llFI1l2 llFll12 llFl112 11Fl112 llF1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11FI112 11F1112 11F1112 11F1112 llF1112 11F1112 11F1112 11F1112 11FI112 11Fl112 11F1112 11F1112 11FI112 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers Sample ID: PUFI6J9-0J (TB - Water) Reporting Units: ugll Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromofonn Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane l,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane l,l-Dichloroethene cis-l,2-Dichloroethene trans-l,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene cis-l,3-Dichloropropene trans-I,3-Dichloropropene Ethylbenzene Hexachlorobutadiene c "C C C ( EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND· ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 \, ( ( ( C ( ( ( ( ( ( ( ( ( , { ( ( ( ( ( l C C C C ( ( TestAmerica Phoenix ( ( Carlene McOltcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except injull, wilhoutwrillen permissionjrom TestAmerica. PUF1619 ( ( ( l ( r TestAmerica THE LEADER IN ENVIRONMENTAL TESTING r 'r 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 20ll Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/28111 Received: 06/281l1 ReportNumber: PUFI619 VOLATILE ORGANICS BY GCIMS (EPA S030B/8260B) Method Analyte Sample ID: PUF1619-01 (TB - Water) - cont. Reporting Units: ugll 2-Hexanone EPA 8260B Iodomethane EPA 8260B EPA 8260B Isopropylbenzene EPA 8260B '- p-Isopropyltoluene EPA 8260B ,- Methylene Chloride EPA 8260B '-- 4-Methyl-2-pentanone (MIBK) EPA 8260B Methyl-tert-butyl Ether (MTBE) EPA 8260B ,.. Naphthalene EPA 8260B '--, n-Propylbenzene , ,- . C~ Styrene , '--J r EPA 8260B EPA 8260B 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene EPA 8260B EPA 8260B EPA 8260B Toluene '--, 1,2,3-Trichlorobenzene r 1,2,4-Trichlorobenzene 'r '--, r EPA 8260B EPA 8260B EPA 8260B 1,1 , I-Trichloroethane 1,1,2-Trichloroethane Trichloroethene EPA 8260B EPA 8260B '-" r Trichlorofluoromethane "-~ r- "--~ EPA 8260B 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromofiuoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromofiuorobenzene (70- J30%) EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B Batch Reporting Limit IIFII12 11F1112 11F1112 IIFII12 11F1112 11F1112 IIFII12 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 IIFI112 11F1112 IIF1112 IIFI112 IIF1112 IIF1112 11F1112 IIF1112 IIF1112 IIF1112 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 Sample Dilution Date Result Factor Extracted ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 Date Analyzed Data Qualifiers 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 lJ1 % 99% 98% TestAmerica Phoenix '--- Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shalll/ot be reproduced. except in/ull, without wrillenpermissionji-om restAmerica. PUF1619 I ,~ ( TestAmerica THE: LEADER ( IN E:NVIRONMENTAl TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437 3340 Fax:(602) 454-9303 M Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/28111 Received: 06/28111 Report Number: PUP 1619 "C ( ( VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Method Ana1yle Batch Reporting Limit Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers \~ Samp1e!D: PUF1619-02 (W-13 - Water) C Reporting Units: ugll Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carhon disulfide Carbon tetrachloride Chlorohenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane l,l-Dichloroethane 1,2-Dichloroethane l,l-Dichloroethene cis-l,2-Dichloroethene trans-I,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-l ,3-Dichloropropene trans-l ,3 -Dichloropropene Ethylbenzene Hexachlorobutadiene EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B . EPA 8260B EPA 8260B EPA 8260B EPA 8260B 11Fl112 11Fl112 11Fl112 11Fll12 11F1112 11F1112 11F1112 11Fll12 11Fl112 11F1112 11Fl112 11Fl112 11Fl112 11Fl112 11F1112 11Fl112 11F1112 11Fll12 11Fl112 11Fl112 11F1112 11Fll12 11Fll12 11Fll12 11F1112 11F1112 11Fll12 11F1112 11Fl112 11F1112 11Fll12 11Fll12 11F1112 11F1112 11Fl112 11Fll12 11Fl112 11Fl112 11Fl112 11Fl112 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.8 ND ND ND ND ND ND ND ND ND ND ND 0.81 ND 2.5 3.0 ND ND ND ND ND ND ND ND ND 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 TestAmerica Phoenix Carlene McCutcheon Project Manager ( ( ~. ( ( ( C ( (, ( ( ( C ( ( ( ( ( ( ( i, C C ( C ( c ( The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except in/ull, without written permission/rom TesfAmerica. PUFl619 C C ( ( ( , (" ( TestAmerica 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437~3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING ( C Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/28111 Received: 06/28111 Report Number: PUFI619 C VOLATILE ORGANICS BY GCIMS (EPA S030B/8260B) C Reporting Sample Dilution Date Analyte Method Batch Limit Result Factor Extracted C ID: PUF1619-02 (W-13 - Water) - cont. ,( Sample Reporting Units: ugII c " r ,\.... '- ' 2-Hexanone Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl Ether (MTBE) Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1, 1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B 11F1112 11F1112 IIF1112 IIFII12 11F1112 IIFI112 IIFI112 11F1112 IIF1ll2 IIFI112 IIF1112 IIF1ll2 11F1112 IIF1ll2 IIFI112 IIFI112 IIF1112 IIFII12 11F1112 IIFI112 IIF1112 IIF1112 11FIlI2 IIF1112 IIF1112 11F1112 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 ND ND ND ND ND ND ND ND ND ND ND ND 9.3 ND ND ND ND ND 30 ND ND ND ND ND ND ND 113% 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 Date Analyzed Data Qualifiers 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 100% 102% '- TestAmerica Phoenix '---~.' Carlene McCutcheon Project Manager The results pertain Dilly to the samples tested in the laboratory. This report shall /lot be reproduced. except ;IIjull, wilhoutwrittellpermissionji'om TestAmerica. PUF1619 ( ( ( TestAmerica 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING Project!D: PO #802.10 June 20ll Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson ( ( , ( VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Method Batch Reporting Limit llFI112 IIFI112 llFIl12 I1Fll12 11F1112 llFll12 llFI112 11F1112 llFll12 llFIl12 llFI112 IIFI112 llFI112 I1F1112 llFI112 llF1ll2 11F1112 11FI112 llFIl12 llFll12 I1Fll12 I1Flll2 llFI1I2 11Flll2 lIF1112 llFll12 lIFll12 I1F1112 llFll12 11F1l12 llF1112 llFll12 11F1112 llFll12 11F1112 11F1112 I1FIl12 I1FI112 llFll12 I1Flll2 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers Sample!D: PUF1619-03 (W-2 - Water) Reporting Units: ug/1 Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromofonn Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B Chloroform EPA 8260B Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane I ,2-Dibromoethane (EDB) Dibromomethane l,2-Dichlorobenzene 1,3-Dichlorobenzene EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B l,4-Dichlorobenzene EPA 8260B Dichlorodifluoromethane EPA 8260B l,l-Dichloroethane EPA 8260B 1,2-Dichloroethane EPA 8260B l,l-Dichloroethene cis-l,2-Dichloroethene EPA 8260B trans-l,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,I-Dichloropropene cis-I,3-Dichloropropene trans-I,3-Dichloropropene Ethylbenzene Hexachlorobutadiene EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3.4 ND ND ND ND ND ND ND ND ND ND ND 2.0 ND 5.0 7.2 ND ND ND ND ND ND ND ND ND C \ Sampled: 06/28111 Received: 06/28111 Report Number: PUF1619 C 6/30/20ll 6/30/2011 6/30/2011 6/30/2011 6130120ll 613012011 6/30/20ll 6/30/2011 6/3012011 6/30/20ll 6/30/20ll 6/30/2011 6/30/2011 6/30/20ll 613012011 6/3012011 6130/2011 6130/2011 6/30/2011 6/30/2011 6/30/20ll 6/30/2011 6/30120ll 6/30/20ll 6/30/2011 6/30/2011 6/30/2011 6/30/20 II 6/30/2011 6/30120ll 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/20ll 6/30/2011 6/30/20ll 6/30/2011 613012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6130/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6130/2011 613012011 613012011 6/30/2011 6/30/20ll 6/30/2011 6/30/2011 6/30/2011 613012011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/20 II 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6/3012011 ( ( ( ( ( ( c ( ( ( ( ( ( C ( ( C ( ( C ( C ( ( r- '(" ( TestAmerica Phoenix Carlene McCutcheon ( Project Manager The results pertain only to the samples tested in the laboratory. This report shallllot be reproduced, except injull, wUhou/writtenpermissiolljrom res/America. PUFl619 ( ( l r c ,( r~ ,'- r C C C r '( "- C ,'- ,'- ,'-(-'--' '-', '-- (-. L. r '--" r '-~ '-- r '--, ,,"--, '--, ,'-- r ~, r~' c'-r ~ ~ TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/28111 Received: 06/28111 Report Number: PUFI619 VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Reporting Analyte Method Batch Limit 11F1112 IIFI112 11FII12 11F1112 IIFII12 11Fl112 11F1112 11Fll12 11Fll12 11F1112 11F1112 11F1112 IIFII12 11FII12 11FI112 11FI112 11FI112 IIFII12 11F1112 11Fll12 11FI112 IIFI1I2 11FI112 11F1112 11FI1I2 11FI112 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 Sample Dilution Result Date Factor Extracted Date Analyzed 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 Data Qualifiers Sample ID: PUF1619-03 (W-2 - Water) - cont. Reporting Units: ugll 2-Hexanone Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methy1-tert-buty1 Ether (MTBE) Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromofluoromethane (70-130%) Surrogate: Toluene-dB (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND 14 ND ND ND ND ND 75 0.52 ND ND NO ND ND ND 114% 106% 100% TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only fo the somples tested in the loboratory. This report shall not be reproduced, except in/ul!, withoutwritlenpenllissioll/rom TestAmerica. PUFl619 '--. ( TestAmerica ( 4625 East Cotton Center Blvd. Ste l89, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING Project ID: PO #802.1 0 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Received: 06/28/11 ( (~ VOLA TILE ORGANICS BY GCfMS (EPA 5030B/8260B) Method Analyte Batch Reporting Limit Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers Sample JD: PUF1619-04 (EB-2 - Water) Reporting Units: ug/l Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromofonn Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chlorofonn Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane l,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1A-Dichlorobenzene Dichlorodifluoromethane l,l-Dichloroethane 1,2-Dichloroethane l,l-Dichloroethene cis-l,2-Dichloroethene trans-l,2-Dichloroethene 1,2-Dichloropropane l,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-I,3-Dichloropropene trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene c ( ( Sampled: 06/28/11 Report Number: PUFI619 ( ( c: ( EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B 11F1112 11F1112 11F1112 IIFIlI2 IIFIlI2 IIFIlI2 IIFIlI2 11F1112 11F1112 lIFII12 IIFII12 IIFII12 11FI1l2 IIFII12 IIFlI 12 11F1112 11FlI 12 11F1112 11F1112 IIFI1l2 11FI I 12 IIF11 12 llFI1l2 11FlI 12 lIFII12 lIFII12 11F1112 IIFI1l2 IIFI1l2 IIFI1l2 11F1112 11FlI 12 11F1112 11F1112 IIFI112 IIFI1l2 11F1112 IIFI I 12 11F1112 11F1112 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6/30/2011 6/3012011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 ( ( ( \ ( ( ( ( ( ( ( ( ( C C ( C ( \ c ( ( C C ( ( ( '. C c TestAmerica Phoenix Carlene McCutcheon Project Manager ( The results pertaill ollly to the samples tested ill the laboratory. This report shallllot be reproduced, except injull, without writfenpermissionjrom TestAmerica. PUF1619 ( ( ( l ,r, c , , , ,, , ,"'- ,",'- TestAmerica 4625 East Cotton Center Blvd Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Project ID: PO #802.10 June 2011 Sampled: 06/28111 Received: 06/28111 Report Number: PUFI619 VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Method Sample ill: PUF1619-04 (EB-2 - Water) - cont. Reporting Units: ugII EPA 8260B 2-Hexanone 'EPA 8260B Iodomethane 'EPA 8260B Isopropylbenzene EPA 8260B p-Isopropyltoluene '-EPA 8260B Methylene Chloride ,-. 4-Methyl-2-pentanone (MIBK) EPA 8260B EPA 8260B Methyl-tert-butyl Ether (MTBE) '-J EPA 8260B Naphthalene EPA 8260B '-- n-Propylbenzene ,. EPA 8260B Styrene '-- ' EPA 8260B 1,1,1,2-Tetrachloroethane ,-,' 1,1,2,2-Tetrachloroethane EPA 8260B ,EPA 8260B Tetrachloroethene '---_/ EPA 8260B Toluene "'-- ' 1,2,3-Trichlorobenzene EPA 8260B EPA 8260B 1,2,4-Trichlorobenzene '--' EPA 8260B 1,1,1-Trichloroethane EPA 8260B 1,1,2-Trichloroethane '-- ' ,EPA 8260B Trichloroethene EPA 8260B ,~' Trichlorofluoromethane EPA 8260B 1,2,3-Trichloropropane '--' EPA 8260B 1,2,4-Trimethylbenzene ~~ EPA 8260B , 1,3,5-Trimethylbenzene EPA 8260B Vinyl Acetate '--' EPA 8260B Vinyl chloride EPA 8260B Xylenes, Total Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-dB (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) Batch Reporting Limit IIF1112 IIFI1I2 IIF1112 I1FII12 IIFII12 IIFI1I2 IIFI112 IIFII12 IIFII12 IIFII12 IIFII12 IIFII12 IIFII12 IIFII12 I1FII12 I1FII12 IIFII12 IIFII12 I1FII12 IIFII12 IIF1112 I1FII12 IIFII12 IIFII12 I1FII12 IIFII12 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 Sample Dilution Date Result Factor Extracted Date Analyzed 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 Data Qualifiers ,. , , , , " ". , ~, ~. ~. ~. NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 111% 104% 100% TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the labaratary. This report shall not be reproduced, except in/III/, without written permission/rom TestAmerica. PUF1619 ~ ( TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project 1D: PO #802.1 0 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Report Number: PUF1619 ( ( ( Method Analyle Batch Reporting Limit C 11FI112 11F1112 11F1112 11F1112 11F1112 11FI112 11FI112 11F1112 11FI112 11F1112 11F1112 11F1112 11F1112 IIFl112 11F1112 11F1112 11FI112 11FI112 11F1112 11F1112 IIFI112 1IFII12 11FI112 11FI112 11FI112 11F1112 11F1112 11FI112 11F1112 11FI112 11F1112 IIFI112 11FI112 11F1112 11F1112 11F1112 11F1112 11F1112 11FI112 11FI112 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers Sample ID: PUF1619-05 (W-20 - Water) ( C ( EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B Chloroe1hane Chloroform EPA 8260B Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane l,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane EPA 8260B l,l-Dichloroethane EPA 8260B l,2-Dichloroethane EPA 8260B 1,1-Dichloroethene cis-l,2-Dichloroeth ene EPA 8260B trans-l,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene cis-l,3-Dichloropropene trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene ( ( ( Sampled: 06/28/11 Received: 06/28111 VOLATILE ORGANICS BY GCIMS (EPA S030B/8260B) Reporting Units: ugll Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromofonn Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene ... EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.9 ND ND ND ND ND ND ND ND ND ND ND 1.6 ND 3.1 6.4 ND ND ND ND ND ND ND ND ND 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 TestAmerica Phoenix Carlene McCutcheon Project Manager ( ( C ( ( ( C ( ( ( ( ( ( ( C ( C ( C C ( ( C ( ( C C C ( The results pertain only 10 Ihe samples lested in the laboratory. This report shalll/ot be reproduced, except il/jull, withoufwrillenpermissionjrom TestAmerica. PUF1619 ( ( ( , ( ," ,- TestAmerica ,- THE LEADER IN ENVIRONMENTAL TESTING , \ , Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson ",- 4625 East Cotton Center Blvd Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Sampled: 06/28/11 Received: 06/28/11 Report Number: PUF1619 ,- VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) \ ,- Batch Reporting Limit 11F1112 I1F1112 11F1112 11F1112 11F1112 11FI112 11F1112 11F1112 11FI112 11F1112 11FI112 11F1112 11FI112 11Fl112 11F1112 11FI112 11FI112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 \ r Method Analyte Sample Dilution Date Result Factor Extracted Date Analyzed 6/30/2011 6/30/2011 6/30/2011 613012011 6/30/2011 6/3012011 613012011 6/30/2011 613012011 6/30/2011 6/30/2011 613012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 Data Qualifiers '-- ,- Sample ID: PUF1619-05 (W-20 - Water) - cont. ,'- Reporting Units: ugll 2-Hexanone Iodomethane \ Isopropylbenzene p-Isopropyltoluene \ Methylene Chloride '-- 4-Methyl-2-pentanone (MIBK) \ . . Methy1-tert-buty1 Ether (MTBE) Naphthalene '-- n-Propylbenzene Styrene ,'--' 1,1,1,2-Tetrachloroethane ~1,1,2,2-Tetrachloroethane '-- , " , , ,-- ,. , , Tetrachloroethene \. ~/ ,~, " ~/ ,,'/ ~ ,.---., ~- ~ Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,S-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromofluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bl'omojluorobenzene (70-130%) EPA 82608 EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 82608 EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND 9.7 ND ND ND ND ND 56 ND ND ND ND ND ND ND 114% 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 100% 98% ~ ~. TestAmerica Phoenix Carlene McCntcheon Project Manager The results pertain only to the samples tested ill the laboratory. This report shall nof be reproduced, except inJull. without wrillen permission/rom Tes/America. PUFl619 ",.( TestAmerica ( THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson ( Sampled: 06/28/11 Received: 06/28/11 Report Number: PUFI619 C ( C VOLATILE ORGANICS BY GCfMS (EPA S030Bf8260B) Analyte Method Batch Reporting Limit l1F1112 11F1112 11F1112 11F1112 IIF1112 IIF1112 IIFI112 IIFl112 IIFII12 11F1112 11F1112 11F1112 11FI112 IIF1112 IIFI112 llFII12 l1F1112 11F1112 11F1112 llFII12 IIFll12 IIF1112 IIF1112 I1F1112 IIFII12 11F1112 llFII12 IIFIll2 11F1112 l1FII12 11F1112 I1F1112 11F1112 11F1112 llFI112 11F1112 llFI1l2 IIFII12 IIFII12 I1F1112 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 Sample Dilution Date Result Factor Extracted Analyzed 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 613012011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 613012011 6/30/2011 6/30/2011 6130/2011 6/30/2011 6/30/2011 6/30/2011 613012011 6/3012011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6130/2011 6/30/2011 613012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/20 II 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 Date Data Qualifiers Sample ID: PUF1619-06 (W-21 - Water) Reporting Units: ugll Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromofonn Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3 -chloropropane 1,2-Dibromoethane (EOB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene l,4-Dichlorobenzene Dichlorodifluoromethane l,l-Dichloroethane 1,2-Dichloroethane l,l-Dichloroethene cis-l,2-Dichloroethene trans-I,2-Dichloroethene 1,2-Dichloropropane l,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene cis-l,3-Dichloropropene trans-I,3-Dichloropropene Ethylbenzene Hexachlorobutadiene ( ( EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND NO NO NO NO NO ND ND NO NO NO NO NO NO NO 2.9 NO NO NO NO NO NO NO ND NO NO ND 1.6 NO 2.6 6.2 NO NO ND ND NO NO NO NO NO ( C ( ( ( C ( C ( ( ( ( ( ( ( ( ( C ( C ( ( ( ( C C ( C C ( TestAmerica Phoenix ( Carlene McCutcheon Project Manager The results pertain only /0 the samples tested in the laboratory. This repOrt shall IIot be reproduced, except infull. without writtenpermissionfrom TestAmerica. PUFl619 C C ( ( ,~ r TestAmerica r ,~ THE LEADER IN ENVIRONMENTAL TESTING r 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 ,~ Project ID: PO #802~ 10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson , r ,r Sampled: 06/28/11 Received: 06/28111 Report Number: PUF1619 VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) r Batch Reporting Limit I1F1112 11F1112 I1F1112 I1F1112 11F1112 I1F1112 I1F1112 11FI112 llF1112 I1F1112 11FI112 llF1112 I1F1112 llFI112 I1F1112 llFI112 llFI112 llFI112 I1F1112 llFI112 llF1112 llFI112 llFI112 llFI112 llFI112 llFI112 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 "- r Method Analyte Sample Dilution Date Result Factor Extracted Date Analyzed 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 Data Qualifiers ,~ r Sample!D: PUF1619-06 (W-21- Water) - cont. ,~ Reporting Units: ugll r EPA 82608 EPA 8260B EPA 8260B EPA 82608 EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 82608 EPA 8260B EPA 8260B 2-Hexanone ,~ r Iodomethane Isopropylbenzene r p-Isopropyltoluene r Methylene Chloride "- 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl Ether (MTBE) '-' r .~ Naphthalene '-~ n-Propylbenzene Styrene '1,1,1,2-Tetrachloroethane '-' 1,1,2,2-Tetrachloroethane r Tetrachloroethene Toluene r '-' 1,2,3-Trichlorobenzene ",-. 1,2,4-Trichlorobenzene r , 1,1,1-Trichloroethane 1,1,2-Trichloroethane r TrichIoroethene Trichlorofluoromethane ' - 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5·Trimethylbenzene ' . Vinyl Acetate Vinyl chloride Xylenes, Total , ,. ,. ~ ~j ~. ~~ ,~ '--.~ ~ ~~ ~ ~~ Surrogate: Dibromof/uoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) ND ND ND ND ND ND ND ND ND ND ND ND 8_6 ND ND ND ND ND 54 ND ND ND ND ND ND ND l17% 102% 100% TestAmerica Phoenix Carlene McCutcheon Project Manager Tile results pertain only to the samples fested ill the laboratory. This report shall not be reproduced, except infull, without wri1fenpermissiolljrom Tes/America. PUF1619 ~. ( TestAmerica C THE lEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/28/11 Received: 06/28/11 Report Number: PUF1619 Method Sample!D: PUF1619-07 (W-14 - Water) Reporting Units: ugll Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane l,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane l,2-Dichlorobenzene 1,3-Dichlorobenzene l,4-Dichlorobenzene Dichlorodifluoromethane Batch Reporting Limit Sample Dilution Date Result Factor Extracted Date Analyzed ( ( ( VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Analyte ( Data Qualifiers ( ( ( C ( EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B 1,1-Dichloroethane EPA 8260B 1,2-Dichloroethane EPA 8260B l,l-Dichloroethene cis-1 ,2-Dichloroethene EPA 8260B trans-l,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene cis-l,3-Dichloropropene trans-! ,3-Dichloropropene Ethylbenzene Hexachlorobutadiene EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B l1F1112 l1F1112 llF1112 llFII12 llFI112 llF1112 l1F1112 l1F1112 l1F1112 l1FI112 llF1112 llFI112 llFII12 llFI112 l1F1112 l1F1112 l1FI112 l1F1112 11F1112 llFI112 l1FI112 l1F1112 l1F1112 l1F1112 l1F1112 llF1112 llFI112 l1F1112 llFI112 l1F1112 llFl112 l1F1112 llF1112 llFI112 llFI112 llF1112 llF1112 l1F1112 l1F1112 llFI112 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1-2 ND ND ND ND ND ND ND ND ND ND ND 4.4 ND 7.9 9.8 ND ND ND ND ND ND ND ND ND 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 C ( ( ( C ( C ( ( ( C ( ( C C ( C ( C ( C C ( C ( ( C TestAmerica Phoenix ( Carlene McCutcheon Project Manager ( The results pertain only to the samples tested in the laboratory. This report shallllot be reproduced, except infull, without writtenpermissionji-om TestAmerica. PUFI619 ( ( ( ,~ r c' r , TestAmerica 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/28111 Received: 06/28111 Report Number: PUF1619 r VOLATILE ORGANICS BY GC/MS (EPA S030B/8260B) , ~, ,----. , ,~ Method Analyte Batch Reporting Limit 11F1112 11F1112 11F1112 11F1112 11Fl112 11FI112 11F1112 11FI112 11F1112 11FI112 11FI112 11F1112 11F1112 11F1112 11FII12 11FI112 11FI112 11F1112 11F1112 11F1112 11Fl112 11F1112 11FI112 11F1112 11FI112 IIFI112 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 Sample Dilution Date Result Factor Extracted Date Analyzed 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 Data Qualifiers Sample JD: PUF1619-07 (W-14 - Water) - cont. Reporting Units: ugll 2-Hexanone Iodomethane Isopropylbenzene r p-Isopropyltoluene r Methylene Chloride '4-Methyl-2-pentanone (MIBK) " Methy1-tert-butyl Ether (MTBE) ,-' r Naphthalene 'n-Propylbenzene ,- Styrene 'r, 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane 'r'. TetrachIoroethene ~' Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene ,-" r· 1,1,1-Trichloroethane ' - 1,1,2-Trichloroethane TrichIoroethene ,- Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojlllorobenzene (70-130%) , ~ ~ ~ ~' ~ ~' ~' ~ EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND 4.6 ND ND ND ND ND 58 ND ND ND ND ND ND ND 115% 102% 104% v TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested ill the laboratory. This report shallllat be reproduced, except infull, wilhout written permissionjrom TcstAmerica. PUF1619 ~. ( TestAmerica ( THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Sampled: 06/28111 Received: 06/28111 Report Number: PUFI619 Attention: Joel Peterson Method Analyte Batch Reporting Limit 11Fl112 11FI112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11Fl112 11F1112 11FI112 11FI112 11F1112 11F1ll2 11F1112 11F1112 I1F1112 11Fl112 11F1112 11F1112 IIFI112 11F1112 11F1112 IIFI112 11F1112 11Fl112 11F1112 11F1112 11F1112 I1F1112 11F1112 11F1112 11F1112 11F1112 I1Fl112 11FI112 I1F1112 11FI112 11F1112 l1FI112 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers Sample ID: PUF1619-08 (W-15 - Water) EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B Chloroform EPA 8260B Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B 1,2-Dibromoethane (EDB) EPA 8260B Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane EPA 8260B l,l-Dichloroethane EPA 8260B 1,2-Dichloroethane EPA 8260B l,l-Dichloroethene cis-l,2-Dichloroethene EPA 8260B trans-l ,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene cis-I,3-Dichloropropene trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene ( ( ( ( VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Reporting Units: ugll Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane (. EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.4 ND ND ND ND ND ND ND ND ND ND ND 2.6 ND 4.2 5.4 ND ND ND ND ND ND ND ND ND 6/30/2011 6/30/2011 6130/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 613012011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 613012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 613012011 613012011 6/30/2011 6/3012011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 613012011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 613012011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 C , \. C ( ( ( C ( C ( ( ( C ( ( ( C (. ( C C ( ( ( (, . ( C ( ( ( ~ C C TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only (0 the somples tested in fhe laboratory. This report shall not be reproduced, except infull, without writfenpermissionjrom TestAmerica. PUF1619 ( ( ( ( ,, ,~ TestAmerica 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) THE LEADER IN ENVIRONMENTAL TESTING ,~ 454-9303 c- Project ID: PO #802.10 June 2011 Synergy Environmental, LLC , 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 c- Sampled: 06/28111 Received: 06/28111 Report Number: PUFI619 Attention: Joel Peterson r VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) .~ ,-'c- Analyte '-c- Method Batch Reporting Limit Sample Dilution Date Result Factor Extracted Date Analyzed 6/30/2011 6/30/2011 6/30/2011 613012011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/3012011 613012011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6/30/2011 6/30/2011 6130/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 Data Qualifiers Sample!D: PUF1619-08 (W-15 - Water) - cont. , ,~ Reporting Units: ugll 2-Hexanone Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride r , r '-~ ,. ~. r. ~ ,. 'r ~ 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl Ether (MTBE) Naphthalene n-Propylbenzene Styrene l,l,l,2-Tetrachloroethane . 1,1,2,2-Tetrachloroethane Tetrachloroethene r ~" ,~ ~" v ~- Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B 11F1112 11FII12 11F1112 11F1112 11FII12 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 11F1112 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 ND ND ND ND ND ND ND ND ND ND ND ND 7.1 ND ND ND NO ND 17 ND ND ND ND NO ND ND 114% 102% 96% 6/3012011 6/30/2011 613012011 6/3012011 6/3012011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/3012011 6/30/2011 TestAmerica Phoenix Carlene McCutcheon Project Manager The resllits perlaill Ollly to Ihe samples tested in Ihe laborolory. This reporl shall 1101 be reprodllced, excepl ill/IIII, withoul wriltellpermissioll/rom TestAmerica. PUF1619 \ ... C C TestAmerica THE LEAOgR IN ENIIIRONMgNTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.1 0 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson ~eport Number: Sampled: 06/28111 Received: 06/28/11 PUFI619 ( Method Analyte C Batch Reporting Limit Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers Sample!D: PUF1619-09 (W-17 - Water) Bromofonn Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane l,2-Dichlorobenzene l,3-Dichlorobenzene l,4-Dichlorobenzene Dichlorodifluoromethane l,l-Dichloroethane 1,2-Dichloroethane l,l-Dichloroethene cis-l,2-Dichloroethene trans-l,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene cis-l,3-Dichloropropene trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene ( ( ( VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Reporting Units: ugll Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane ( ( C ( EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B llFI112 llFI112 llF1112 IIF1112 IIF1112 IIFll12 IIFI112 IIFII12 llFI1l2 llFII12 llF1112 llFlll2 IIFll12 IIFI1l2 IIFI1l2 IIF1112 llFII12 llFlll2 llFlll2 IIFII12 IIFII12 llFI1l2 llFI112 IIFII12 llFlll2 IIFlll2 IIFI112 IIFI112 llFlll2 IIFII12 llFlll2 IIFII12 IIFII12 IIFI112 llFI112 llF1112 IIFI112 IIF1112 IIFll12 IIFI112 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.87 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.51 ND ND ND ND ND ND ND ND ND ND 613012011 6/30/2011 6/30/2011 6/30/20 II 6/30120 II 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/20 II 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/20 II 6/3012011 6/30/2011 6/30/2011 6/30/20 II 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30120 II 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/20 II 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/20 II 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30120 II 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/20 II 6/30/2011 613012011 6/30/2011 6/30/20 II 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/20 II 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/20 II 6/30/2011 ( ( ( C ( ( C ( c ( C ( ( C C ( r ( c ( ( C ( ( ( C ( TestAmerica Phoenix C Carlene McCutcheon ( Project Manager The results pertain ollly to the samples tested in the laboratory. This report shall not be reproduced, except injull, without writlenpermissionjrom TestAmerica. PUF1619 ( ( ( ,r r ,r ,. ,- TestAmerica %25 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) THE LEADER IN ENVIRONMENTAL TESTING 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/28111 Received: 06/28111 Report Number: PUFI619 ~ VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) "- c Batch Reporting Limit IIFI112 IIFI112 11F1112 IIF1112 IIFI112 11F1112 IIFI112 11FII12 11FII12 11FII12 11FII12 11F1112 IIF1112 11FII12 11FII12 11F1112 11FII12 11F1112 IIF1ll2 11F1112 11FIl12 11F1112 11F1112 11F1112 I1FII12 11F1112 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 ~- r- ,r Method AnaIyte Sample Dilution Date Result Factor Extracted Date Analyzed 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/3012011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 Data Qualifiers Sample!D: PUF1619-09 (W-17 - Water) - cont. ~. Reporting Units: ugll 2-Hexanone r Iodomethane ",- Isopropylbenzene p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) ,.Methyl-tert-butyl Ether (MTBE) r Naphthalene ~.' n-Propylbenzene r. Styrene v 1,1,1,2-Tetrachloroethane r ~- 1,1,2,2-Tetrachloroethane ~ EPA 8260B ~ EPA 8260B EPA 8260B EPA 8260B , EPA 8260B EPA 8260B ~. EPA 8260B ~. ~ ~. ,~~ ~" v ~ roo, ~. ~ ~'. ~-' -. v EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B Tetrachloroethene EPA 8260B Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B Trichloroethene EPA 8260B Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND 5.3 ND ND ND ND ND 0.57 ND ND ND ND ND ND ND 115% 101% 101% TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report slJallllot be reproduced, except infull, without wrillellpenllissioll/i"om TestAmerica. PUF1619 ~ .. ( TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437~3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson C c C VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Method Batch Reporting Limit Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers Sample!D: PUF1619-10 (W-16 - Water) ( C ( Reporting Units: ugll Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-0ibromoethane (EOB) Dibromomethane 1,2-Dichlorobenzene l,3-Dichlorobenzene l,4-Dichlorobenzene Dichlorodifluorornethane 1,1-Dichloroethane l,2-Dichloroethane l,l-Dichloroethene cis-l,2-Dichloroethene trans-l,2-Dichloroethene l,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-l,3-Dichloropropene trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene C ( Sampled: 06/28111 Received: 06/28111 Report Number: PUF16l9 ( ( EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B llF11l2 llF11l2 11Fll12 11Fll12 11Fl112 11F11l2 llFl112 llF11l2 IIF1112 llFll12 11Fll12 11F1112 11Fl112 11F11l2 11Fl112 11Fll12 llF11l2 IIFIl12 11F1112 llFll12 11F11l2 11F11l2 llFll12 llF11l2 llF11l2 11Flll2 11Fl112 11F11l2 llF1112 llF11l2 llF1112 IIFII12 11Fl112 11F1112 11FI112 11F1112 IIFll12 llF1112 IIFII12 11F1112 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO 0.59 NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30120 II 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 C ( ( ( ( ( C ( ( ( C ( ( C ( ( ( ( ( ( ( C C C C C ( TestAmerica Phoenix C Carlene McCutcheon Project Manager ( The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except inJull. without writlcnpermissionjrom TestAmerica. PUF1619 C ( ( ,'r TestAmerica , THE LEADER IN ENVIRONMENTAL TESTING r- r Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson , , 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Sampled: 06/28/11 Received: 06/28/11 Report Number: PUFI619 , VOLATILE ORGANICS BY GCIMS (EPA S030B/8260B) ,'-. Batch Reporting Limit 11F1112 11F1112 11F1112 11F1112 11F1112 11FII12 11Fll12 11F1112 11F1112 11FI112 IIFII12 11F1112 11FI112 IIF1112 11F1112 IIFII12 IIFII12 IIF1112 11FI112 IIF1112 IIF1112 I1FI112 IIFII12 IIFI112 I1FI112 IIFII12 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 '- r c. Method Analyte , Date Sample Dilution Date Result Factor Extracted Analyzed 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 Data Qualifiers Sample ID: PUF1619-10 (W-16 - Water) - cont. '-. Reporting Units: ugll 2-Hexanone ,'- Iodomethane Isopropylbenzene r p-Isopropyltoluene r Methylene Chloride '4-Methyl-2-pentanone (MIBK) r. ,- Methyl-tert-butyl Ether (MTBE) Naphthalene v n-Propylbenzene Styrene '-- r 1,1,1,2-Tetrachloroethane ~- 1,1,2,2-Tetrachloroethane EPA 8260B EPA 8260B ~ EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ~ r- ~. r ~ ~ .. .. ~ ,-~. ,~ EPA 8260B EPA 8260B EPA 8260B EPA 8260B Tetrachloroethene Toluene EPA 8260B EPA 8260B 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane EPA 8260B EPA 8260B EPA 8260B TrichIoroethene EPA 8260B Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) '-" Surrogate: 4-Bromojluorobenzene (70-130%) ND ND ND ND ND ND ND ND ND ND ND ND 12 ND ND ND ND ND 0.56 ND ND ND ND ND ND ND 117% 100% 99% TestAmerica Phoenix Carlene McCutcheon Project Manager The resliits pertaill ollly to the samples tested ill the laboratory. This report shall II0t he reproduced, except ill/ull, withollt wrirtellpermissiollji"om TestAmerica. PUF1619 ( ( TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. SIc 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 c Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/28111 Received: 06/28111 Report Number: PUFI619 ( c (j VOLATILE ORGANICS BY GC/MS (EPA 5030Bf8260B) Method Analyte Batch Reporting Limit IIF1110 IIFlllO IIF1110 11F1110 11F111O 11FIIIO IIFll10 IIFlllO IIF1110 IIF1110 11F1110 11F1110 11F111O 11FlllO 11FIIIO IIF1110 IIFIllO IIFlllO IIF1110 11F1110 IIFIIIO 11FlllO 11FIIIO 11FIIIO IIFlllO IIFlllO IIFIIIO 11FlllO 11F1110 11F1110 IIFI110 IIFlllO IIFlllO IIFlllO IIFlllO IIF1110 11F111O IIFIIIO I1Fll1O IIFlllO 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 Sample Dilution Date Result Factor Extracted Date Analyzed 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 613012011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/20 II 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 Data Qualifiers Sample JD: PUF1619-11 (Duplicate B - Water) Reporting Units: ugll Acetone Benzene Bromohenzene Bromochloromethane Bromodichloromethane Bromofonn Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane c ( c EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B Chloroform EPA 8260B Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane I ,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene l,4-Dichlorobenzene Dichlorodifluoromethane l,l-Dichloroethane 1,2-Dichloroethane l,l-Dichloroethene cis-l,2-Dichloroethene trans-I,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene cis-l ,3-Dichloropropene trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 82606 EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.5 ND ND ND ND ND ND ND ND ND ND ND 0.72 ND 2.8 3.2 ND ND ND ND ND ND ND ND ND ( l. ( ( ~ ( C ( C ( ( ( ( ( ( ( C C C ( ( ( ( C ( C C ( C C C C TestAmerica Phoenix Carlene McCutcheon Project Manager ( The results pertain only to the samples tested in the laboratory. This report shall not be reproduced. except infull, without written permission from TestAmerica. PUFl619 ( ( ( r TestAmerica 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437~3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING ~ . Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/28111 Received: 06/28111 Report Number: PUF1619 VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) ~ ~ Method Analyte Batch Reporting Limit 11Fl110 11F1110 11 F111 0 11FIIIO 11Fl110 11Fl110 11Fl110 11Fl110 11Fl110 llFlllO llFlllO l1F111O l1F1110 l1F1110 l1Flll0 llFlllO l1Flll0 l1Flll0 11F1110 11Fl110 11F1110 11F1110 11Fl110 11Fl110 11FI110 11FlllO 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 Date Sample Dilution Result Factor Extracted Date Analyzed Data Qualifiers Sample!D: PUFI619-11 (Duplicate B - Water) - cont. Reporting Units: ugll ,. ~' ~ ~, ~' ~' ~' ~ c' ~ r. ~ ~ ~' ~' v 2-Hexanone Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (M1BK) Methyl-tert-butyl Ether (MTBE) Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane I, I ,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND 9.6 ND ND ND ND ND 31 ND ND ND ND ND ND ND 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 613012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/3012011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6/30/2011 6130/2011 6/30/2011 97% 99% 100% TestAmerica Phoenix Carlene McCutcheon '.' Project Manager The results pertain Ollly to the samples tested ill the laboratory. This report shalf IIot be reproduced. except illju". without wriltenpermission!rom TestAmerica. PUF1619 ( TestAmerica c THe: LEADER IN ENVIRONMe:NTAL Te:STING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project lD: PO #802.10 June 2011 Synergy Environmental, LLC !O645 N. Tatum Blvd .• Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson \ ( Sampled: 06/28111 Received: 06/28111 Report Number: PUF1619 l METHOD BLANKlQC DATA. ( ( VOLATILE ORGANICS BY GC/MS (EPA 5030B/S260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC ( %REC Limits RPD RPD Limit Data Qualifiers Batch: 11 F111 0 Extracted: 06/30/11 Blank Analyzed: 06/30/2011 (11 F111 0-BLK1) ND Acetone ND Benzene Bromobenzene ND Bromochloromethane Bromodichloromethane ND Bromofonn Bromomethane ND NO ND 2-Butanone (MEK) ND n-Butylbenzene sec-Butylbenzene tert-Butylbenzene ND Carbon disulfide Carbon tetrachloride ND Chlorobenzene Chloroethane ND Chlorofonn Chloromethane NO NO NO NO NO NO 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 ND 1,2-Dibromoethane (EDB) Dibromomethane ND 1,2-Dichlorobcnzene 1,3-Dich!orobenzenc 1,4-Dichlorobenzene Dichlorodifluoromethane ND l,l-Dich!oroethane 1,2-Dichloroethane ND 0.50 0.50 NO NO 0.50 0.50 ND 0.50 0.50 l,l-Dich!oroethene cis-! ,2-Dichloroethene NO NO NO ND NO ND trans-J ,2-Dichloroethene 1,2-Dichloropropane ND 1,3-Dichloropropane 2,2-Dichloropropane ND NO ND ( C 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane ND l 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 ( ( ( ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ( ( C ( ( ( ( ( C ( ( ( ( ( ( C ( (, C c TestAmerica Phoenix ( Carlene McCutcheon Project Manager ( The results pertain only to the samples tested in the laboratory. This report shallllot be reproduced. except illjull, without wrirlenpennissionjrom Tes/America. / PUFl619 \ ( ( , , , TestAmerica , THE LEADER IN ENVIRONMENTAL TESTING Project ID: PO #802.1 0 June 2011 Synergy Environmental, LLC c 10645 N. Tatum Blvd., Suite 200-437 , Phoenix, AZ 85028 Attention: Joel Peterson 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Sampled: 06/28/11 Report Number: PUF16l9 Received: 06/28/11 ~ " METHOD BLANKlQC DATA ~. r ~ r r VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Analyte Result Reporting Limit Spike Units Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: IIFIIIO Extracted: 06/30/11 r ~ r Blank Analyzed: 06/30/2011 (IIFIIIO-BLKI) l,l-Dichloropropene NO 0.50 ugll 0.50 ugll 0.50 ugll Ethylbenzene NO NO NO 0.50 ugll Hexachlorobutadiene NO 1.0 ugll 2-Hexanone Iodomethane NO 2.5 ugll NO 2.5 ugll Isopropylbenzene NO 0.50 ugll p-Isopropylto!uene NO 0.50 ugll Methylene Chloride 1.0 ugll 4-Methyl-2-pentanone (MIBK) NO NO 2.5 ugll Methyl·tert·butyl Ether (MTBE) NO 0.50 ugll cis-l,3-Dichloropropene r. ~ ~ c· ~. ~. trans-l ,3-Dichloropropene Naphthalene NO 2.5 ugll n·Propylbenzene NO 0.50 ugll Styrene NO NO 0.50 ugll 1,1,1,2·Tetrachloroethane 0.50 ugll I, I ,2,2-Tetrachloroethane NO 0.50 ugll Tetrachloroethene NO NO 0.50 ugll Toluene 0.50 ugll 1,2,3-Trichlorobenzene NO 1.0 ugll ugll 1,2,4·Trichlorobenzene NO 1.0 1,1,1·Trichloroethane NO 0.50 ugll 1,1,2-Trichloroethane NO 0.50 ugll Trichloroethene NO 0.50 ugll Trichlorofluoromethane NO 0.50 ugll 1,2,3·Trichloropropane 1.0 ugll 1,2,4·Trimethylbenzene NO NO 0.50 ugll 1,3,5-Trimethylbenzene NO 0.50 ugll Vinyl Acetate NO 1.0 ugll Vinyl chloride NO 0.50 ugll Xylenes, Total NO 1.5 Surrogate: Dibromojllloromethane 24.0 ugll 25.0 Surrogate: Toluene·d8 24.0 ugll 25.0 Surrogate: 4·Bromojluorobenzene 23.3 ugll 25.0 ugll 96 96 93 70-130 70-130 70-130 ~. TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain ollly to the samples tested in the laboratory. This report shall not be reproduced. e.r:cept inJull, without writtellpermissionji-om TestAmerica. PUF1619 ( TestAmerica c THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd_, Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/28111 Received: 06/28111 Report Number: PUFI619 ( ( ( ( c ( Jij~:;rHC'D BLANKlQC ( c c VOLATILE ORGANICS BY GC/MS (EPA 5030B/S260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: 11Fl110 Extracted: 06/30/11 ( C C LCS Analyzed: 06/30/2011 (l1F1110-BSI) Acetone Benzene Bromobenzene Bromochloromethane 18.3 22.9 23.6 22.3 Bromodichlorometbane Bromofonn Bromomethane 2-Butanone (MEK) 23.1 23.6 20.9 22.5 n-Butylbenzene sec-Butylbenzene tert-Butylbenzene 26.2 26.6 25.2 Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chlorofonn Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene l,4-Dichlorobenzene Dichlorodifluoromethane I,I-Dichloroethane 1,2-Dichloroethane l,l-Dichloroethene cis-l,2-Dichloroethene trans-l,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 26.5 23.6 23.0 20.9 21.4 20.2 24.3 24.8 24.0 23.1 22.1 22.0 24.8 24.0 24.1 2004 21.3 21.2 22.3 22.2 22.4 21.3 20.1 23.0 10 0.50 0.50 0.50 O.SO 1.0 1.0 2.S O.SO 0.50 0.50 0.50 0.50 O.SO 1.0 O.SO 1.0 0.50 0.50 0.50 2.5 O.SO O.SO O.SO O.SO 0.50 0.50 0.50 0.50 0.50 0.50 O.SO O.SO O.SO 1.0 ug/J ug/J ug/J ugll ugll ugll ug/J ug/J ug/J ug/J ugll ug/J ugll ugll ugll ug/J ug/J ug/J ug/J ugll ugll ugll ugll ug/J ug/J ug/J ug/J ug/J ugll ug/J ugll ugll ug/J ug/J ug/J 2S.0 2S.0 2S.0 2S.0 2S.0 2S.0 2S.0 2S.0 2S.0 2S.0 2S.0 2S.0 2S.0 2S.0 2S.0 2S.0 2S.0 2S.0 25.0 2S.0 2S.0 2S.0 2S.0 2S.0 25.0 2S.0 2S.0 2S.0 2S.0 2S.0 2S.0 25.0 2S.0 2S.0 2S.0 ( 73 92 94 30-ISO 70-130 70-130 ( 89 92 94 83 70-130 70-130 67-122 64-132 ( 90 lOS 106 48-ISO 70-130 70-130 101 106 94 70-130 61-126 70-130 ( 92 84 86 70-130 69-128 70-130 ( 81 97 99 96 56-131 70-130 70-130 70-130 92 88 88 63-129 70-130 70-130 99 96 70-130 70-130 96 82 8S 70-130 42-150 70-130 85 89 72-133 70-130 89 89 70-130 70-130 85 81 92 70-130 70-130 70-130 ( ( ( ( ( C C ( C ( ( ( ( C C ( C ( C TestAmerica Phoenix ! c Carlene McCutcheon Project Manager The resul/s pertain only /0 the samples tested in the laboratory. This report shalll/ot be reproduced, except inJull, without writren permissionjrom TestAmerica. PUF1619 ( ( ( \1 .1 \l 7? jr 1411.14". 1t H. - Tes?tAmerico THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Synergy Environmental, LLC Project ID: PO #30110 June 2011 10645 N. Tatum Blvd., Suite 200-437 Sampled: 062?281?11 Phoenix, AZ 85028 Report Number: PUF1619 Received: 06t28t'11 Attention: Joel Peterson METHOD DATA VOLATILE ORGANICS BY (EPA Reporting Spike RPD Data Analyte Result Limit Units Level Limits RPD Limit Quali?ers Batch: IIF1110 Extracted: 06t?30!11 LCS Analyzed: 0680/2011 (11F1110-BSI) 1,1-Dichloropropene 22.7 0.50 ug/l 25.0 91 70-130 eis-1,3-Diehloropropene 24.2 0.50 ug/l 25 .0 97 70-130 trans-1,3-Dichloropropene 24.1 0.50 ug/l 25.0 96 70-130 26.4 0.50 ugfl 25.0 106 70-130 - Hexaehlorobutadiene 26.0 1.0 ugll 25.0 104 70-130 2-Hexanone 23.6 2.5 ug/l 25.0 94 44-1 50 Iodoniethane 25.2 2.5 ug/l 25.0 101 58-138 Isopropylbenzene 26.8 0.50 ug/l 25.0 107 70-130 p-Isopropyltoluene 27.4 0.50 ug/l 25.0 109 70-130 Methylene Chloride 21.2 1.0 ug/l 25.0 85 70-130 4-Methyl-2-pentanone (MIBK) 25.7 2.5 ug/l 25.0 103 61 -142 Methyl-tert-butyl Ether (MTBE) 20.0 0.50 ug/l 25 .0 80 70-130 Naphthalene 25.1 2.5 ugll 25.0 101 65-129 n-Propylbenzene 26.9 0.50 ug/l 25.0 108 70-130 Styrene 26.0 0.50 ug/l 25.0 104 70-130 1,1,1,2-Tetraehloroethane 23.3 0.50 ug/l 25.0 93 70-130 1,1,2,2-Tetrachloroethane 17.9 0.50 ugll 25.0 72 70-130 Tetrachloroethene 23.7 0.50 ug/l 25.0 95 70-1 30 Toluene 24.7 0.50 ug/l 25.0 99 70-130 1,2,3-Trichlorobenzene 25.6 1.0 ug/l 25.0 103 70-130 1,2,4-Trichlorobenzene 25.1 1.0 ug/l 25.0 1 00 70-130 22.0 0.50 ug/l 25.0 88 70-130 1,1,2-Trichloroethane 22.0 0.50 ugll 25.0 88 70-130 Trichloroethene 23 .2 0.5 0 1130 25.0 93 70-130 - Triehlorofluoromethane 23.5 0.50 ug/l 25.0 94 78-149 1,2,3?Trichloropropane 20.8 1.0 ug/l 25.0 83 70-130 26.9 0.50 ug/l 25.0 108 70-130 1,3,5-Trimethy1benzene 26.5 0.50 ug/l 25.0 106 70-130 Vinyl Acetate 20.5 1.0 ug/l 25.0 82 57-149 Vinyl chloride 22.0 0.50 ug/l 25.0 88 66-134 Xylenes, Total 52.1 1.5 ug/l 50.0 104 70-130 Surrogate: 23.1 ttg/I 25.0 92 70-130 Surrogate: Toluene-d8 25.0 ttg/I 25.0 100 70-130 Surrogate: 4-Bromo?ttorobenzette 25.2 ttg/I 25.0 101 70-130 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain om); to the samples tested in the toborotmy. This report shalt not be reproduced, except tofu?, written TestAmert'co. PUFI619 ~ TestAmerica ( c 4625 East Cotton Center Blvd. Ste 189, Phoenix. AZ 85040 (602) 437-3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING Project ID: PO #802.10 June 2011 Synergy Environmental, LLC Phoenix, AZ 85028 -( Sampled: 06/28111 Received: 06/28111 10645 N. Tatum Blvd., Suite 200-437 Report Number: PUF1619 ( ( Attention: Joel Peterson ( METHon':BEANKlQC DATA ( " "".,)1 I.. VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result ( %REC e %REC Limits RPD RPD Limit Data Qualifiers Batch: llFU10 Extracted: 06/30/11 ( ( ( LCS Dup Analyzed: 06/3012011 (lIF1110-BSDl) Acetone 17.8 25.0 0.50 ugll ugll ugll ugll 25.6 0.50 ugll 25.0 1.0 ugll 10 Benzene 25.0 0.50 Bromobenzene 24.7 0.50 Bromochloromethane 23.8 Bromodichloromethane Bromoform 71 30-150 3 35 25.0 100 70-130 9 20 25.0 99 70-130 5 20 25.0 95 70-130 6 20 25.0 102 70-130 10 20 25.0 100 67-122 6 20 25.0 88 64-132 92 48-150 6 2 20 25.0 25.0 120 70-130 14 20 25.0 114 70-130 7 20 7 3 20 ( ( ( ( ( Bromomethane 22.1 1.0 2-Butanone (MEK) 22.9 2.5 n-Butylbenzene 0.50 sec-Butylbenzene 30.0 28.5 tert-Butylbenzene 27.0 0.50 ugll ugll ugll ugll ugll 25.0 108 70-130 Carbon disulfide 27.2 0.50 ugll 25.0 109 61-126 Carbon tetrachloride 26.3 0.50 105 70-130 11 20 ( 25.4 0.50 25.0 102 70-130 10 20 Chloroethane 22.4 1.0 25.0 89 69-128 7 20 ( Chloroform 23.0 0.50 ( Chloromethane 21.0 1.0 2-Chlorotoluene 25.6 0.50 4-Chlorotoluene 26.8 0.50 ugll ugll ugll ugll ugll ugll ugll 25.0 Chlorobenzene Dibromochloromethane 26.9 0.50 ugll 1,2-Dibromo-3-chloropropane 25.0 2.5 1,2-Dibromoethane (EDB) 24.6 0.50 Dibromomethane 24.3 0.50 1,2-Dichlorobenzene 26.6 0.50 1,3-Dichlorobenzene 25.8 0.50 1,4-Dichlorobenzene 26.0 0.50 Dichlorodifluoromethane 21.8 1,I-Dichloroethane 23.0 1,2-Dichloroethane 0.50 33 20 ( ( ( 25.0 92 70-130 7 20 25.0 84 56-131 4 20 25.0 102 70-130 5 20 25.0 107 70-130 8 20 25.0 108 70-130 11 20 25.0 100 63-129 8 25 C 25.0 99 70-130 11 20 ( 25.0 97 70-130 10 20 25.0 106 70-130 7 20 ( 25.0 103 70-130 7 20 25.0 104 70-130 8 20 ( 0.50 ugll ugll ugll ugll ugll ugll ugll 25.0 87 42-150 7 20 ( 0.50 ugll 25.0 92 70-130 7 20 22.8 0.50 25.0 91 72-133 7 20 ( 25.0 94 70-130 6 20 25.0 95 70-130 6 20 I,l-Dichloroethene 23.6 0.50 cis-I,2-Dichloroethene 23.6 0.50 ugll ugll ugll trnns-l,2-Dichloroethene 23.4 0.50 ugll 25.0 94 70-130 5 20 1,2-Dichloropropane 23.7 0.50 ugll 25.0 95 70-130 11 20 l,3-Dichloropropane 22.3 0.50 ugll 25.0 89 70-130 10 20 2,2-Dichloropropane 22.3 1.0 ugll 25.0 89 70-130 3 20 TestAmerica Phoenix Carlene McCutcheon Project Manager ( ( C ! C C C ( The results pertain only to the samples tested in fhe laboratory. This report shall not be reproduced, except infull, withoutwrittenpermissionji-om TestAmerica. PUF1619 ( ( ( r TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/28111 Received: 06/28/11 Report Number: PUF16l9 METHOD BLANIDQC DATA VOLATILE ORGANICS BY GCIMS (EPA 5030B/S260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: llFlllO Extracted: 06/30/11 LCS Dup Analyzed: 06/30/2011 (l1Fl110-BSDl) 1,1-Dichloropropene '-- . cis-l ,3-Dichloropropene r-" trans-!,3 -Dichloropropene ~' Ethylbenzene '--- ,. Hexachlorobutadiene 2-Hexanone Iodomethane Isopropylbenzene p-Isopropyltoluene ~~ Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl Ether (MTBE) Naphthalene r n-Propylbenzene Styrene 1, 1,1,2-Tetrachloroethane 1, I ,2,2-Tetrachloroethane Tetrachloroethene '-- Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1, I-Trichloroethane 1, I,2-Trichloroethane .... -. Trichloroethene 24.8 26.7 26.6 2S.7 2S.0 26.5 26.9 28.0 29.9 22.4 29.1 21.4 28.S 28.8 28.6 25.7 19.4 25.6 26.9 29.9 28.6 23.6 24.7 Trichlorofluoromethane 1,2,3-Trichloropropane 25.6 24.5 22.0 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene 29.4 28.4 Vinyl Acetate Vinyl chloride 22.9 23.5 0.50 0.50 0.50 0.50 1.0 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 ugll ugll ugll 25.0 25.0 25.0 ugll 25.0 25.0 25.0 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 99 107 70-130 70-130 106 115 112 70-130 70-130 70-130 106 44-150 58-138 70-130 25.0 25.0 25.0 25.0 108 112 120 25.0 25.0 116 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 89 85 115 115 114 103 77 102 lOS 120 114 95 99 102 ugll ugll ugll ugll 25.0 25.0 98 25.0 25.0 liS ugll ugll 25.0 25.0 Xylenes, Total 56.S ugll 50.0 Surrogate: Dibromojluoromethal1e 23.0 ugll 25.0 Surrogate: Toluene-dB 25.3 ug/l 25.0 Surrogate: 4-Bromojluorobenzene 26.0 ug/l 25.0 88 114 92 94 114 92 101 104 70-130 70-130 61-142 70-130 65-129 70-130 9 20 10 10 20 20 20 8 7 12 7 20 31 25 5 9 20 20 5 20 22 13 6 14 7 20 20 20 70-130 70-130 70-130 10 8 20 70-130 70-130 70-130 S 9 20 15 20 13 7 20 20 11 10 20 20 4 20 5 20 9 7 20 70-130 70-130 70-130 70-130 78-149 70-130 70-130 70-130 57-149 66-134 70-130 10 20 20 20 20 II 21 7 20 20 9 70-130 70-130 70-130 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only 10 Ihe samples tested in the laboratory. n,is report shall not be reprodllced, except in/lIl1, witholll wrillenpermissionji-om TestAmerica. PUF1619 \.. ( TestAmerica ( 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/28111 Received: 06/28111 Report Number: PUFI619 ,./.METHOD BLANKlQC DATA "";';;'2<"' ' ,,', 'J;++::,0G"""~ .. ,~,~~~,,~_,, VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC C %REC Limits RPD RPD Limit Data Qualifiers l Batch: llFlllO Extracted: 06/30/11 Matrix Spike Analyzed: 06/30/2011 (lIFlIIO-MSl) c Source: PUF1619-11 25.0 ND 57 10-150 25.0 94 94 70-130 25.0 ND ND 25.0 ND 87 70-130 ( ( 0.50 ugll ugll ugll ugll ugll 25.0 ND 95 70-130 ( 22.9 1.0 ugll 25.0 ND 92 62-126 Bromomethane 2-Butanone (MEK) 20.8 1.0 25.0 83 55-136 20.0 2.5 25.0 ND ND 80 22-150 n-Butylbenzene sec-Butylbenzene tert-Butylbenzene 27.0 0.50 ugll ugll ugll 25.0 ND 108 70·130 27.6 0.50 ugll 25.0 70-130 0.50 ugll 25.0 Carbon disulfide Carbon tetrachloride 24.2 0.50 ugll 25.0 25.3 0.50 23.9 0.50 25.0 21.1 1.0 ugll ugll ugll 25.0 Chlorobenzene Chloroethane ND ND ND ND ND 110 27.0 25.0 Acetone 14.2 10 Benzene 23.6 0.50 Bromobenzene Bromochloromethane Bromodichloromethane 23.6 0.50 21.8 0.50 23.8 Bromofonn 70-130 ( 108 70-130 97 56-132 101 76-I3I ( 96 70-130 ND 84 67-134 ( C Chlorofonn 23.7 0.50 ugll 25.0 2.52 Chloromethane 19.0 1.0 ugll 25.0 ND 85 76 50-135 2-Chlorotoluene 25.3 0.50 25.0 ND 101 70-130 ( 4-Chlorotoluene 25.8 0.50 ugll ugll 25.0 70-130 ( 23.9 0.50 ugll 25.0 96 70-130 21.8 2.5 ugll 25.0 ND ND ND 103 Dibromochloromethane 1,2-Dibromo-3 -chloropropane 87 60-135 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 22.1 0.50 ugll 25.0 ND 88 70-130 21.6 0.50 25.0 ND 70-130 24.5 0.50 25.0 ND 86 98 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 24.2 0.50 ugll ugll ugll 25.0 ND 97 70-130 ( ( ~ 70-130 24.3 0.50 ugll 25.0 70-130 0.50 ugll 25.0 ND ND 97 21.5 86 36-150 24.4 0.50 25.0 0.720 95 70-130 21.0 0.50 25.0 ND 84 68-143 25.5 0.50 25.0 2.82 91 70-130 ( 25.0 3.18 88 70-130 ( 25.0 ND 91 70-130 ND ND ND 86 70-130 c 80 70-130 93 66-130 ( 1,1-Dichloroethene cis-I,2-Dichloroethene trans-I,2-Dichloroethene 25.2 0.50 22.7 0.50 ugll ugll ugll ugll ugll 1,2-Dichloropropane 21.4 0.50 ugll 25.0 1,3-Dichloropropane 2,2-Dichloropropane 20.1 0.50 ugll 25.0 23.3 1.0 ugll 25.0 l,l-Dichloroethane 1,2-Dichloroethane 70·130 ( C ( TestArnerica Phoenix Carlene McCutcheon Project Manager ( The results pertain only to the samples tested in the laboratory. This report shalll/ot be reproduced, except inJull, without writlenpermissionjrom TesfAmerica. PUF1619 C ( ( , ( , TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/28111 Received: 06/28111 Report Number: PUF1619 METHOD BLANKlQC DATA VOLATILE ORGANICS BY GCIMS (EPA 5030B/S260B) Analyte ,--- Result Reporting Limit Units Spike Level Source Result %JU[C %JU[C Limits RPD Source: PUF1619-11 25.0 NO 96 70-130 0.50 ugll ugll 25.0 NO 96 70-130 23.7 0.50 ugll 25.0 NO 95 71-132 27.5 0.50 25.0 NO 110 70-130 "- . Hexachlorobutadiene ,--- 2-Hexanone Iodomethane 27.0 1.0 ugll ugll 25.0 NO 108 66-129 22.1 2.5 ugll 25.0 NO 88 18-150 25.4 2.5 25.0 NO 102 47-141 ,---. 28.0 0.50 25.0 NO 112 78-137 28.3 0.50 25.0 NO 113 70-130 25.0 NO 83 74-132 25.0 NO 95 56-145 25.0 NO 70 67-138 25.0 1.02 94 54-135 25.0 NO 112 70-130 25.0 NO 102 51-123 l,l-Dichloropropene 23.9 0.50 cis-l,3-Dichloropropene 24.1 trans-l ,3-Dichloropropene Ethylbenzene Methylene Chloride 20.8 1.0 ,---. 4-Methyl-2-pentanone (MIBK) 23.7 2.5 r' Methyl-tert-butyl Ether (MTBE) 17.5 0.50 ,--. Naphthalene 24.5 2.5 n-Propylbenzene 28.0 0.50 Styrene 25.6 0.50 23.8 0.50 25.0 NO 95 70-130 17.5 0.50 ugll 25.0 NO 70 69-133 33.8 0.50 9.58 97 70-130 0.50 ugll ugll 25.0 25.1 25.0 NO 101 70-130 25.6 1.0 ugll 25.0 NO 102 70-130 25.0 1.0 25.0 NO 100 66-126 23.0 0.50 ugll ugll 25.0 NO 92 76-132 21.3 0.50 ugll 25.0 NO 85 70-130 51.5 0.50 31.4 81 70-130 24.5 0.50 25.0 NO 98 74-150 20.1 1.0 25.0 NO 80 70-130 27.0 0.50 25.0 NO 108 70-130 27.6 0.50 25.0 NO 111 61-138 20.6 1.0 25.0 NO 82 50-150 22.8 0.50 25.0 NO 91 58-139 '--_" Xylenes, Total 53.6 1.5 ugll ugll ugll ugll ugll ugll ugll ugll 25.0 '---- 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 50.0 NO 107 70-130 Surrogate: Dibromojluoromethane 22.6 ugll 25.0 90 70-130 Surrogate: Tolue1le-dB 25.1 ug/l 25.0 70-130 Surrogate: 4-Bromojluorobenzene 25.7 IIgll 25.0 100 103 Isopropylbenzene r, p-IsopropyIto!uene '-'---_ '- '-- Data Qualifiers Batch: 11F1110 Extracted: 06/30/11 Matrix Spike Analyzed: 06/30/2011 (l1Fl110-MSl) r- RPD Limit 70-130 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertaill ollly to the samples tested ill the laboratory. This reporr shall not be reproduced, except infull, withoutwriltell permissionFom restAmerica. PUFl619 c ( TestAmerica ( 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 mE LEADER IN ENVIRONMENTAL TESTING Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Sampled: 06/28/11 Received: 06/28/11 Report Number: PUF1619 ( Attention: Joel Peterson ( ME'IiIOD BLANKIQC DATA C l. ( VOLATILE ORGANICS BY GCIMS (EPA S030B/8260B) Reporting Analyte Result Limit Spike Units Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: IIF1110 Extracted: 06/30111 Matrix Spike Dup Analyzed: 06/30/2011 (l1Fl110-MSDl) Acetone ( ugll ugll ugll ugll 25.0 0.50 1.0 15.0 10 Benzene 22.3 0.50 Bromobenzene 23.4 0.50 Bromochloromethane 21.4 0.50 Bromodichloromethane 22.1 Bromofonn 20.3 Source: PUF1619-11 ND 60 10-150 5 35 ( '- c c ( 25.0 ND 89 70-130 6 20 25.0 ND 93 70-130 0.9 20 25.0 ND 86 70-130 2 20 ( ugll 25.0 ND 88 70-130 7 20 ( ugll 25.0 ND 81 62-126 12 20 ( Bromomethane 20.2 1.0 ugll 25.0 ND 81 55-136 3 24 2-Butanone (MEK) 21.1 2.5 25.0 ND 84 22-150 25.3 0.50 25.0 ND 101 70-130 6 7 31 n-Butylbenzene 20 sec-Butylbenzene 25.5 0.50 25.0 ND 102 70-130 8 20 tert-Bulylbenzene 25.1 0.50 ugll ugll ugll ugll 25.0 ND 100 70-130 20 Carbon disulfide 15.3 0.50 ugll 25.0 ND 61 56-132 7 45 Carbon tetrachloride 0.50 ugll 25.0 ND 92 76-131 10 20 ( 0.50 ugll 25.0 ND 91 70-130 5 20 Chloroethane 22.9 22.8 20.9 1.0 ugll 25.0 ND 84 67-134 I 20 C Chloroform 23.1 0.50 ugll 25.0 2.52 82 70-130 3 20 ( Chloromethane 19.3 1.0 25.0 ND 77 50-135 20 2-Chlorotoluene 23.6 0.50 25.0 ND 94 70-130 7 24.6 0.50 25.0 ND 98 70-130 Dibromochloromethane 21.8 0.50 25.0 ND 87 70-130 5 9 1,2-Dibromo-3 -chloropropane 22.4 2.5 ugll 25.0 ND 89 60-135 2 20 20 20 29 ( 4-Chlorotoluene ugll ugll ugll ugll Chlorobenzene 20 ( ( NJ c ( ( ( 1,2-0ibromoethane (BOB) 22.4 0.50 ugll 25.0 ND 90 70-130 2 20 Oibromomethane 21.4 0.50 ugll 25.0 ND 86 70-130 0.5 1,2-Dichlorobenzene 23.5 0.50 25.0 ND 94 70-130 4 1,3-Dichlorobenzene 23.4 0.50 25.0 ND 94 70-130 3 1,4-Dichlorobenzene 23.4 0.50 25.0 ND 93 70-130 4 20 20 20 20 Dichlorodifluoromethane 20.8 0.50 25.0 ND 83 36-150 3 22 ( 25.0 0.720 83 70-130 12 20 ( 25.0 ND 84 68-143 0.2 20 25.0 2.82 88 70-130 2 20 25.0 3.18 83 70-130 5 4 l,l-Dichloroethene 24.9 0.50 cis-I,2-Dichloroethene 24.0 0.50 ugll ugll ugll ugll ugll ugll ugll ugll trans-I,2-Dichloroethene 21.7 0.50 ugll 25.0 ND 87 70-130 1,2-Dichloropropane 20.7 0.50 ugll 25.0 ND 83 70-130 3 1,3-Dichloropropane 20.2 0.50 ugll 25.0 ND 81 70-130 0.9 20 20 20 20 2,2-Dichloropropane 23.1 1.0 ugll 25.0 ND 92 66-130 0.9 20 1,1-Dichloroethane 21.6 0.50 1,2-Dichloroethane 21.0 0.50 TestAmerica Phoenix Carlene McCutcheon Project Manager C c ( The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except inJull, without written pennissionJrom Tcs/Amcrica. PUFI619 { ( ( TestAmerica c THE LEADER IN ENVIRONMENTAL TESTING Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson " 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Sampled: 06128111 Received: 06/28/11 Report Number: PUFI619 METHOD BLANKlQC DATA VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Reporting AnaJyte Result Limit Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: llFlUO Extracted: 06/30/11 r- Matrix Spike Dup Analyzed: 06/30/2011 (I1FllIO-MSDl) l,l-Dichloropropene 22.5 0.50 cis-l,3-Dichloropropene 21.8 0.50 ~ Units '--- ~ "--_ '-....--- 90 70-130 6 20 ND 87 70-130 10 20 0.50 ugll 25.0 ND 88 71-132 8 20 25.5 0.50 25.0 ND 102 70-130 8 20 Hexachlorobutadiene 25.3 1.0 ugil ugil 25.0 ND 101 66-129 7 21 2-Hexanone 23.2 2.5 ugll 25.0 5 25 24.8 2.5 25.0 47-141 2 29 Isopropylbenzene 26.4 0.50 ugil ugil 93 99 18-150 Iodomethane 105 78-137 6 20 p-Isopropyltoluene 25.9 0.50 ugll 25.0 103 70-130 9 20 Methylene Chloride 20.6 1.0 25.0 ND ND ND ND ND 82 74-132 I 20 24.7 2.5 25.0 ND 56-145 4 26 18.7 0.50 25.0 ND 99 75 67-138 7 21 23.9 2.5 25.0 1.02 91 54-135 33 n-Propylbenzene 26.2 0.50 25.0 ND 105 70-130 Styrene 24.0 0.50 25.0 23.2 0.50 I,I,2,2-Tetrachloroethane 18.6 0.50 25.0 Tetrachloroethene 32.5 0.50 25.0 9.58 70-130 Toluene 23.8 0.50 25.0 ND 96 93 75 92 95 51-123 1,I,1,2-Tetrachloroethane ND ND ND 3 7 6 3 6 4 70-130 5 20 1,2,3-Trichlorobenzene 25.2 1.0 25.0 101 70-130 I 20 1,2,4-Trichlorobenzene 24.3 1.0 25.0 ND ND 97 66-126 1,1,1-Trichloroethane 22.3 0.50 25.0 ND 89 76-132 3 3 25.0 ND 86 70-130 I 25.0 31.4 73 70-130 4 20 20 20 25.0 ND I 20 ND 70-130 ND 25.0 ND 104 61-138 8 6 6 20 25.0 97 87 102 74-150 25.0 ND 78 50-150 5 23 3 9 20 25.0 1,1,2-Trichloroethane 21.5 0.50 Trichloroethene 49.6 0.50 Trichlorofluoromethane 24.2 0.50 1,2,3-Trichloropropane 21.7 1.0 1,2,4-Trimethylbenzene 25.5 0.50 1,3,5-Trimethylbenzene 26.0 0.50 ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil Vinyl Acetate 19.5 1.0 ugll 25.0 Vinyl chloride 22.1 0.50 ND 88 58-139 49.1 1.5 ugil ugil 25.0 Xylenes, Total 50.0 ND 98 70-130 Methyl-tett-butyl Ether (MTBE) ,"---,' Naphthalene v r, ND 25.0 21.9 '---_' 4-Methyl-2-pentanone (MLBK) r-, 25.0 Ethylbenzene '. trans-l,3-Dichloropropene ~ Source: PUFI619-11 ugil ugil 25.0 70-130 69-133 70-130 Surrogate: Dibrolnojluoromethane 23.4 lIg/l 25.0 24.6 ug/l 25.0 94 99 70-130 Surrogate: Toluene-d8 Surrogate: 4-Bromojluorobenzene 25.3 ug/I 25.0 101 70-130 20 21 20 20 20 20 20 33 21 70-130 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except infull, without wriffenpermissionjrom TestAmerica. PUF1619 c (, TestAmerica ( THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189. Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.1 0 June 20\1 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson ( ~. Sampled: 06/28/11 Received: 06/28/11 Report Number: PUFI619 C ( ( ( METHOD BLANKJQC;:; DATA ( ,,- VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC ( %REC Limits RPD RPD Limit Data Qualifiers Batch: 11F1112 Extracted: 06/30/11 Blank Analyzed: 06/3012011 (l1Fl112-BLKl) Acetone NO Benzene NO Bromobenzene NO Bromochloromethane NO Bromodichloromethane NO Bromoform NO Bromomethane NO 2-Butanone (MEK) NO n-Butylbenzene sec-Butylbenzene tert-Butylbenzene NO Carbon disulfide NO Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane l,l-Dichloroethane 1,2-Dichloroethane l,l-Dichloroethene cis-l,2-Dichloroethene trans-I,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO lO 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 C ( ( ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll C ( ( ( \ ( ( ( ( ( ( ( ( ( C ( C C C C C ( '--- ( TestAmerica Phoenix , ( c Carlene McCutcheon Project Manager The results pertain only 10 the samples lesled in the laboratory. This report shall not be reproduced, except in/ull, without writtenpennission/rom TestAmerica. PUFl619 ( ( ( l r ,- TestAmerica ,- THE LEADER IN ENVIRONMENTAL TESTING r r , r 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/28/11 Received: 06/28/11 Report Number: PUFI619 r '- r METHOD BLANKlQC DATA '-- ,'-- ,- VOLATILE ORGANICS BY GCIMS (EPA 5030Bf8260B) '- r ,. AnaIyte ,.'- Batch: 11 Fl112 Extracted: 06/30!11 Result Reporting Limit Spike Units Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers '- r '-.. r '... ,... ,... '-.-' Blank Analyzed: 06/30/2011 (I1FI112-BLKl) ND I,I-Dichloropropene cis-l,3-Dichloropropene ND trans-l,3-Dichloropropene ND Ethylbenzene ND Hexachlorobutadiene r 2-Hexanone '--"' Iodomethane ,... ~. '-. ,... '-.- ,... ND ND ND Isopropylbenzene ND p-Isopropyltoluene ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl Ether (MTBE) Naphthalene r n-Propylbenzene '- " Styrene r 1, I, I ,2-Tetrachloroethane r' 1, 1,2,2-Tetrachloroetlfane Tetrachloroethene r '- Toluene ,.. 1,2,3-Trichlorobenzene '--" 1,2,4-TrichlorObenzene 1, I ,I-Trichloroethane r. 1,1,2-Trichloroethane '--" Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane '-.-. 1,2,4-Trimethylbenzene r 1,3,5-Trimethylbenzene Vinyl Acetate '--" Vinyl chloride Xylenes, Total ''--" ~ ~ ND ND ND ND ND ND ND ~ ~. ~ ~. ND ND ND ND ND ND ND ND ND ND 0.50 0.50 0.50 0.50 1.0 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 ugll LO LO ugll ugll ugll 0.50 0.50 0.50 0.50 LO ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ND 0.50 0.50 ND LO ugll ugll ND 0.50 1.5 ugll ugll ND Sllrrogate: Dibroillojluoromethane 28.3 ug/I 25.0 113 70-130 ~. Surrogate: Toluene-dB 25.3 ug/l 25.0 101 70-130 , Surrogate: 4-Bromojluorobenzel1e 24.8 ugll 25.0 99 70-130 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced. except injull, without wril1cnpermissionji-om TestAmerica. PUFl619 "--. ( TestAmerica ( '---- THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Sampled: 06/28111 Received: 06/28111 Report Number: PUF 1619 Phoenix, AZ 85028 Attention: Joel Peterson VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC ( %REC Limits RPD RPD Limit Data Qualifiers Batch: llFI112 Extracted: 06/30/11 LCS Analyzed: 06/3012011 (l1Fl112-BSJ) Acetone 18.6 10 ugil 0.50 0.50 0.50 ugil 0.50 1.0 1.0 2.5 0.50 ugil Benzene Bromobenzene Bromochloromethane Bromodichloromethane 25.0 26.5 25.2 27.2 Bromofonn Bromomethane 2·Butanone (MEK) 24.0 25.9 22.3 n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide 29.8 29.0 28.5 29.2 Carbon tetrachloride Chlorobenzene 29.1 26.5 0.50 0.50 ugil Chloroethane Chloroform Chloromethane 2-Chlorotoluene 24.5 27.6 30.4 28.7 1.0 0.50 1.0 0.50 4-Chlorotoluene Dibromochloromethane I,2-Dibromo-3-chloropropane 29.4 27.1 28.3 0.50 0.50 2.5 ugil ugil ugil ugil ugil ugil ugil 0.50 0.50 0.50 ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil I,2-Dibromoethane (EDB) Dibromomethane I,2-Dichlorobenzene 25.9 25.3 27.8 0.50 0.50 0.50 I,3-Dichlorobenzene 1A-Dichlorobenzene Dichlorodifluoromethane 27.9 27.9 28.4 0.50 0.50 0.50 l,l-Dichloroethane l,2-Dichloroethane 25.9 30.4 0.50 0.50 I,l-Dichloroethene cis-I,2-Dichloroethene trans-I,2-Dichloroethene 24.6 24.1 24.0 0.50 0.50 24.3 24.7 0.50 0.50 0.50 ugil 1,2-Dichloropropane I,3-Dichloropropane 2,2-Dichloropropane 27.7 1.0 ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil ugil 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 c c ( c c c c Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tiltum Blvd., Suite 200-437 ( c ( ( 74 30-150 100 106 101 109 70-130 70-130 70-130 70-130 96 104 89 67-122 64-132 48-150 119 116 114 117 70-130 70-130 70-130 61-126 116 106 98 70-130 70-130 69-128 III 122 115 70-130 56-131 70-130 118 108 113 70-130 70-130 63-129 104 101 III 112 70-130 70-130 70-130 70-130 ( 112 114 70-130 42-150 ( 104 121 70-130 72-133 98 96 70-130 70-130 96 97 99 70-130 70-130 70-130 III 70-130 , ( ( ( ( ( ( ( ( C c.. C ( C ( C C C C ( ( ( TestAmerica Phoenix ( Carlene McCutcheon Project Manager C The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except injull, without writtenpennissionjrom TestAmerica. PUFl619 ( ( ( , , , TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 Synergy Environmental, LLC Sampled: 06/28111 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Received: 06/2811 I Report Number: PUF1619 Attention: Joel Peterson METHOD BLANKlQC DATA VOLATILE ORGANICS BY GC/MS (EPA S030B/S260B) Analyte r Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: llFI112 Extracted: 06/30111 '-. =: r \ LeS Analyzed: 06/30/2011 (I1FI112-BSI) 25.3 1,I-Dichloropropene 26.3 cis-! ,3-Dichloropropene 0.50 27.8 0.50 27.4 0.50 28.0 1.0 2-Hexanone 26.0 2.5 Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride 30.4 2.5 29.6 0.50 29.4 0.50 24.0 1.0 4-Methyl-2-pentanone (MIBK) 29.3 2.5 Methyl-tert-butyl Ether (MTBE) 26.2 0.50 28.6 2.5 '--_ ,-, trans-I,3-DichloTopropene '-.-" r ' Ethylbenzene ,-/ Hexachlorobutadiene "--_ ,,- "--J' Naphthalene ,. n-Propylbenzene Styrene 1,1,1,2-Tctrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene '•.../ Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene '--_ 1,I,I-Trichloroethane 1,1,2-Trichloroethane '--- Trichloroethene '--- Trichlorofluoromethane 1,2,3-Trichloropropane '-....-- 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate '-- Vinyl chloride Xylenes, Total 29.1 0.50 25.5 0.50 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 25.8 0.50 ugll 25.0 103 70-130 25.6 0.50 25.0 102 70-130 25.6 0.50 ugll ugll 25.0 102 70-130 25.4 0.50 ugll 25.0 102 70-130 29.4 1.0 117 70-130 1.0 ugll ugll 25.0 29.2 25.0 117 70-130 28.9 0.50 ugll 25.0 115 70-130 24.6 0.50 25.0 98 70-130 25.9 0.50 25.0 104 70-130 30.7 0.50 25.0 123 78-149 27.6 1.0 ugll ugll ugll ugll 25.0 III 70-130 30.1 0.50 ugll 25.0 120 70-130 30.0 0.50 25.0 120 70-130 24.8 1.0 25.0 99 57-149 26.9 0.50 ugll ugll ugll 25.0 108 66-134 52.5 1.5 ugll 70-130 0.50 25.0 101 70-130 25.0 105 70-130 25.0 III 70-130 25.0 110 70-130 25.0 112 70-130 25.0 104 44-150 25.0 122 58-138 25.0 119 70-130 25.0 118 70-130 25.0 96 70-130 25.0 117 61-142 25.0 105 70-130 25.0 115 65-129 25.0 117 70-130 25.0 102 70-130 50.0 105 Surrogate: Dibromojluoromethane 26.9 ltg/I 25.0 108 70-130 Surrogate: Toluene-d8 26.2 ug/I 25.0 105 70-130 Surrogate: 4-Bromojluorobenzene 26.6 ugll 25.0 106 70-130 TestAmerica Phoenix Carlene McCutcheon Project Manager The resliits pertain only to the samples tested in the laboratory. This report shall not be reproduced. e.r:cept in/Ill!. withollt written permission!rom TestAmerica. PUFl619 ~­ ( TestAmerica C THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson METHOD BLAJ.iWQC DATA C VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC C ( ( ( ( ( Sampled: 06/28/11 Received: 06/28111 Report Number: PUFI619 ( ( %REC Limits RPD RPD Limit Data Qualifiers Batch: llF1112 Extracted: 06/30/11 ( ( ( LCS Dup Analyzed: 06/30/2011 (l1F1112-BSDl) Acetone 17.8 Benzene 25.0 Bromobenzene 27.2 Bromochloromethane 24.7 Bromodichloromethane 26.9 Bromoform 23.8 Bromomethane 26.4 2-Butanone (MEK) 21.8 29.1 n-Butylbenzene sec-Butylbenzene 28.5 tert-Butylbenzene 28.1 29.7 Carbon disulfide Carbon tetrachloride 28.6 25.9 Chlorobenzene Chloroethane 23.8 Chloroform 26.7 Chloromethane 29.0 2-Chlorotoluene 27.9 4-Chlorotoluene 29.1 Dibromochloromethane 25.9 1,2-Dibromo-3-chloropropane 28.1 1,2-0ibromoethane (EOB) 24.6 Dibromomethane 24.6 1,2-Dichlorobenzene 27.2 27.7 1,3-Dichlorobenzene 1,4-Dichlorobenzene 27.3 Dichlorodifluoromethane 27.2 1,1-Oichloroethane 26.2 1,2-Dichloroethane 28.4 1,1-Dichloroethene 25.3 cis-l,2-Dichloroethene 24.2 trans-! ,2-Dichloroethene 25.0 1,2-Dichloropropane 24.0 1,3-Dichloropropane 24.3 2,2-Dichloropropane 26.4 10 ugll 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 71 100 109 99 107 95 105 87 116 114 113 119 114 104 95 107 116 112 117 104 112 99 98 109 III 109 109 105 114 101 97 100 96 97 105 30-150 70-130 70-130 70-130 70-130 67-122 64-132 48-150 70-130 70-130 70-130 61-126 70-130 70-130 69-128 70-130 56-131 70-130 70-130 70-130 63-129 70-130 70-130 70-130 70-130 70-130 42-150 70-130 72-133 70-130 70-130 70-130 70-130 70-130 70-130 4 0.1 2 2 I 0.9 2 2 2 2 2 2 3 4 5 3 0.9 4 0.8 5 3 2 0.6 2 4 I 7 3 0.4 4 2 5 35 20 20 20 20 20 20 33 20 20 20 20 20 20 20 20 20 20 20 20 25 20 20 20 20 20 20 20 20 20 20 20 20 20 20 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall nol be reproduced, except infull, without written permission from TeslAmerica. PUF1619 ( C ( ( ( C ( C ( C C ( ( r ( c c ( ( C C ( ( C C C ( ( ( r r TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437·3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/28111 Received: 06/28111 Report Number: PUFI619 METHOD BLANKlQC DATA VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte r '- r '-- / r" '-j r, '-' '--_ r-, r r. '- '-_ ::: ......' '--"/ '-- Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: l1Fl112 Extracted: 06/30/11 LCS Dup Analyzed: 06/30/2011 (IIFlIl2-BSDl) l,l-Dichloropropene 25.0 26.3 cis-l,3-Dichloropropene 26.2 trans-I,3-Dichloropropene 27.1 Ethylbenzene 28.1 Hexachlorobutadiene 24.4 2-Hexanone Iodomethane 30.8 30.0 Isopropylbenzene p-Isopropylto!uene 28.7 24.3 Methylene Chloride 4-Methyl-2-pentanone (MIBK) 27.9 25.7 Methyl-tett-butyl Ether (MTBE) 28.4 Naphthalene n-Propylbenzene 29.1 25.0 Styrene 24.8 1,1, J,2-Tetrachloroethane 25.5 I ,1,2,2-Tetrachloroethane 25.5 Tetrachloroethene 25.3 Toluene 28.8 1,2,3-Trichlorobenzene 28.7 1,2,4-Trichlorobenzene I,I,I-Trichloroethane 27.9 24.6 1,1,2-Trichloroethane 25.6 Trichloroethene 30.3 Trichlorofluoromethane 26.7 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 29.0 29.1 1,3,5~ Trimethylbenzene 24.1 Vinyl Acetate Vinyl chloride 26.5 50.6 Xylenes, Total 27.0 Surrogate: Dibromojluoromethane 26.0 Surrogate: Toluene-d8 SW7·ogate: 4-Bromojluorobenzene 24.9 0.50 0.50 0.50 0.50 1.0 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ug/! ltg/I ugll 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 50.0 25.0 25.0 25.0 100 105 105 109 112 98 123 120 115 97 III 103 114 116 100 99 102 102 101 lIS lIS 112 99 102 121 107 116 116 96 106 101 108 104 100 70-130 70-130 70-130 70-130 70-130 44-150 58-138 70-130 70-130 70-130 61-142 70-130 65-129 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 78-149 70-130 70-130 70-130 57-149 66-134 70-130 70-130 70-130 70-130 0.2 6 1 0.04 6 2 1 5 2 0.9 0.2 2 4 0.5 0.3 0.6 2 2 3 0.3 4 4 3 3 2 4 20 20 20 20 20 31 25 20 20 20 22 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 21 20 20 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested ill the laboratory. This report shall 1I0t be reproduced, except illfull, without written permissionFom TestAmerica. PUF1619 ( ( TestAmerica c THE LEADER IN ENVIRONMENTAL Te:sTING 4625 East Cotton Center Blvd. Stc 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.1 0 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson c ( c METHOD BLANKlQC.D!TA ( """ ",~~Ji::J:.~:: c c VOLATILE ORGANICS BY GC/MS (EPA S030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: llFII12 Extracted: 06/30/11 Matrix Spike Analyzed: 06/30/2011 (IIFl112-MSI) Acetone 11.8 47 10·150 c ( Benzene 19.6 0.50 ugll ugll 25.0 NO 78 70·130 Bromobenzene 20.0 0.50 ugll 25.0 80 70·130 Bromochloromethane 19.0 0.50 ugll 25.0 ND ND 76 70·130 Bromodichloromethane 20.9 0.50 ugll 25.0 1.66 77 70·130 Bromofonn 17.0 1.0 ugll ugll ugll ugll ugll 25.0 0.370 66 62-126 25.0 ND 87 55-136 25.0 NO 63 22-150 25.0 NO 86 70-130 Bromomethane 21.7 1.0 2-Butanone (MEK) 15.9 2.5 n-Butylbenzene 21.5 0.50 sec-Butylbenzene 22.0 0.50 tert-Butylbenzene 22.0 0.50 Carbon disulfide 25.7 0.50 Carbon tetrachloride 22.9 0.50 Chlorobenzene 20.1 0.50 Chloroethane 19.9 1.0 Chlorofonn 24.0 Chloromethane 25.0 NO c c c Source: PUFlS84-11 10 ( ( Sampled: 06/28111 Received: 06/28111 Report Number: PUF1619 ( c c ( ( ( 25.0 NO 88 70-130 ugll ugll 25.0 ND 88 70-130 25.0 NO 103 56·132 25.0 ND 91 76-131 25.0 NO 80 70-130 25.0 NO 80 67-134 0.50 ugll ugll ugll ugll 25.0 3.04 84 70-130 23.9 1.0 ugll 25.0 96 50-135 2-Chlorotoluene 21.1 0.50 25.0 84 70-130 4-Chlorotoluene 21.4 0.50 ugll ugll 25.0 ND ND ND 86 70-130 ( Dibromochloromethane 19.7 0.50 ugll 25.0 0.700 76 70-130 1,2-Dibromo-3-chloropropane 18.2 2.5 ugll ugll ugll ugll 25.0 NO 73 60-135 c 25.0 73 70-130 71 70-130 25.0 ND ND ND 81 7()'130 ugll ugll ugll 25.0 NO 82 70-130 25.0 ND 82 70-130 25.0 NO 89 36-150 ugll ugll ugll ugll ugll 25.0 0.210 83 70-130 25.0 ND 85 68-143 25.0 0.490 84 70-130 25.0 0.740 73 70-130 25.0 ND 82 70-130 1,2-Dibromoethanc (EDB) 18.2 0.50 Dibromomethane 17.8 0.50 25.0 I,2-Dichlorobenzene 20.3 0.50 1,3-Dichlorobenzene 20.5 0.50 lA-Dichlorobenzene 20.4 0.50 Dichlorodifluoromethane 22.2 0.50 l,l-Dichloroethane 21.1 0.50 1,2-Dichloroethane 21.2 0.50 l,l-Dichloroethene 21.6 0.50 cis-I,2-Dichloroethene 19.1 0.50 trans-I,2-Dichloroethene 20.6 0.50 1,2-Dichloropropane 18.1 0.50 ND 72 70·130 17.7 0.50 ugll ugll 25.0 1,3-Dichloropropane 25.0 NO 71 70-130 2,2-Dichloropropane 22.9 1.0 ugll 25.0 ND 91 66-130 c ( c c ( ( ( c c c c ( c c ( c TestAmerica Phoenix c Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except injull, wirhoutwrillenpermissionjrom TesrAmerica. PUFl619 ( ( , TestAmerica c THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/28/11 Received: 06/28111 Report Number: PUFI619 METHOD BLANKlQC DATA VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Analyte Result r Batch: IIFlll2 Extracted: 06/30/11 ~_. Matrix Spike Analyzed: 06/30/2011 (IIFl112-MSl) 1,I-Dichloropropene 20.4 Reporting Limit Units ,-. cis-l,3-Dichloropropene 19.5 0.50 trans-! ,3-Dichloropropene ,,-. Ethylbenzene 19.0 0.50 21.8 0.50 20.4 1.0 ugl1 16.5 26.2 2.5 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll '. c'-- . Hexachlorobutadiene r- 2-Hexanone '------ Iodomethane .. 0.50 2.5 Isopropylbeozene 23.7 0.50 r p-Isopropyltoluene 21.8 0.50 '--- Methylene Chloride 18.6 1.0 "'----'" 4-Methyl-2-pentanone (MIBK) 18.5 2.5 r-, Methyl-tert-butyl Ether (MTBE) 18.4 0.50 '-- Naphthalene 19.4 2.5 n-Propylbenzene 22.1 0.50 Styrene 19.1 0.50 19.3 0.50 17.8 0.50 22.8 0.50 18.8 '-.. r 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene '---_ I,I,I-Trichloroethane 1,1,2-Trichloroethane Trichloroethene '---- Trichlorofluoromethane 1,2,3-Trichloropropane '---- 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate '----- Vinyl chloride ,__ %REC Limits RPD ND 82 70-130 25.0 ND 78 70-130 25.0 ND 76 71-132 25.0 ND 87 70-130 25.0 ND 82 66-129 25.0 ND 66 18-150 25.0 ND 105 47-141 25.0 ND 95 78-137 25.0 ND 87 70-130 25.0 ND 25.0 ND 75 74 56-145 25.0 ND 74 67-138 25.0 ND 77 54-135 25.0 ND 88 70-130 25.0 ND 51-123 ugl1 25.0 ND 77 77 ugl1 25.0 ND 71 69-133 25.0 1.91 84 70-130 0.50 ugll ugll 25.0 ND 75 70-130 19.5 1.0 ugl1 25.0 ND 19.6 1.0 25.0 ND 66-126 22.6 0.50 ugll ugll 25.0 ND 78 78 90 17.0 0.50 ugl1 25.0 ND 68 70-130 24.2 0.50 25.0 4.24 80 70-130 24.2 0.50 25.0 ND 97 74-150 19.0 1.0 25.0 ND 76 70-130 22.2 0.50 ugll ugll ugll ugll 25.0 ND 89 70-130 22.3 0.50 ugl1 25.0 ND 89 61-138 ugll ugll ugll 25.0 ND 70 50-150 25.0 ND,,~ 91 58-139 50.0 ND 81 70-130 106 103 101 70-130 70-130 70-130 17.6 1.0 0.50 Xylenes, Total 40.5 1.5 Surrogate: Dibromojluoromethane 26.5 25.8 ugll 25.0 ugll 25.0 25.4 ugfl 25.0 Surrogate: 4-Bromojluorobenzene %REC 25.0 22.7 '----- Surrogate: Toluene-d8 Source Result RPD Limit Data Qualifiers Source: PUFlS84-11 ugll ugll ugll ugll r Spike Level 74-132 70-130 70-130 76-132 M2 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, e.xcept infull, without writlenpermissiolljrom TestAmerica. PUF1619 ~ ( TestAmerica ( 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING Project!D: PO #802.1 0 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson ( Sampled: 06128111 Received: 06/28111 Report Number: PUFI619 ( ( C METHOD BLANKlQCJ:)A;'lX ( C VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Analyte C C Result Reporting Limit Units Spike Level Source Result %REC %REC Limits ( RPD RPD Limit Data Qualifiers Batch: llFl112 Extracted: 06/30/11 Matrix Spike Dup Analyzed: 06/30/2011 (l1FI112-MSDI) Acetone 16.4 10 ugll 25.0 ND 66 10-150 33 35 25.0 101 70-130 25 20 25.0 ND ND 106 70-130 28 20 25.0 ND 99 70-130 26 20 25.0 1.66 106 70-130 30 20 25.0 0.370 94 62-126 34 20 Bromomethane 26.7 1.0 25.0 ND 107 55-136 21 24 2-Butanone (MEK) 20.0 2.5 ugll 25.0 ND 80 22-150 23 31 n-Butylbenzene 28.3 0.50 25.0 ND 113 70-130 27 20 sec-Butylbenzene 28.2 0.50 ugll ugll 25.0 ND 113 70-130 25 20 25.0 ND 115 70-130 26 20 ND 121 56-132 16 20 25.0 ND 114 76-131 22 20 25.0 ND 106 70-130 27 20 25.3 0.50 Bromobenzene 26.6 0.50 Bromochloromethane 24.7 0.50 Bromodichloromethane 28.3 0.50 Bromofonn 23.9 1.0 tert-Butylbenzene 28.7 0.50 ugll Carbon disulfide 30.2 0.50 25.0 Carbon tetrachloride 28.5 0.50 Chlorobenzene 26.4 0.50 Chloroethane 23.7 1.0 ugll ugll ugll ugll 25.0 ND 95 67-134 17 20 Chlorofonn 28.9 0.50 ugll 25.0 3.04 103 70-130 19 20 Chloromethane 28.8 1.0 ugll 25.0 ND 115 50-135 19 20 2-Chlorotoluene 27.6 0.50 ugll 25.0 ND III 70-130 27 20 4-Chlorotoluene 27.8 0.50 ugll 25.0 ND III 70-130 26 20 Dibromochloromethane 26.7 0.50 ugll 25.0 0.700 104 70-130 30 20 1,2-Dibromo-3-chloropropane 26.6 2.5 25.0 ND 106 60-135 38 29 25.0 ND 99 70-130 30 20 25.0 ND 96 70-130 30 20 RJ RJ RJ RJ RJ RJ RJ RJ RJ RJ RJ RJ RJ RJ RJ RJ RJ RJ RJ 1,2-Dibromoethane (EDB) 24.8 0.50 Dibromomethane 24.1 0.50 ugll ugll ugll 1,2-Dichlorobenzene 26.6 0.50 ugll 25.0 ND 106 70-130 27 20 1,3-Dichlorobenzene 26.8 0.50 ugll 25.0 ND 26 20 26.7 0.50 25.0 ND 70-130 27 20 Dichlorodifluoromethane 26.1 0.50 25.0 ND 105 36-150 16 22 l,l-Dichloroethane 25.8 0.50 25.0 70-130 20 20 27.3 0.50 25.0 0.210 ND 102 1,2-Dichloroethane 109 68-143 25 25.4 25.0 0.490 100 70-130 16 20 20 RJ l,l-Dichlorocthene cis-I,2-Dichloroethene 23.8 0.50 25.0 0.740 92 70-130 22' 20 trans-I,2-Dichloroethene 25.5 0.50 ugll ugll ugll ugll ugll ugll ugll 107 107 70-130 l,4-Dichlorobenzene 25.0 ND 102 70-130 21 20 1,2-Dichloropropane 24.5 0.50 ugll 25.0 ND 98 70-130 30 1,3-Dichloropropane 24.4 0.50 ugll 25.0 ND 97 70-130 31 20 20 2,2-Dichloropropane 28.3 1.0 ugll 25.0 ND 113 66-130 21 20 RJ RJ RJ RJ RJ 0.50 .4,· ( C Source: PUFlS84-11 ugll ugll ugll ugll ugll ugll Benzene C ( ( ( ( ( C ( ( ( C C ( ( ( ( ( ( C C ( C ( ( ( TestAmerica Phoenix ( Carlene McCutcheon Project Manager C The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except infull, without written permissionfrom TestAmerica. PUF1619 <.Page 43 oj46> ( ( ( , ,~ , TestAmerica Tf-IE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437~3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N~ Tatum Blvd~, Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/28/11 Received: 06/28/11 Report Number: PUF1619 METHOD BLANIDQC DATA VOLATILE ORGANICS BY GelMS (EPA 5030B/8260B) Result Analyte Reporting Limit ,-- Batch: 11FI112 Extracted: 06/30/11 >-, Matrix Spike Dup Analyzed: 06/30/2011 (I1Fll12-MSD1) l,l-Dichloropropene 25.7 0.50 ::=: r' "-- %REC %REC Limits RPD Source: PUFlS84-11 ND 103 70-130 70-130 NO 103 26.7 1.0 0.50 23.3 0.50 ugll 25.0 30.2 0.50 25.0 28.5 0.50 ugll ugll 25.0 NO 4.24 NO 25.6 1.0 ugll 25.0 ND 103 70-130 2S.4 0.50 ugll 25.0 113 70-130 2S.9 0.50 ugll 25.0 NO NO 115 61-138 24.1 1.0 ugll 25.0 ND 96 50-150 26.7 0.50 ugll 25.0 ND 107 58-139 52.2 1.5 ND 25.9 0.50 trans-I,3-Dichloropropene 26.0 0.50 Ethylbenzene 27.1 0.50 Hexachlorobutadiene 2-Hexanone 25.7 1.0 23.S 2.5 Iodomethane 31.5 2.5 Isopropylbenzene p-Isopropyltoluene 29.S 0.50 28.0 0.50 Methylene Chloride 23.7 1.0 4-Methyl-2-pentanone (MIBK) 26.4 2.5 Methyl-tert-butyl Ether (MTBE) 24.1 0.50 Naphthalene 26.2 2.5 29.0 0.50 Styrene 24.7 0.50 1,1,1,2-Tetrachloroethane 25.4 0.50 ..-~, 1,1,2,2-Tetrachloroethane 24.8 0.50 27.6 0.50 26.1 0.50 26.6 1.0 Surrogate: Dibromojluoromethane Source Result 2S.2 cis-l,3-Dichloropropene Tetrachloroethene Toluene 1,2,3~ Trichlorobenzene 1,2,4-Trichlorobenzene 1,1 ,I-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Spike Level ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll n-Propylbenzene ~.' Units 25.0 25.0 RPD Limit 23 20 28 20 25.0 ND 104 71-132 31 20 25.0 lOS 70-130 22 20 103 66-129 23 21 95 18-150 25 126 47-141 36 IS 119 78-137 23 20 25.0 NO ND ND ND ND ND 112 70-130 20 25.0 ND 95 74-132 25 24 25.0 105 56-145 35 25.0 ND ND 96 67-138 27 25.0 ND 105 54-135 30 25.0 ND 116 70-130 27 25.0 ND 99 51-123 25 25.0 ND 102 70-130 27 25.0 NO 99 69-133 33 26 21 33 20 21 20 20 25.0 1.91 103 70-130 19 20 25.0 ND 104 70-130 32 20 25.0 NO 106 70-130 31 25.0 ND 107 66-126 31 25.0 ND 113 76-132 93 70-130 22 31 20 20 20 104 70-130 22 114 74-150 16 30 25 26 31 16 25 25.0 25.0 25.0 25.0 ugll 50.0 104 70-130 25.6 ugll 25.0 103 70-130 SW7·ogate: Toluene~d8 25.6 ugll 25.0 103 70-130 Surrogate: 4~Bromojluorobel1zel1e 25.0 ugll 25.0 100 70-130 Data Qualifiers R1 R1 R1 R1 R1 R1 29 20 20 20 20 20 20 33 23 21 20 R1 R1 R1 R1 R1 R1 R1 R1 R1 R1 R1 R1 R1 R1 R1 R1 R1 R1 R1 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain ollly to the samples tested in the laboratory. This report sllallllot be reproduced. except infull, without writlenpermissionjrolll TestAmerica. PUFl619 l~ . ( TestAmerica ( '_. THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Report Number: PUF1619 Sampled: 06/28/11 Received: 06/28111 ( ( ( C C C DATA QUALIFIERS AND DEFINITIONS ( M2 Matrix spike recovery was low; the associated blank spike recovery was acceptable. Nt See case narrative. Rl The RPD/RSD exceeded the method acceptance limit. ( ND Analyte NOT DETECTED at or above the reporting limit or MDL, ifMDL is specified. C RPD Relative Percent Difference ( C C ( ( ( C ( C ( C ( C C C ( ( ( C C C ( ( ( ( C ( TestAmerica Phoenix C Carlene McCutcheon Project Manager ( The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except infull, without writtenpermissionjrom TestAmerica. PUF1619 ( ( ( f r TestAmerica THE LEADER IN ENVIRONMENTAL TESTING ( 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Report Number: PUFI619 Sampled: 06/28/11 Received: 06/28111 Certification Summary TestAmerica Phoenix Method Matrix Nelac Arizona EPA 8260B Water x x Nevada and NELAP provide analyte specific accreditations. Analyte specific information/or TestAmerica may be obtained by contacting the laboratory or visiting our website at www.testamericainc.com ~. TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested ill the laboratory, This report shalll/ot be reproduced, except inJull. withoia wrillenpennissionjrom TestAmerica. PUF1619 J~~0J~0GU~U0U~U~J~U~~~0~UUU~U~_UUUUU0UUU~UU'~ TestAmerica CHAIN OF CUSTODY FORM ) Spectallnstructlons 'l,rM~T \ t1..11I1 -=-1 \d'" c:>< W ~J!L.I? ~(uhd~1 W'1 tx' W ~~F I~ Io/zglHlom IX \N ~-¥=r~r~l\\l~ \\cOl><::' 'il 1'\3~1 ~ M'VE:\ \ 1 \o\\lw.-Q l>< \1\1. ~/~f.1 ~ ~f~llil\9S{.,1 \-1-C~- .D< W ~~iC I ~ 1*'f,;h\I\\'1.?'1 ~cll>« 1 'i\J I~h~ 1 '3 I~'f~hd \\4101 'Ac1> V ~i'&~C[ ~61:;gh~1 \'iQIIWJ- R I\f\J Pdr/t,/10- . os o/. Dl D~ 109 I0 I~ot= 13 ~r\l\I-hx_lIX ifftlile\~me,/ 17PD IRece:;:~~::?,r_ .... Da&iTlmef Date/.Tlme: ~ IReceived !'y: !Recelve~ in Lab By: l/ ITurnaround Time: Date/Time: GrZlr-/{ Date/Time: Date.fTime: I:?:rf::l (Check) same day ~ __ 24 hours days ")( 48 hours no Sample Integrity: (Check) intact Note: By relinquishing samples to TestAmerica,' client ag;~es. to ~~y for the serviC~~ reqUe;~ed on this cha-i-~ of-cust~dY form-and Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days. . Ill) 1/\ ;}. b3 04 . I __ t ~ ~ wi B~--'J... ~ f\ IrnqU1Shn~'- Matrix of B~ > Fax Number: Sample Description \ ~(}l ~ Phone Number: croeL~t-\ Page Analysis Required 1 ~-\O I~~\'l. k2- &5dl-"6 Project Manager: mpler: Project/PO Number: on ice ....- ~ny additional analyses p;rtormed o-n this project.7 J,.a~V r ~ .. TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 LABORATORY REPORT Prepared For: ,- Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Project: PO #802.10 June 2011 Sampled: 06/29111 Received: 06/29111 Issued: 07111111 12:31 , NELAP #0 II 09CA Arizona DHS#AZ0728 The results listed within this Laboratory Report pertain only to the samples tested in the laboratory. The analyses contained in this report were pelformed in accordance with the applicable certifications as noted All soil samples are reported all a wet weight basis unless otherwise noted in the report. This Laboratory Report is confidential and is intended/or the sole lise alTes/America and its client. This report shall not be reproduced, except inJull, without written permission/rom Tes/America. The Chain o/Custody, 1 page, is included and is an integral part 0/ this report. This entire report was reviewed and approved/or release. CASE NARRATlVE LABORATORY ID CLIENTID MATRIX PUFI729-01 PUF 1729-02 PUF 1729-03 PUF 1729-04 TB Water Water Water Water W-l W-IS Duplicate E TestAmerica Phoenix Carlene McCutcheon Project Manager PUF1729 l. ( TestAmerica ( THE LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 Report Number: PUFI729 Sampled: 06/29/11 Received: 06/29/11 SAMPLE RECEIPT: Samples were received intact, at 3°e, on ice and with chain of custody documentation. HOLDING TIMES: All samples were analyzed within prescribed holding times andlor in accordance with the TestAmerica Sample Acceptance Policy unless otherwise noted in the report. PRESERVATION: Samples requiring preservation were verified prior to sample analysis. QA/QC CRITERIA: All analyses met method criteria, except as noted in the report with data qualifiers. No significant observations were made. SUBCONTRACTED: No analyses were subcontracted to an outside laboratory. C ( ( c c c ( L3 EPA 8260B:Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was above the acceptance limits. Analyte not detected, data not impacted. Rl EPA 8260B:The RPD exceeded the acceptance limit. Nl EPA 8260B:The samples were first analyzed with Bromomethane failing low in the CCV. PUF1729-01 is a tripblank with only one vial. PUF 1729-02 vial Band C were spiked and used as MSIMSD for the first analysis. Vial A was re-analyzed with headspace. COMMENTS: ( c ( c ( , I~ ( ( ( ( ( ( ( C C ( ( (" . ( ( C C C C Reviewed By: ( C ( .~ ( TestAmerica Phoenix C Carlene McCutcheon Project Manager ( The results pertain only 10 the samples tested in the labora/ory. This report shall not be reproduced, except in/ull, without written permission/rom TestAmerica. PUFI729 ( ( , TestAmerica THE LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Sampled: 06/29111 Received: 06/29111 Report Number: PDF 1729 Attention: Joel Peterson VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Analyte Method , Sample ill: PUFI729-01 (TB - Water) ,-- Acetone Benzene EPA 8260B ~ Brornobenzene EPA 8260B Batch Reporting Limit IIGOOl8 I !G0018 IIGOOl8 IIGOOl8 IIGOOl8 IIGOOl8 IIGOOl8 I !G0018 IIGOOl8 IIGOOl8 I !G0018 IIGOOl8 IIGOOl8 IIGOOl8 IIGOOl8 I !G0018 IIGOOl8 IIGOOl8 IIGOOl8 IIGOOl8 IIGOOl8 llGOOl8 I !G0018 llGOOl8 llGOOl8 llGOOl8 llGOOl8 llGOOl8 I !G0018 llGOOl8 llGOOl8 llGOOl8 I !G0018 llGOOl8 I !G0018 IIGOOl8 llGOOl8 IIGOOl8 IIGOOl8 IIGOOl8 0.50 0.50 0.50 0.50 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 2.5 Sample Dilution Date Result Factor Extracted Date Analyzed 7/112011 711/2011 7/112011 7/112011 7/1/2011 7/112011 7/112011 7/112011 7/1/2011 7/112011 7/1/2011 7/112011 7/112011 7/1/2011 7/1/2011 7/112011 7/112011 711/2011 711/2011 711/2011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 711/2011 71112011 711/2011 71112011 711/2011 7/112011 7/1/2011 7/112011 7/1/2011 7/1/2011 711/2011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 71112011 7/1/2011 7/112011 71112011 71112011 711/2011 7/112011 711/2011 7/112011 711/2011 711/2011 7/112011 711/2011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 7/1/2011 7/112011 7/112011 7/112011 7/112011 711/2011 7/112011 Data Qualifiers Reporting Units: ugll r' "-.. _ ~. r . '--' r '"--, '--~. r - '- ~ ,_ Bromochloromethane Bromodichloromethane Bromofonn 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chlorofonn Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane I ,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene l,4-Dichlorobenzene Dichlorodifluoromethane l,l-Dichloroethane 1,2-Dichloroethane 1,I-Dichloroethene cis-l,2-Dichloroethene trans-l,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-l,3-Dichloropropene trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B 10 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND VI TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shalll/or be reproduced, except infull, without wrillenperlllissionjrolll TestAlllerica. PUF1729 TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 ( VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Method Batch Reporting Limit Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers Sample ID: PUFl729-01 (TB - Water) - cont. Reporting Units: ugll Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl Ether (MTBE) Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorohenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromojluoromelhane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) ( C Sampled: 06/29/11 Received: 06/29111 Report Number: PUFI729 Phoenix, AZ 85028 Attention: Joel Peterson ( C C C ( ( EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B IIGOOl8 IIGOOl8 11GOOI8 IIGOOl8 IIGOOl8 IIGOOl8 IIGOOl8 IIGOOl8 IIGOOl8 11GOOI8 IIGOOl8 11GOOI8 11GOOI8 11GOOI8 IIGOOl8 IIGOOl8 IIGOOl8 IIGOOl8 11GOOI8 11GOOI8 IIGOOl8 IIGOOl8 IIGOOl8 11GOOI8 11GOOI8 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 ND ND ND ND ND ND ND ND ND ND ND ND ND 7/112011 71112011 7/112011 711/2011 711/2011 71112011 7/112011 711/2011 7/112011 7/112011 7/112011 711/2011 7/112011 7/112011 ND. 711/2011 7/112011 ND ND ND ND ND ND 7/112011 7/112011 7/112011 7/112011 7/112011 711/2011 7/112011 71112011 ND 7/1/2011 711/2011 ND ND ND ND 106% 105% 102% 7/112011 7/112011 711/2011 C C C ( 711/2011 7/112011 711/2011 7/1/2011 7/112011 ( 7/112011 711/2011 7/112011 7/112011 711/2011 71112011 C 711/2011 7/112011 7/112011 711/2011 ( ( ( ( VI 7/112011 7/1/2011 71112011 ( ( ( C 7/112011 ( 7/112011 711/2011 ( ( ( C ( C C C ( C C C TestAmerica Phoenix ( Carlene McCutcheon Project Manager The results perlain only (0 rhe samples fested in the laboratory. This report shallllot be reproduced, except inJull, without writlenpennission!rom TestAmerica. PUF1729 ( ( ( ( ~ TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/29/11 Received: 06/29111 Report Number: PUF 1729 ,- VOLATILE ORGANICS BY GCIMS (EPA 5030B/S260B) ,r· '~- ,. r Analyte Method Batch Reporting Limit Sample Dilution Date Result Factor Extracted Date Analyzed Sample ID: PUFI729-0IREI (TB - Water) - cont. Data Qualifiers NI Reporting Units: ugll EPA 8260B Bromomethane Surrogate: Dibromofluoromethane (70-130%) ~~. Surrogate: Toluene-d8 (70-130%) '- Surrogate: 4-Bromojluorobenzene (70-130%) '- llGOI00 1.0 ND 7/612011 7/6/2011 92% iJl % 97% ~. r. ,- TestAmerica Phoenix Carlene McCutcheon Project Manager The reslllts pertain only to the samples res/cd in the laboratory. nil's report shalll/ot be reproduced. except inJul/, without wrilfenpermissionjrom TestAmerica. PUF1729 ~ ( TestAmerica c THE LEADE'R IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 c C Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Sampled: 06/29/11 ( Report Number: PUFI729 Received: 06/29/11 ( . Phoenix, AZ 85028 Attention: Joel Peterson L -_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _~~_ _ _ _ _ _ _ _~_ _ _ _ _ _~~~( C VOLATILE ORGANICS BY GCIMS (EPA 5030B/S260B) Method Analyte Batch Reporting Limit 11GOOI8 IIGOOl8 IIGOOl8 IIGOOl8 11GOOI8 11GOOI8 IIGOOl8 11GOOI8 IIGOOl8 IIGOOl8 IIGOOl8 IIGOOl8 11GOOI8 11GOOI8 IIGOOl8 IIGOOl8 11GOOI8 IIGOOl8 11GOOI8 11GOOI8 11GOOI8 IIGOOl8 11GOOI8 11GOOI8 IIGOOl8 IIGOOl8 IIGOOl8 11GOOI8 IIGOOl8 IIGOOl8 IIGOOl8 IIGOOl8 IIGOOl8 IIGOOl8 IIGOOl8 11GOOI8 11GOOI8 IIGOOl8 IIGOOl8 11GOOI8 10 0.50 0.50 0.50 0.50 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 2.5 Sample Dilution Date Result Factor Extracted Date Analyzed 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 711/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 711/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/112011 7/1/2011 7/1/2011 711/2011 7/1/2011 7/1/2011 7/1/2011 711/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 711/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 711/2011 7/1/2011 711/2011 711/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 711/2011 7/112011 7/1/2011 7/1/2011 711/2011 Data Qualifiers Sample ill: PUFl729-02 (W-l- Water) Reporting Units: ugll Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromofonn 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotolucne 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene l,4-Dichlorobenzene Dichlorodifluoromethane EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B l,l-Dichloroethane EPA 8260B l,2-Dichloroethane EPA 8260B 1,1-Dichloroethene cis-l,2-Dichloroethene EPA 8260B trans-l,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene cis-l ,3-Dichloropropene trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.3 ND ND ND ND ND ND ND ND ND ND ND 3.2 ND 4.4 12 ND ND ND ND ND ND ND ND ND ND ( C C C ( C ( ( ( ( ( ( ( ( ( ( ( ( ( ( ( VI ( C C ( ( C C ( ( TestAmerica Phoenix C Carlene McCutcheon Project Manager ( The results pertain only to the samples tested in the laboratory. This report shalll/of be reproduced, except iI/full, without written pennissiol/from resfAmerica. PUF1729 ( C ( c ~ c ~ ~ r ~ TestAmerica THE LEADER IN ENVIRONMENTAL TESTING %25 East Cotton Center Blvd. Ste 189, Phoenix. AZ 85040 (602) 437-3340 FBX:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Sampled: 06/29/11 Received: 06/29/11 Report Number: PUFI729 Attention: Joel Peterson ,- VOLATILE ORGANICS BY GC/MS (EPA S030B/8260B) c ,~ ~ Analyte Method 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl Ether (MTBE) " Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene ,~" , Reporting Limit 11GOOI8 11GOOI8 11 GOOI 8 11GOOI8 11GOOI8 I1GOOl8 1!GOO I 8 I1GOOl8 I1GOOl8 I1GOOl8 I1GOOl8 I1GOOl8 I1GOOl8 11GOOIS IIGOOIS IIGOOIS IIGOOIS 11GOOI8 11GOOIS 11GOOIS IIGOOIS I!GOOIS 11GOOIS IIGOOIS I!GOOIS 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers Sample ID: PUFI729-02 (W-l - Water) - cont. Reporting Units: ug/1 Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride ~. Batch 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 82608 EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND 3.9 ND ND ND ND ND 71 0.82 ND ND ND ND ND ND 109% 104% 104% 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/112011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 711/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 VI M2 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall 1/01 be reproduced, except infull. wilhoutwriftenpermissionjrom TestAmerica. PUF1729 ~. ( TestAmerica C THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson ( C ( VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte ( i. Sampled: 06/29111 Received: 06/291l1 Report Number: PUFI729 ( Method Batch Reporting Limit Date Sample Dilution Result Factor Extracted Date Analyzed Data Qualifiers Nl Sample ID: PUFl729-02REl (W-l - Water) - cont. Reporting Units: ug/l Brornomethane EPA 8260B Surrogate: Dibromofluoromethane (70-130%) Surrogate: Toluene-dB (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) 1100100 1.0 ND 7/6/2011 7/6/2011 98% 112% 99% ( , ( C ( ( ( ( ( l. ( ( ( ( ( ( C ( ( C ( l. ( C C C ( ( C ( TestAmerica Phoenix ( Carlene McCntcheon Project Manager ( The results pertain only to the samples tested in the laboratory. This report shalll/ot be reproduced, except iI/full, withoutwrillen permissiol/jrom TestAmerica. PUFl729 ( ( , TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Colton Center Blvd Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/29/11 Received: 06/29111 Report Number: PUFI729 VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Method Analyte , Sample JD: PUFI729-03 (W-18 - Water) '- Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane l,l-Dichloroethane 1,2-Dichloroethane l,l-Dichloroethene cis-l ,2-Dichloroethene trans-l,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-l,3-Dichloropropene trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone Batch Reporting Limit 1100018 I !G0018 1100018 1100018 1100018 1100018 I !G0018 1100018 I !G0018 1100018 I !G0018 1100018 1100018 1100018 1100018 I !G0018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 I !G0018 1100018 I !G0018 I !G0018 1100018 1100018 IO 0.50 0.50 0.50 0.50 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 2.5 Sample Dilution Date Result Factor Extracted Date Analyzed 711/2011 711/2011 7/1/2011 7/1/2011 7/112011 7/112011 7/112011 7/112011 7/1/2011 7/1/2011 7/112011 7/1/2011 7/1/2011 7/1/2011 711/2011 7/112011 7/112011 7/112011 7/112011 7/112011 7/1/2011 7/112011 7/112011 7/1/2011 7/112011 7/112011 711/2011 7/112011 711/2011 7/1/2011 7/1/2011 7/112011 711/2011 7/112011 71112011 7/112011 7/112011 71112011 7/112011 7/112011 7/112011 71112011 7/112011 7/112011 7/112011 7/1/2011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 7/1/2011 7/112011 7/112011 7/112011 7/112011 7/112011 7/112011 711/2011 711/2011 7/112011 711/2011 7/1/2011 7/112011 7/112011 7/112011 7/112011 711/2011 7/112011 7/112011 711/2011 7/112011 711/2011 7/112011 Data Qualifiers Reporting Units: ugll r- r "--,. '--_/ r-, '-,'- ,.-'- ---" EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.1 ND ND ND ND ND ND ND ND ND ND ND 2.9 ND 3.2 12 ND ND ND ND ND ND ND ND ND ND VI TestAmerica Phoenix Carlene McCutcheon Project Manager Tile results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except infull, wifhoutwrittenpermissiollfrom TestAmerica. PUF1729 ,,_. ( TestAmerica ( THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06129111 Received: 06/29111 Report Number: PUFl729 ( ( VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Method Batch Reporting Limit 11GOO18 11GOO18 11GOO18 11GOO18 1100018 1100018 11GOO18 11GOO18 1100018 11GOO18 11GOO18 1100018 11GOO18 1100018 1100018 11GOO18 11GOO18 1100018 11GOO18 1100018 11GOO18 11GOO18 11GOO18 11GOO18 1100018 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 Date Sample Dilution Result Factor Extracted Date Analyzed 711/2011 7/112011 711/2011 7/1/2011 7/112011 7/112011 711/2011 7/112011 7/112011 711/2011 7/1/2011 7/1/2011 7/112011 711/2011 7/112011 711/2011 7/112011 7/112011 7/112011 711/2011 7/112011 7/112011 711/2011 7/112011 7/112011 711/2011 711/2011 7/112011 7/1/2011 7/112011 7/112011 71112011 7/112011 7/112011 7/112011 7/112011 71112011 7/112011 711/2011 7/112011 7/112011 7/112011 711/2011 7/112011 7/112011 711/2011 7/112011 7/112011 711/2011 71112011 Data Qualifiers Sample ID: PUF1729-03 (W-18 - Water) - cont. Reporting Units: ugll Iodomethane Isopropylbenzene p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MlBK) Methy1-tert-buty1 Ether (MTBE) Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-dB (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B ( C ( ND ND ND ND ND ND ND ND ND ND ND 2.9 ND ND ND ND ND 61 ND ND ND ND ND ND ND ( ( C ( ( ( ( ( ( ( VI 112% 105% 101 % ( ( ( C ( ( C ( C ( C ( C ( ( C ( TestAmerica Phoenix ( Carlene McCutcheon Project Manager ( The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except inJull. withuut written permissionfrom TestAmerica. PUF1729 C , I c , TestAmerica THE LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Sampled: 06/29/11 Received: 06/29/1 I Report Number: PUFI729 VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Analyte Method Sample!D: PUFI729-03REI (W-18 - Water) - cont. Reporting Units: ugl1 EPA 8260B Bromomethane Surrogate: Dibromojluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) Batch Reporting Limit 11 GOIOO 1.0 Sample Dilution Date Result Factor Extracted Date Analyzed 7/6/2011 7/6/2011 ND Data Qualifiers 100% 112% 99% ~. r-. r. TestAmerica Phoenix Carlene McCutcheon Project Manager The reslllts pertain only to the samples rested in the laboratory. This report shall not be reproduced, except injul/, without writtenpermissionjro/1/ TestAmerica. PUF1729 ( TestAmerica c 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson c Project!D: PO #802.1 0 June 2011 Sampled: 06/29/11 Received: 06/29/11 Report Number: PUFI729 c C r VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Method Sample!D: PUFI729-04 (Duplicate E - Water) Reporting Units! ugll EPA 8260B Acetone EPA 8260B Benzene EPA 8260B Bromobenzene EPA 8260B Bromochloromethane EPA 8260B Bromodichloromethane EPA 8260B Bromofonn EPA 8260B 2-Butanone (MEK) EPA 8260B n-Butylbenzene EPA 8260B sec-Butylbenzene EPA 8260B tert-Butylbenzene EPA 8260B Carbon disulfide EPA 8260B Carbon tetrachloride EPA 8260B Chlorobenzene EPA 8260B Chloroethane EPA 8260B Chloroform EPA 8260B Chloromethane EPA 8260B 2-Chlorotoluene EPA 8260B 4-Chlorotoluene EPA 8260B Dibromochloromethane EPA 8260B 1,2-Dibromo-3-chloropropane EPA 8260B 1,2-Dibromoethane (EDB) EPA 8260B Dibromomethane EPA 8260B 1,2-Dichlorobenzene EPA 8260B 1,3-Dichlorobenzene EPA 8260B 1,4-Dichlorobenzene EPA 8260B Dichlorodifluoromethane I,I-Dichloroethane EPA 8260B 1,2-Dichloroethane EPA 8260B I,I-Dichloroethene cis-I,2-Dichloroethene EPA 8260B trans-l,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-I,3-Dichloropropene trans-l,3-Dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone ( ( EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B Batch Reporting Limit Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers ( ( ( IIGOOl8 11G0018 11G0018 11GOOI8 11GOOI8 IIGOOl8 IIGOOl8 IIGOOl8 11G0018 11G0018 11GOOI8 11G0018 11GOOI8 11GOOI8 IIGOOl8 IIGOOl8 IIGOOl8 11G0018 11GOOI8 11GOOI8 IIGOOl8 11G0018 11GOOI8 IIGOOl8 11G0018 11G0018 IIGOOl8 11G0018 11G0018 11G0018 IIGOOl8 11GOOI8 11G0018 11GOOI8 11GOOI8 11G0018 IIGOOl8 IIGOOl8 11G0018 11GOOI8 10 0.50 0.50 0.50 0.50 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 1.0 2.5 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.2 ND ND ND ND ND ND ND ND ND ND ND 3.0 ND 3.2 12 ND ND ND ND ND ND ND ND ND ND 7/1/2011 7/1/2011 711/2011 7/1/2011 711/2011 7/112011 7/1/2011 7/1/2011 711/2011 711/2011 7/1/2011 711/2011 7/112011 7/112011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 711/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/112011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/112011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 711/2011 7/1/2011 7/1/2011 7/112011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 711/2011 7/1/2011 711/2011 7/1/2011 711/2011 711/2011 7/1/2011 7/1/2011 711/2011 7/1/2011 7/112011 7/1/2011 7/1/2011 7/1/2011 711/2011 711/2011 711/2011 7/1/2011 7/1/2011 7/1/2011 711/2011 711/2011 711/2011 7/1/2011 7/1/2011 7/1/2011 C ( ( C ( ( l ( C ( ( ( ( ( ( ( VI ( ( VI C C C C C C C ( ( TestAmerica Phoenix ( , Carlene McCutcheon Project Manager ( The results pertain only to the samples tested in the laboratOJY. This report shallllot be reproduced, except injull, without writtenpermissionji-om TestAmerica. PUFI729 , ( ( l ,,r , , , ',r , TestAmerica 4625 East Cotlon Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437~3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Project ID: PO #802.10 June 2011 Sampled: 06/29111 Received: 06/29111 Report Number: PUFI729 '- VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) "- r Batch Reporting Limit 1100018 I !G0018 1100018 1100018 1100018 1100018 1100018 I !G0018 1100018 1100018 1100018 1 \G0018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 1100018 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 '-- r ,'- Analyte Method Sample ill: PUFl729-04 (Duplicate E - Water) - cont. Reporting Units: ugll EPA 8260B Iodomethane 'EPA 8260B Isopropylbenzene "EPA 8260B p-Isopropyltoluene ,-EPA 8260B Methylene Chloride "EPA 8260B r 4-Methyl-2-pentanone (MIBK) '-- Methyl-tert-butyl Ether (MTBE) EPA 8260B EPA 8260B Naphthalene 'EPA 8260B n-Propylbenzene EPA 8260B Styrene EPA 8260B "'- 1,1,1,2-Tetrachloroethane EPA 8260B ,. 1,1,2,2-Tetrachloroethane EPA 8260B Tetrachloroethene EPA 8260B ",. Toluene EPA 8260B 1,2,3-Trichlorobenzene EPA 8260B 1,2,4-Trichlorobenzene EPA 8260B " 1,1,1-Trichloroethane EPA 8260B 1,1,2-Trichloroethane EPA 8260B Trichloroethene EPA 8260B Trichlorofluoromethane EPA 8260B 1,2,3-Trichloropropane r. EPA 8260B 1,2,4-Trimethylbenzene EPA 8260B 1,3,5-Trimethylbenzene EPA 8260B Vinyl Acetate EPA 8260B Vinyl chloride EPA 8260B , Xylenes, Total Surrogate: DibromojIuoromethane (70-130%) Surrogate: Toluene-dB (70-130%) Surrogate: 4-BromojIuorobenzene (70-130%) , Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers "- , , , ~ ~ ~, ~ ~, ~ ~ ~. ~, ~ ND ND ND ND ND ND ND ND ND ND ND 3.0 ND ND ND ND ND 61 ND ND ND ND ND ND ND III % 105% 102% 7/1/2011 7/1/2011 711/2011 71112011 7/1/2011 7/1/2011 711/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 711/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/201 I 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/201 I 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 7/1/2011 VI ~/ TestAmerica Phoenix Carlene McCutcheon Project Manager The resul/s per/ain only to the samples tested ill /he laboratory. This report shall not be reproduced, except inJull. withoutwritlenpermissionji-om Tes/America. PUFl729 ~. ( TestAmerica C THE: LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fllx:(602) 454-9303 Project ID: PO #802.10 June 2011 ( Sampled: 06/29/11 Received: 06/29/1 I Report Number: PUF1729 C C VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte ( ( Method Batch Reporting Limit Sample Dilution Date Result Factor Extracted Date Analyzed Data Qualifiers Sample ID: PUFl729-04REl (Duplicate E - Water) - cont. C ( Reporting Units: ugll Bromomethane EPA 8260B Surrogate: Dibromofluoromethane (70-130%) Surrogate: Toluene-d8 (70-130%) Surrogate: 4-Bromojluorobenzene (70-130%) ( ( IIGOIOO 1.0 ND 7/612011 7/6/2011 97% 112% 98% ( ( ( ( ( ( l ( ( ( C ( ( l ( ( ( ( C C c c c ( ( ( ( TestAmerica Phoenix ( Carlene McCutcheon Project Manager ( The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except in/ul!, wilhoutwrittenpermissionJrom TestAmerica. PUFl729 ( ( ( , , , TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/29111 Received: 06/29111 Report Number: PUFI729 METHOD BLANKlQC DATA VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte ,..- Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: llG0018 Extracted: 07/01/11 Blank Analyzed: 07/0112011 (l1GOO18-BLKl) Acetone NO NO Benzene Bromobenzene NO Bromochloromethane NO Bromodichloromethane NO Bromofonn NO 2-Butanone (MEK) NO NO n-Butylbenzene sec-Butylbenzene NO NO tert-Butylbenzene Carbon disulfide NO NO Carbon tetrachloride Chlorobenzene NO Chloroethane NO Chlorofonn NO Chloromethane NO NO 2-Chlorotoluene NO 4-Chlorotoluene NO Dibromochloromethane 1,2-Dibromo-3-chloropropane NO 1,2-Dibromoethane (EDB) NO Dibromomethane NO 1,2-Dichlorobenzene NO 1,3-Dichlorobenzene NO NO 1,4-Dichlorobenzene NO Dichlorodifluoromethane I,I-Dichloroethane NO 1,2-Dichloroethane NO l,l-Dichloroethene NO cis-l,2-Dichloroethene NO trans-l,2-Dichloroethene NO 1,2-Dichloropropane NO 1,3-Dichloropropane NO 2,2-Dichloropropane NO 1,I-Dichloropropene NO 10 0.50 0.50 0.50 0.50 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll VI TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except infull. without wriflenpermissionjrom TestAmerica. PUF1729 .. ~ ( ( TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project 10: PO #802.1 0 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/29111 Received: 06/29111 Report Number: PUF 1729 ( ( ( C C C ( C C VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result O/OREC O/OREC Limits RPD RPD Limit Data Qualifiers Batch: llG0018 Extracted: 07/01111 NO trans-! ,3-Dichloropropene NO Ethylbenzene NO Hexachlorobutadiene NO 2-Hexanone NO Iodomethane NO Isopropylbenzene NO p-Isopropylto!uene NO Methylene Chloride NO 4-Methyl-2-pentanone (MIBK) NO Methyl-tert-butyl Ether (MTBE) NO Naphthalene NO n-Propylbenzene NO Styrene NO 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene NO Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene I, I, I-Trichloroethane I, I,2-Trichloroethane Trichloroethene Trichlorotluoromethane NO NO NO NO NO NO NO NO NO 0.50 0.50 0.50 1.0 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 ( ugil ugil C ugll ( ugil ugil C ugll ( ugil ugil ugil ugil ugil ( ( ugll C ugll ( ugll C C ugil ugil ugll ( ( ugil ugil ugll ugil VI ( ugll C ugil ugil ( NO 1,3,5-Trimethylbenzene Vinyl Acetate NO Vinyl chloride Xylenes, Total NO Surrogate: Dibromofluoromethane 26.8 ugll 25.0 107 70-130 Surrogate: Toluene-d8 25.3 uglt 25.0 101 70-/30 Surrogate: 4-Bromofluorobenzene 25.6 ugll 25.0 103 70-130 NO NO C ugll 1,2,3-Trichloropropane I ,2,4-Trimethylbenzene NO ( C Blank Analyzed: 07/0112011 (11GOOI8-BLKI) cis-l,3-Dichloropropene C ugll ( ugll ( ugil ugil ugil C C C C C TestAmerica Phoenix ( Carlene McCutcheon Project Manager C The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except in/ull, without written permission/rom TestAmerica. PUF1729 ( ( ( , '- r ~ TestAmerica THE LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 4625 East Cotton Center Blvd. Ste 189. Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.1 0 June 2011 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 r '- Sampled: 06/29/11 Received: 06/29/11 Report Number: PUF 1729 Attention: Joel Peterson r "- r METHOD BLANKlQC DATA "- ,.r r VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) '- r '( AnaIyte , Batch: 11GOOI8 Extracted: 07/01111 r LeS Analyzed: 07/01/2011 (l1GOOI8-BSI) ,,-." ,- " Acetone 21.4 10 23.1 0.50 24.8 0.50 23.7 0.50 Bromodichloromethane 27.3 0.50 Bromoform 23.6 1.0 Units Spike Level Source Result %REC %REC Limits RPD 23.9 2.5 ugll ugll ugll ugll ugll ugll ugll 25.0 96 n-Butylbenzene 28.3 0.50 ugll 25.0 II3 70-130 sec-Butylbenzene 28.0 0.50 25.0 112 70-130 25.0 105 70-130 25.0 110 61-126 70-130 ~/ 2-Butanone (MEK) , Reporting Limit Benzene Bromobenzene "----"' Bromochloromethane ...._j Result tert-Butylbenzene 26.2 0.50 ugll ugll Carbon disulfide 27.6 0.50 ugll Carbon tetrachloride 29.1 0.50 Chlorobenzene 25.7 0.50 Cbloroethane 23.3 1.0 Chloroform 27.1 0.50 ugll ugll ugll ugll 23.4 1.0 ugll 2-Chlorotoluene 26.8 0.50 4-Chlorotoluene 27.4 0.50 ugll ugll 26.4 0.50 28.8 2.5 25.5 0.50 24.5 0.50 26.6 0.50 25.6 0.50 26.6 0.50 23.9 0.50 '--.- Chloromethane ,--. Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) '--- Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane !,I-Dichloroethane 1,2-Dichloroethane 1, l-Dichloroethene cis-! ,2-Dichloroethene trans-l,2-Dichloroethene 1,2-Dichloropropane "---~ 1,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene 25.2 0.50 30.0 0.50 23.9 0.50 23.0 0.50 23.4 0.50 23.4 0.50 24.6 0.50 28.0 1.0 25.0 0.50 25.0 86 92 30-150 25.0 25.0 99 70-130 25.0 95 70-130 25.0 109 70-130 25.0 94 67-122 48-150 RPD Data Limit Qualifiers 70-130 25.0 116 25.0 103 70-130 25.0 93 69-128 25.0 108 70-130 25.0 94 56-131 25.0 107 70-130 25.0 110 70-130 ugll 25.0 106 70-130 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 25.0 115 63-129 25.0 102 70-130 25.0 98 70-130 25.0 106 70-130 25.0 103 70-130 25.0 106 70-130 25.0 96 42-150 25.0 101 70-130 25.0 120 72-133 25.0 96 70-130 25.0 92 70-130 25.0 94 70-130 25.0 93 70-130 25.0 70-130 25.0 98 112 25.0 100 70-130 VI 70-130 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain ollly 10 the samples tested in the laboratory. fllis report shalll/ot be reproduced, except infulI, withoulwrittenpermissionji'om TestAmerica. PUF1729 ( ( ( TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson C ( ( 0~0.~0~~~'''7:h1:; METHOD BLAN~Q0.~~TA C C VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result ( ( Sampled: 06/29111 Received: 06/29/11 Report Number: PUFI729 ( %REC C %REC Limits RPD RPD Limit Data Qualifiers Batch: 11GOOI8 Extracted: 07/01111 ( ( C LCS Analyzed: 07/0112011 (11GOO18-BS1) cis-l,3-Dichloropropene 25.9 0.50 ugll 25.0 103 70-130 ( ( trans-l ,3-Dichloropropene 27.7 0.50 ugll 25.0 III 70-130 Ethylbenzene 26.9 0.50 ugll 25.0 108 70-130 Hexachlorobutadiene 27.7 1.0 ugll 25.0 III 70-130 2-Hexanone 24.7 2.5 ugll 25.0 99 44-150 Iodomethane 26.7 2.5 ugll 25.0 107 5S-138 Isopropylbenzene 28.0 0.50 ugll 25.0 1I2 70-130 p-Isopropylto!uene 27.6 0.50 ugll 25.0 110 70-130 Methylene Chloride 23.4 1.0 ugll 25.0 94 70-130 4-Methyl-2-pentanone (MIBK) 28.3 2.5 ugll 25.0 113 61-142 Methyl·tert-butyl Ether (MTBE) 26.3 0.50 ugll 25.0 105 70-130 Naphthalene 27.2 2.5 ugll 25.0 109 65-129 n-Propylbenzene 27.0 0.50 ugll 25.0 108 70-130 Styrene 24.9 0.50 ugll 25.0 100 70-130 70-130 ( ( ( C ( C ( ( ( 1,1,1,2·Tetrachloroethane 25.6 0.50 ugll 25.0 102 1,1,2,2·Tetrachloroethane 24.2 0.50 ugll 25.0 97 70-130 Tetrachloroethene 25.0 0.50 ugll 25.0 100 70-130 Toluene 24.8 0.50 ugll 25.0 99 70-130 1,2,3·Trichlorobenzene 2S.0 1.0 ugll 25.0 1I2 70-130 1,2,4·Trichlorobenzene 27.6 1.0 ugll 25.0 110 70-130 1,1,1-Trichloroethane 28.8 0.50 ugll 25.0 115 70-130 1,1,2·Trichloroethane 24.7 0.50 ugll 25.0 99 70-130 ( Trichloroethene 24.S 0.50 ugll 25.0 99 70-130 Trichlorofluoromethane 29.6 0.50 ugll 25.0 lIS 78-149 C 1,2,3·Trichloropropane 26.7 1.0 ugll 25.0 107 70-130 ( 1,2,4·Trimethylbenzene 28.3 0.50 ugll 25.0 113 70-130 VI C C C 1,3,5·Trimethylbenzene 26.9 0.50 ugll 25.0 107 70-130 C Vinyl Acetate 24.9 1.0 ugll 25.0 100 57-149 25.2 0.50 ( Vinyl chloride ugll 25.0 101 66-134 Xylenes, Total 51.2 1.5 ugll 50.0 102 70-130 Surrogate: DibromojIuoromethane 26.9 ugll 25.0 107 Surrogate: Toluene·d8 26.1 ugll 25.0 Surrogate: 4·BromojIuorobenzelle 27.1 ug/l 25.0 104 109 70-130 70-130 ( C C C C 70-130 TestAmerica Phoenix ( Carlene McCutcheon Project Manager The results pertain only 10 the samples tested in the laboratory. This report shallllot be reproduced, except in/ul!, withoutwriflenpermission/rom TesfAmerica. PUF1729 ( ( ( ( , ,- , TestAmerica ,-- THE LEADER IN ENVIRONMENTAL TESTING ,- ,,'- r 4625 East Colton Center Blvd. Ste 189, Phoenix. AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/29/11 Received: 06/29/11 Report Number: PUFI729 ,"- r METHOD BLANKlQC DATA ',. '- r VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) "- r r Reporting Analyte Result Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers ,- Batch: 11G0018 Extracted: 07/01111 LCS Dup Analyzed: 07/0112011 (l1G0018-BSDl) '-- Acetone 18.5 r---. '-- / Benzene ,.- -, Bromobenzene Bromochloromethane Bromodichloromethane Bromofonn 2-Butanone (MEK) n-Butylbenzene ,--- sec-Butylbenzene 27.8 25.8 22.3 29.4 27.4 tert-Butylbenzene 28.4 Carbon disulfide Carbon tetrachloride 28.3 29.4 26.4 Chlorobenzene Chloroethane Chlorofonn "--- Chloromethane ,.- -". 2-Chlorotoluene 4-Chlorotoluene ..... _ Dibromochloromethane ~. 24.8 27.9 24.5 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) '-...-/ Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane I,I-Dichloroethane 1,2-Dichloroethane I,I-Dichloroethene cis-I,2-Dichloroethene trans-I,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane l,l-Dichloropropene 23.8 26.6 24.9 28.5 29.5 27.3 30.4 25.9 25.1 27.2 27.6 27.4 23.5 24.9 29.9 24.3 23.1 24.2 24.4 25.2 26.9 25.0 10 0.50 0.50 0.50 0.50 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 0.50 1.0 0.50 ugll 0.50 0.50 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 ugll ugll 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 ugll 25.0 25.0 ugll 25.0 74 30-150 15 99 112 98 70-130 70-130 70-130 7 III 103 89 70-130 67-122 48-150 118 110 114 113 70-130 70-130 70-130 61-126 118 106 70-130 70-130 95 106 100 69-128 70-130 56-131 114 118 109 70-130 70-130 70-130 122 104 101 63-129 70-130 70-130 109 III 70-130 70-130 8 20 110 94 100 70-130 42-150 70-130 20 20 20 120 97 72-133 70-130 93 70-130 70-130 3 2 0.9 0.2 2 0.8 3 97 98 101 107 100 12 3 2 9 7 4 2 8 3 35 20 20 20 20 20 33 20 20 20 20 I 20 3 2 2 20 20 6 6 20 7 20 3 20 5 2 25 20 20 2 20 20 20 20 VI 20 20 70-130 70-130 4 2 20 20 20 70-130 70-130 4 0.2 20 20 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain ollly to the samples fested ill the laboratory. This report shall/fOt be reproduced, except infull, without wri1fenpermissionjrom TestAmerica. PUF1729 \ ( TestAmerica C THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson C ( Sampled: 06/29/11 Received: 06/29111 Report Number: PUFI729 C C ( C ( C VOLATILE ORGANICS BY GC/MS (EPA 5030B/S260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC ( %REC Limits RPD RPD Limit Data Qualifiers Batch: llG0018 Extracted: 07/01111 LCS Dup Analyzed: 07/0112011 (l1G0018-BSDl) cis-l ,3-Dichloropropene 26.6 trans-! ,3-Dichloropropene 27.7 Ethylbenzene 28.0 Hexachlorobutadiene 29.5 2-Hexanone 26.3 Iodomethane 29.7 Isopropylbenzene 29.4 p-Isopropyltoluene 29.1 Methylene Chloride 23.7 4-Methyl-2-pentanone (MIBK) 29.1 Methyl-tert-butyl Ether (MTBE) 25.7 29.3 Naphthalene n-Propylbenzene 29.5 Styrene 26.0 1,1,1,2-Tetrachloroethane 26.1 1, 1, 2,2-Tetrachloroethane 26.4 Tetrachloroethene 25.8 Toluene 25.6 1,2,3-Trichlorobenzene 30.1 1,2,4-Trichlorobenzene 29.6 1,1,1-Trichloroethane 28.1 1,1,2-Trichloroethane 24.8 Trichloroethene 25.6 29.3 Trichlorofluoromethane 1,2,3-Trichloropropane 28.0 1,2,4-Trimethylbenzene 29.3 1,3,5-Trimethylbenzene 30.0 Vinyl Acetate 24.4 24.8 Vinyl chloride Xylenes, Total 53.0 ( C 0.50 0.50 0.50 1.0 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 ugil ugil ugll ugil ugil ugil ugil ugil ugil ugll ugll ugil ugil ugil ugil ugll ugll ugil ugll ugil ugil ugil ugll ugll ugil ugil ugil ugil ugll ugil Surrogate: Dibromojluoromethane 26.3 ugll Surrogate: Toluene-d8 2S.8 2S.0 ugll Surrogate: 4-Bromojluorobenzene C ug/l 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 50.0 2S.0 2S.0 25.0 107 III 112 118 105 119 117 116 95 116 103 117 118 104 104 106 103 102 120 119 113 99 102 117 112 117 120 98 99 106 lOS 103 100 70-130 70-130 70-130 70-130 44-150 58-138 70-130 70-130 70-130 61-142 70-130 65-129 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 78-149 70-130 70-130 70-130 57-149 66-134 70-130 70-130 70-130 70-130 3 0.2 4 6 6 10 5 5 I 3 2 8 9 4 2 9 3 3 7 7 2 0.5 3 0.8 5 3 II 2 2 3 20 20 20 20 31 25 20 20 20 22 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 21 20 20 ( ( ( C ( C ( C ( C C. ( ( VI ( C C C C C ( ( ( TestAmerica Phoenix Carlene McCutcheon Project Manager The resulls pertain only to the samples tested in the laboratory. This report shallllot be reproduced, except illjull, without writtenpermissiolljrom TestAmerka. C PUF1729 C C C C ( ( r , TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Sampled: 06/29/11 Phoenix, AZ 85028 ( , Report Number: PUFI729 Received: 06/29/11 Attention: Joel Peterson ~ "'- METHOD BLANKlQC DATA ('" '- r VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) ,-, " ~ (" 'r Analyte Result Reporting Limit Units Spike Level Source Result %REC %REC Limits Matrix Spike Analyzed: 07/0112011 (IIGOOI8-MSl) Acetone 14.5 Benzene 21.1 0.50 25.0 NO 85 70-130 22.6 0.50 ugll 25.0 NO 90 70-130 Bromochloromethane 20.9 0.50 25.0 NO 84 70-130 Bromodichloromethane 22.8 0.50 ugll ugll 25.0 91 70-130 Bromofonn 20.1 1.0 ugll 25.0 80 62-126 "'-, 10 25.0 2-Butanone (MEK) 17.4 2.5 25.0 70 22-150 "-_ n-Butylbenzene 24.9 0.50 ugll ugll NO NO NO 25.0 NO 99 70-130 r sec-Butylbenzene 24.4 0.50 ugll 25.0 NO 98 70-130 tert-Butylbenzene 24.2 0.50 25.0 70-130 24.5 0.50 25.0 NO NO 97 Carbon disulfide ugll ugll 98 56-132 r' Carbon tetrachloride 24.9 0.50 ugll 25.0 NO 100 76-131 , Chlorobenzene 22.5 0.50 25.0 NO 90 70-130 Chloroethane 20.6 1.0 ugll ugll 25.0 NO 82 67-134 Chlorofonn 24.9 0.50 ugll 25.0 2.31 90 70-130 Chloromethane 21.4 1.0 ugll 25.0 NO 85 50-135 2-Chlorotoluene 23.8 0.50 ugll 25.0 NO 95 70-130 4-Chlorotoluene 24.6 0.50 ugll 25.0 98 70-130 Dibromochloromethane 22.8 0.50 25.0 91 70-130 1,2-Dibromo-3-chloropropane 22.3 2.5 ugll ugll NO NO 25.0 NO 89 60-135 '- ,---. ~, Data Qualifiers Source: PUFI729-02 NO 58 10-150 r . Bromobenzene '- Limit Batch: IIGOOl8 Extracted: 07/01111 ugll ugll I RPD RPD 1,2-Dibromoethane (EDB) 21.2 0.50 ugll 25.0 70-130 19.9 0.50 25.0 80 70-130 1,2-Dichlorobenzene 22.0 0.50 25.0 NO 88 70-130 1,3-Dichlorobenzene 23.3 0.50 25.0 NO 93 70-130 1,4-Dichlorobenzene 23.6 0.50 ugll ugll ugll ugll NO NO 85 Dibromomethane 25.0 NO 94 70-130 Dichlorodifluoromethane 15.5 0.50 ugll 25.0 NO 62 36-150 1,1-Dichloroethane 24.4 0.50 3.24 85 70-130 24.5 0.50 ugll ugll 25.0 1,2-Dichloroethane 25.0 NO 98 68-143 I,I-Dichloroethene 25.4 0.50 ugll 25.0 4.41 84 70-130 cis-I,2-Dichloroethene 31.1 0.50 12.3 75 70-130 21.4 0.50 25.0 NO 85 70-130 1,2-Dichloropropane 20.2 0.50 ugll ugll ugll 25.0 trans-I,2-Dichloroethene 25.0 NO 81 70-130 1,3-Dichloropropane 21.1 0.50 ugll 25.0 NO 85 70-130 2,2-Dichloropropane 24.3 1.0 25.0 NO 97 66-130 l,l-Dichloropropene 21.5 0.50 ugll ugll 25.0 NO 86 70-130 Vi TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report sha//l1ot be reproduced, except injull, without writtenpermissionjrom TestAmerica. PUF1729 l ( TestAmerica C 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson ( C ME~1tIO» BLANKlQC DATA ( C C VOLATILE ORGANICS BY GCIMS (EPA 5030B/S260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC '%REC Limits RPD RPD Limit Data Qualifiers Batch: IIG0018 Extracted: 07/01111 Matrix Spike Analyzed: 07/0112011 (IIG0018-MSl) 21.5 cis-l,3 -Dichloropropene 22.4 trans-l ,3 -Dichloropropene 23.5 Ethylbenzene 24.0 Hexachlorobutadiene 20.2 2-Hexanone 24.9 Iodomethane 25.6 Isopropylbenzene 24.9 p-Isopropyltoluene 20.2 Methylene Chloride 1,1, 1~ Trichloroethane 1, I ,2~ Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3~ Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total 24.0 24.5 20.0 82.8 24.9 21.2 23.9 24.9 19.0 21.0 44.8 Surrogate: Dibromojluoromethane 26.7 ugll Surrogate: Toluene-dB 25.1 ugll SlIn·ogafe: 4-Bromojlllorobenzene 25.7 ugll 21.3 Methyl-tert-butyl Ether (MTBE) 21.2 Naphthalene 22.9 24.3 21.2 21.6 20.4 26.4 21.9 n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1 ,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trich lorobenzene 1,2,4~Trichlorobenzene 23.4 0.50 0.50 0.50 1.0 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 ugll ugll ugll ugll 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 50.0 25.0 4-Methyl-2-pentanone (MIBK) ( ( ( Sampled: 06129111 Received: 06/29111 Report Number: PDF 1729 ( ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll Source: PUFl729-02 ND 86 70-130 ND 89 71-132 ND 94 70-130 ND 96 66-129 ND 81 18-150 ND 100 47-141 ND 102 78-137 ND 100 70-130 ND 81 74-132 ND 85 56-145 ND 85 67-138 ND 92 54-135 ND 97 70-130 ND 85 51-123 ND 86 70-130 ND 81 69-133 3.90 90 70-130 ND 88 70-130 ND 94 70-130 ND 96 66-126 ND 76-132 98 ND 80 70-130 70-130 71.1 47 0.820 74-150 96 ND 70-130 85 ND 96 70·130 ND 61-138 100 ND 76 50-150 ND 84 58-139 ND 90 70-130 107 70-130 25.0 100 70-130 25.0 103 70-130 ( ( C ( C ( ( ( C ( C ( C C C ( VI C ( M2 ( ( C ( C ( ( C ( TestAmerica Phoenix C Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except infull, without writtenpermissionji-om TestAmerica. PUFl729 ( ( ( ( ,, ,( ,r TestAmerica , THE LEADER IN ENVIRONMENTAL TESTING Synergy Environmental, LLC 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Sampled: 06/29111 Received: 06/29111 Report Number: PUFl729 Attention: Joel Peterson METHOD BLANKlQC DATA VOLATILE ORGANICS BY GCIMS (EPA S030B/8260B) Analyte Result Reporting Limit r-- Batch: 11G0018 Extracted: 07/01111 ('- Matrix Spike Dup Analyzed: 07/0112011 (11G0018-MSDl) Acetone 15.8 10 Benzene 22.3 0.50 Bromobenzene 23.9 0.50 22.3 Bromochloromethane 0.50 24.2 0.50 Bromodichloromethane Bromoform 21.6 1.0 2-Butanone (MEK) 18.4 2.5 n-Butylbenzene 25.4 0.50 25.7 0.50 sec-Butylbenzene tert-Butylbenzene 25.5 0.50 Carbon disulfide 26.2 0.50 Carbon tetrachloride 26.4 0.50 23.6 0.50 Chlorobenzene Chloroethane 20.9 1.0 26.5 Chloroform 0.50 21.5 Chloromethane 1.0 2-Chlorotoluene 0.50 25.5 25.4 0.50 4-Chlorotoluene 24.0 Dibromochloromethane 0.50 1,2-Dibromo-3-chloropropane 24.2 2.5 22.6 1,2-Dibromoethane (EDB) 0.50 21.9 Dibromomethane 0.50 1,2-Dichlorobenzene 24.2 0.50 l,3-Dichlorobenzene 24.1 0.50 24.0 0.50 1,4-Dichlorobenzene Dichlorodifluoromethane 16.3 0.50 l,l-Dichloroethane 25.9 0.50 25.3 0.50 1,2-Dichloroethane 26.4 I,l-Dichloroethene 0.50 cis-l,2-Dichloroethene 32.6 0.50 22.4 0.50 trans-I,2-Dichloroethene 1,2-Dichloropropane 22.2 0.50 22.1 1,3-Dichloropropane 0.50 24.9 1.0 2,2-Dichloropropane 22.9 1, l-Dichloropropene 0.50 '--,- L, r ~, ,.,. "--..,-.~.' r-'--./ r- '-.' r-, "r '--- ,'-." r '--_ '----_ coo, '-'- ' r --'----, '-, '---' "-- Units ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugl1 ugll Spike Level 25.0 25.0 25.0 25.0 25.0 25.0 25.0 Source Result %REC %REC Limits Source: PUF1729-02 ND 63 10-150 70-130 ND 89 ND ND ND ND ND 25.0 25.0 25.0 25.0 ND 25.0 ND ND ND ND 70-130 70-130 70-130 5 87 73 102 62-126 22-150 70-130 7 103 102 105 70-130 70-130 56-132 76-131 5 70-130 67-134 5 106 95 84 25.0 25.0 25.0 25.0 ugll 25.0 25.0 25.0 ND ND ugll 25.0 25.0 25.0 ND 88 70-130 70-130 ugll ugll 25.0 25.0 ND ugll 25.0 25.0 25.0 ND 97 97 96 70-130 70-130 70-130 36-150 70-130 ugll ugll ugll ugll ugll ugll ND 2.31 ND ND ND ND ND 97 86 102 102 96 97 90 70-130 50-135 70-130 70-130 70-130 60-135 25.0 25.0 ND 65 91 101 4.41 88 68-143 70-130 ugll ugll ugll ugll 25.0 12.3 25.0 25.0 25.0 ND 81 90 70-130 70-130 ND 89 ND 88 ugll 25.0 25.0 ND 100 ND 91 ugll ugll ugll ND 3.24 9 5 95 89 97 ugll ugll ugll ugll ND RPD 6 6 5 2 5 7 6 I 6 0.6 7 3 5 8 6 10 10 4 RPD Limit Data Qualifiers 35 20 20 20 20 20 31 20 20 20 20 20 20 20 20 20 20 20 20 29 20 20 20 20 2 20 5 22 6 3 20 4 20 20 5 20 70-130 70-130 5 9 4 20 20 20 66-130 70-130 2 6 20 20 VI , TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertaill ollly to the samples tested ill the laboratory. This report shall not be reproduced. except infull, without wrilfenpermissionfrom TestAmerica. PUF1729 TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson c ( Sampled: 06/29111 Received: 06/29111 Report Number: PUFI729 ( C ( ( ( c VOLATILE ORGANICS BY GCIMS (EPA S030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result c . %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: 11GOOI8 Extracted: 07/01/11 Matrix Spike Dup Analyzed: 07/0112011 (llGOOI8-MSDl) cis-I,3-Dichloropropene 23.6 0.50 trans-l ,3-Dichloropropene 24.6 0.50 0.50 Ethylbenzene 24.8 Hexachlorobutadiene 25.0 1.0 2-Hexanone 21.3 2.5 2.5 26.6 Iodomethane Isopropylbenzene 0.50 27.2 p-Isopropyltoluene 0.50 25.5 21.3 Methylene Chloride 1.0 23.9 4-Methyl-2-pentanone (MIBK) 2.5 Methyl-tert-butyl Ether (MTBE) 22.3 0.50 Naphthalene 24.2 2.5 n-Propylbenzene 0.50 25.9 0.50 Styrene 22.4 1,1,1,2-Tetrachloroethane 23.1 0.50 0.50 1,1,2,2-Tetrachloroethane 21.6 Tetrach1oroethene 27.2 0.50 23.6 0.50 Toluene 24.9 1,2,3-Trichlorobenzene 1.0 1.0 1,2,4-Trichlorobenzene 25.0 1,1 , I-Trichloroethane 25.2 0.50 21.6 0.50 1,1,2-Trichloroethane 0.50 Trichloroethene 87.5 Trichlorofluoromethane 0.50 25.3 1.0 23.6 1,2,3-Trichloropropane 0.50 1,2,4-Trimethylbenzene 25.4 1,3,5-Trimethylbenzene 26.2 0.50 20.7 1.0 Vinyl Acetate 0.50 Vinyl chloride 22.0 Xy1enes, Total 1.5 46.6 Surrogate: Dibromofluoromethane 26.0 Surrogate: Toluene-dB 27.3 Surrogate: 4-Bromofluorobenzel1e 25.0 ugll ugll ugll ugll ugll ugll ugll ugll 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 50.0 ug/l 25.0 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 25.0 ugll 25.0 Source: PUFI729-02 NO 95 70-130 ND 71-132 98 ND 70-130 99 NO 66-129 100 ND 85 18-150 NO 106 47-141 NO 109 78-137 ND 102 70-130 85 74-132 ND NO 95 56-145 NO 89 67-138 ND 97 54-135 NO 104 70-130 ND 90 51-123 ND 92 70-130 NO 86 69-133 3.90 93 70-130 ND 95 70-130 ND 100 70-130 NO 100 66-126 NO 101 76-132 NO 87 70-130 71.1 66 70-130 0.820 98 74-150 ND 95 70-130 NO 102 70-130 NO 105 61-138 ND 83 50-150 NO 88 58-139 NO 93 70-130 104 70-130 109 70-130 100 70-130 9 10 6 4 6 7 6 2 5 11 5 5 7 5 7 6 3 8 6 4 3 8 6 2 11 6 5 9 5 4 20 20 20 21 25 29 20 20 20 26 21 33 20 21 20 20 20 20 20 20 20 20 20 20 20 20 33 23 21 20 c ( c ( ( ( ( ( ( ( c ( ( ( ( ( V1 c ( M2 c ( c C C C ( ( ( TestAmerica Phoenix ( Carlene McCutcheon Project Manager ( The results pertain only to the samples tested in the laboratory. This report shalll/ot be reproduced, except in/ull, without wrilfenpermissiol/jrom TestAmerica. PUF1729 ( ( ( '- TestAmerica r THE LEADER IN ENVIRONMENTAL TESTING r r r' r " 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/29111 Received: 06/29111 Report Number: PUFI729 ~ (- METHOD BLANIDQC DATA '. (-. , VOLATILE ORGANICS BY GC/MS (EPA S030B/S260B) Analyte Result Reporting Limit Units Spike Level Source Result RPD %REC %REC Limits RPD Limit Data Qualifiers Batch: 11GOIOO Extracted: 07/06/11 Blank Analyzed: 07/06/2011 (11GOIOO-BLK1) ND Acetone r '-- r L r. ~ .. NO 0.50 Bromobenzene Bromochloromethane ND 0.50 ND 0.50 Bromodichloromethane NO 0.50 Bromofonn Bromomethane ND 1.0 ND 1.0 2-Butanone (MEK) ND 2.5 n-Butylbenzene sec-Butylbenzene NO 0.50 ND 0.50 tert-Butylbenzene ND 0.50 Carbon disulfide NO 0.50 Carbon tetrachloride ND 0.50 Chlorobenzene NO 0.50 Chloroethane ND 1.0 Chlorofonn ND 0.50 Chloromethane NO 1.0 2-Chlorotoluene ND 0.50 4-Chlorotoluene ND 0.50 Dibromochloromethane 0.50 I ,2-Dibromo-3-chloropropane NO NO 1,2-Dibromoethane (EDB) ND 0.50 Dibromomethane 0.50 1,3-Dichlorobenzene NO NO NO 1,4-Dichlorobenzene ND 0.50 Dichlorodifluoromethane 0.50 I,l-Dichloroethane NO NO l,2-Dichloroethane ND 0.50 I,I-Dichloroethene ND 0.50 cis-l,2-Dichloroethene ND 0.50 trans-l,2-Dichloroethene NO 0.50 1,2-Dichloropropane ND 0.50 1,3-Dichloropropane NO 0.50 2,2-Dichloropropane ND 1.0 l,2-Dichlorobenzene 'r 10 Benzene 2.5 0.50 0.50 0.50 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll Vi TestAmerica Phoenix Carlene McCutcheon Project Manager The resulls pertain only to the somples tested in the laboratory. This report shall not be reprodllced, except in/Ill!, without writtenpermissionji-om TestAmerica. PUF1729 ( ( TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson ( ( Sampled: 06/29111 Received: 06/29111 Report Number: PUFI729 ( ( (. C C ( C VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC ( %REC Limits RPD RPD Limit Data Qualifiers Batch: 11GOIOO Extracted: 07/06/11 Blank Analyzed: 07/06/2011 (l1GOIOO-BLKl) ND l,l-Dichloropropene 0.50 0.50 0.50 0.50 1.0 2.5 2.5 0.50 0.50 1.0 2.5 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 1.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 1.0 0.50 1.5 ND ND 2-Hexanone ND Iodomethane Isopropylbenzene p-Isopropyltoluene ND ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl Ether (MTBE) ND ND Naphthalene ND n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1, I ,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total ND Surrogate: Dibromojluoromethane 23.2 IIg/l Surrogate: Toluene-d8 26.9 ugll Surrogate: 4-Bromojluorobenzene 24.0 ugll ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ( ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll trans-! ,3-Dichloropropene Ethylbenzene Hexachlorobutadiene ND ( C cis-l,3-Dichloropropene ND ( ( ( ( ( ( ( C ( ( ( C ( ( ( C ( C ( 25.0 25.0 25.0 93 108 96 C C 70-130 70·130 70-130 C C ( TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tesTed in the laboratory. This report shall not be reproduced, except in/ull, without written permission/rom TestAmerica. PUFI729 ( ( ( ( ( , , ( (~ r " " TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project!D: PO #802-10 June 2011 Synergy Environmental, LLC 10645 N, Tatum Blvd., Suite 200·437 Sampled: 06/29/11 Received: 06/29/11 Report Number: PUFI729 Phoenix, AZ 85028 Attention: Joel Peterson METHOD BLANKlQC DATA c VOLATILE ORGANICS BY GCIMS (EPA 5030B/S260B) r "r Analyte Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers '(" Batch: 11GOIOO Extracted: 07/06111 r LeS Analyzed: 07/06/2011 (l1GOIOO·BSl) Acetone 46.4 '-- Benzene 23.4 r-' Bromobenzene 24.6 22.7 Bromochloromethane r~ Bromodichloromethane 24.1 ( 21.5 Bromofonn Bromomethane 19.1 2-Butanone (MEK) 28.1 24.8 n-Butylbenzene '-. sec-Butylbenzene 24.1 r 22.9 ,--. tert-Butylbenzene 25.0 r Carbon disulfide "--. Carbon tetrachloride 23.9 23.9 Chlorobenzene 23.8 Chloroethane Chlorofonn 23.4 r ' Chloromethane 21.7 25.8 2-Chlorotoluene L 26.8 4-Chlorotolucne 23.6 Dibromochloromethane 22.4 1,2-Dibromo-3 -chloropropane 1,2-0ibromoethane (EOB) 24.2 21.9 Dibromomethane 1,2-Dichlorobenzene 23.8 1,3-Dichlorobenzene 24.7 r 24.1 1,4-Dichlorobenzene Dichlorodifluoromethane 34.5 23.3 '--~ l,l-Dichloroethane 1,2-Dichloroethane 23.6 23.0 l,l-Dichloroethene cis-I,2-Dichloroethene 21.4 22.8 trans-l,2-Dichloroethene 1,2-Dichloropropane 24.6 22.2 l,3-Dichloropropane 23.6 2,2-Dichloropropane 'r 10 0.50 ugll 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 25.0 25.0 186 94 ugll ugll ugll ugll ugll ugll 25.0 25.0 25.0 99 91 70·130 70·130 70·130 25.0 25.0 25.0 96 86 76 112 70·130 67·122 64·132 48·150 ugll 25.0 25.0 25.0 25.0 99 97 92 100 70·130 70·130 70·130 61·126 25.0 25.0 96 70·130 96 95 94 70·130 69·128 70·130 87 103 107 95 90 97 88 95 99 96 138 93 94 92 85 91 99 89 94 56·131 70·130 70·130 ugll ugll ugll ugll ugll ugll ugll ugll 25.0 25.0 25.0 1.0 0.50 0.50 0.50 ugll ugll 25.0 25.0 25.0 2.5 0.50 ugll ugll 25.0 25.0 0.50 0.50 0.50 ugll 25.0 25.0 25.0 0.50 0.50 ugll 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 25.0 25.0 25.0 25.0 25.0 25.0 ugll 25.0 25.0 25.0 ugll 25.0 30·150 L3 70·130 63·129 70·130 70·130 70·130 70·130 70·130 42·150 V/ 70·130 72·133 70·130 70·130 70·130 70·130 70·130 70·130 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboralOry. This report shalf lIot be reproduced, except infull, without wriftellpermissionji-om TestAmerico. PUF1729 ( ( TestAmerica C THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06/29/11 Received: 06/29111 Report Number: PDF 1729 ( ",¥~~~~~- ••• C C VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) Result Reporting Limit Units Spike Level Source Result ( ( ( ( C METHOD BLMSKJQC DATA ,"" "0\%<),:/" Analyle ( %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: IIGOIOO Extracted: 07/06/11 l ( C LCS Analyzed: 07/06/2011 (IIG0100-BS1) 1,I-Dichloropropene 23.5 0.50 cis-I,3-Dichloropropene 26.3 0.50 trans-l ,3-Dichloropropene 26.0 0.50 Ethylbenzene 26.3 0.50 Hexachlorobutadiene 21.9 1.0 2-Hexanone 35.6 2.5 Iodomethane 21.2 2.5 Isopropy lbenzene 23.9 0.50 p-Isopropylto!uene 25.2 0.50 Methylene Chloride 22.1 1.0 4-Methyl-2-pentanone (MIBK) 28.9 2.5 Methyl-tert-butyl Ether (MTBE) 23.3 0.50 Naphthalene 23.6 2.5 n-Propylbenzene 24.0 0.50 Styrene 20.5 0.50 1,1,1,2-Tetrachloroethane 24.1 0.50 1,1,2,2-Tetrachloroethane 24.4 0.50 Tetrachloroethene 23.1 0.50 Toluene 25.8 0.50 1,2,3-Trichlorobenzene 22.6 1.0 1,2,4-Trichlorobenzene 23.4 1.0 1,1,1-Trichloroethane 24.0 0.50 1,1,2-Trichloroethane 23.2 0.50 Trichloroethene 23.9 0.50 Trichlorofluoromethane 24.8 0.50 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 1,2,3-Trichloropropane 24.2 1.0 1,2,4-Trimethylbenzene 23.3 0.50 1,3,5-Trimethylbenzene 22.7 0.50 Vinyl Acetate 21.5 1.0 Vinyl chloride 25.8 0.50 Xylenes, Total 47.7 1.5 Surrogate: DibromojIuoromethane 23.8 ugll Surrogate: Toluene-dB 27.7 ugll Surrogate: 4-BromojIuorobenzene 25.4 ug/l 25.0 94 70-130 25.0 105 70-130 25.0 104 70-130 25.0 105 70-130 ( ( ( 25.0 88 70-130 25.0 143 44-150 25.0 85 58-138 25.0 96 70-130 25.0 101 70-130 25.0 89 70-130 25.0 116 61-142 25.0 93 70-130 C 25.0 94 65-129 ( 25.0 96 70-130 25.0 82 70-130 ( ( C ( ( L 25.0 96 70-130 25.0 98 70-130 25.0 93 70-130 C 25.0 103 70-130 ( 25.0 90 70-130 25.0 94 70-130 25.0 96 70-130 25.0 93 70-130 25.0 96 70-130 25.0 99 78-149 25.0 97 70-130 25.0 93 70-130 25.0 91 70-130 25.0 86 57-149 c 25.0 103 66-134 i, 50.0 95 70-130 25.0 25.0 25.0 95 70-130 ( III 70-130 70-130 102 C c ( <.. C ( ( TestAmerica Phoenix C Carlene McCutcheon ( Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except in/ul!, withou/written permission/rom TestAmerica. PUF1729 ( ( ( C (- TestAmerica ,. ,. r '- , THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Sle 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.10 June 2011 Synergy Environmental. LLC Sampled: 06129111 Received: 06/29111 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Report Number: PUF 1729 Attention: Joel Peterson METHOD BLANKlQC DATA VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD Limit Data Qualifiers 35 L3 RPD , . Batch: lIGOIOO Extracted: 07/06111 ,- Les Dup Analyzed: 07/06/2011 (l1GOIOO-BSDl) ::=. 25.0 188 30-150 25.0 96 70-130 3 20 25.0 99 70-130 0.2 20 25.0 95 70-130 4 20 0.50 ug/l ug/l ug/l ug/l ug/l 25.0 97 70-130 1.0 ugll 25.0 90 67-122 I 5 20 20 19.0 1.0 76 64-132 0.4 20 2.5 25.0 121 48-150 7 33 25.0 99 70-130 0.2 20 25.0 96 70-130 0.3 20 25.0 92 70-130 0.5 20 25.0 101 61-126 25.0 97 70-130 25.0 97 70-130 2 25.0 95 69-128 0.3 0.50 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 25.0 30.2 0.50 ugll 24.6 0.50 1,2-Dibromo-3-chloropropane 25.4 2.5 '-_ 1,2-Dibromoethane (EDB) 25.9 0.50 22.7 0.50 '--- Dibromomethane 1,2-Dichlorobenzene 24.6 0.50 1,3-Dichlorobenzene 25.0 0.50 1,4-Dichlorobenzene 24.4 0.50 Dichlorodifluoromethane 34.4 0.50 l,l-Dichloroethane 23.6 1,2-Dichloroethane l,l-Dichloroethene Acetone 47.1 10 Benzene r '. Bromobenzene 24.1 0.50 24.7 0.50 r, Bromochloromethane ,-.. Bromodichloromethane 23.7 0.50 24.4 Bromoform Bromomethane 22.5 ,-' 2-Butanone (MEK) .-- n-Butylbenzene 24.8 0.50 '---- sec-Butylbenzene 24.1 0.50 "'--.-_ tert-Butylbenzene r-, Carbon disulfide 23.0 0.50 25.3 0.50 ......... Carbon tetrachloride 24.2 0.50 Chlorobenzene 24.3 0.50 Chloroethane 23.7 1.0 Chloroform Chloromethane 23.9 0.50 21.9 1.0 2-Chlorotoluene 25.8 4-Chlorotoluene 26.7 Dibromochloromethane "- r ,". ~ ,. r- '--- ,- r '-- '-- 20 20 25.0 96 70-130 2 25.0 87 56-131 0.6 25.0 103 70-130 0.1 20 20 20 20 20 25.0 107 70·130 0.4 20 25.0 98 70-130 4 20 25.0 102 63-129 13 25 25.0 104 70·130 7 20 25.0 91 70-130 3 20 25.0 99 70-130 4 20 25.0 100 70-130 20 25.0 98 70-130 I 1 25.0 138 42-150 0.3 20 0.50 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 25.0 94 70-130 I 20 25.4 0.50 ugll 25.0 101 72-133 7 20 23.6 0.50 25.0 94 70-130 21.9 0.50 25.0 87 70-130 2 2 20 cis-l,2-Dichloroethene trans-l,2-Dichloroethene 23.0 0.50 25.0 92 70-130 I 20 1,2-Dichloropropane 23.5 0.50 25.0 94 70-130 5 20 1,3-Dichloropropane 23.8 0.50 25.0 95 70-130 7 20 2,2-Dichloropropane 23.9 1.0 ug/l ug/l ug/l ug/l ug/l ug/l 25.0 96 70-130 20 VI 20 20 '-. TestAmerica Phoenix Carlene McCutcheon Project Manager The res/dis pertain only to the samples tested in the laboratory. This report shall /lot be reproduced, except infull, without wrillenpermission/i'om TestAmerica. PUF1729 ( TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) . -____________________________________________________________________________________________ ~45~4~-9~30~3~ Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson (- ( Sampled: 06/29111 Received: 06/29111 Report Number: PUFl729 __, C C. C ( C ( C VOLATILE ORGANICS BY GCIMS (EPA S030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC ( %REC Limits RPD RPD Limit Data Qualifiers Batch: 11G0100 Extracted: 07/06/11 I, ( C Les Dup Analyzed: 07/06/2011 (I1G0100-BSDl) 20 ( 20 ( 1,1-Dichloropropene 24.4 0.50 ugll 25.0 98 70-130 4 cis-l,3-Dichloropropene 26.9 0.50 ugll 25.0 108 70-130 trans-l ,3-Dichloropropene 27.9 0.50 ugll 25.0 112 70-130 2 7 Ethylbenzene Hexachlorobutadiene 26.5 0.50 106 70-130 0.8 1.0 25.0 89 70-130 2 2-Hexanone Iodomethane 42.0 2.5 25.0 168 44-150 16 31 21.7 2.5 25.0 87 58-138 Isopropylbenzene 23.8 0.50 25.0 95 70-130 25.2 0.50 25.0 101 70-130 2 0.3 0.2 25 20 p-IsopropyJtoluene 20 Methylene Chloride 23.0 1.0 ugll ugll ugll ugll ugll ugll ugll 25.0 22.4 20 20 20 25.0 92 70-130 4 20 4-Methyl-2-pentanone (MIBK) 31.4 2.5 ugll 25.0 126 61-142 8 Methyl-tert-butyl Ether (MTBE) 24.7 0.50 ugll 25.0 99 70-130 6 Naphthalene 100 65-129 6 22 20 20 24.9 2.5 ugll 25.0 n-Propylbenzene 24.3 0.50 97 70-130 20.7 0.50 25.0 83 70-130 0.8 1,1,1,2-Tetrachloroethane 1,1 ,2,2-Tetrachloroethane Tetrachloroethene 24.8 0.50 ugll ugll ugll 25.0 Styrene 25.0 99 70-130 26.3 0.50 ugll 25.0 105 70-130 ( ( L3 20 20 ( C ( ( ( ( 20 C 20 20 C 20 ( ( ( 23.6 0.50 ugll 25.0 94 70-130 Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene I ,I ,I-Trichloroethane 1,1,2-Trichloroethane 26.3 0.50 ugll 25.0 105 70-130 3 7 2 2 23.5 1.0 ugll 25.0 94 70-130 4 20 24.0 1.0 ugll 25.0 96 70-130 20 24.5 0.50 25.0 98 70-130 25.5 0.50 ugll ugll 2 2 25.0 102 70-130 10 20 Trichloroethene Trichlorofluoromethane 23.2 0.50 ugll 25.0 70-130 3 20 c 25.3 0.50 ugll 25.0 78-149 2 20 ( 1,2,3-Trichloropropane 1,2,4-Trimetbylbenzene I ,3,5-Trimethylbenzene 25.5 1.0 ugll 25.0 70-130 5 20 23.5 0.50 ugll 25.0 22.7 0.50 ugll 25.0 93 101 102 94 91 Vinyl Acetate 23.1 1.0 ugll 25.0 92 Vinyl chloride Xylenes, Total Surrogate: Dibro1llofluoromethane 25.7 0.50 25.0 103 48.1 1.5 ugll ugll 50.0 23.9 ug!l Surrogate: Toluene-d8 27.8 Surrogate: 4-Bromojluorobenzene 25.4 70-130 20 20 0.2 20 57-149 7 21 66-134 0.2 20 96 70-130 0.9 20 25.0 96 70-130 ug!l 25.0 25.0 111 102 70-130 ug!l 70-130 ( ( ( C C C 70-130 C TestAmerica Phoenix ~ .. ~.. Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except infull, withoutwrillen permissionFom TestAmerica. PUFI729 ( ( C ( l ( c TestAmerica THE LEADER IN ENVIRONMENTAL TESTING ,, c ,- , , l 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437~3340 Fax:(602) 454-9303 Project ID: PO #802.1 0 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Sampled: 06129111 Received: 06129111 Report Number: PUFI729 C. METHOD BLANKlQC DATA ,'- ,,- VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B) '- r' '(- ,- AnaIyte Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: llGOIOO Extracted: 07106/11 '-- ( Matrix Spike Analyzed: 0710612011 (IIGOIOO-MSl) Acetone 28.5 "--_ Benzene 24.5 r . Bromobenzene 24.2 '- Bromochloromethane 24.2 " Bromodichloromethane 25.8 r. Bromofonn 21.1 ......... Bromomethane 18.6 r "--_ 2-Butanone (MEK) 24.6 r- n-Butylbenzene 24.5 '-- sec-Butylbenzene 23.6 "-, tert-Butylbenzene 22.1 25.8 Carbon disulfide "-- Carbon tetrachloride 24.4 r Chlorobenzene 25.0 L·Chloroethane 24.6 '-- Chlorofonn 26.8 ,.----. Chloromethane 23.4 24.8 2-Chlorotoluene L 4-Chlorotoluene 25.9 24.9 Dibromochloromethane I ,2-Dibromo-3-chloropropane 23.8 ...... _ 1,2-Dibromoethane (EDB) 26.6 Dibromomethane 24.5 '-- 1,2-Dichlorobenzene 24.3 24.3 1,3-Dichlorobenzene 1,4-Dichlorobenzene 23.4 Dichlorodifluoromethane 37.0 27.4 "-' ' I,l-Dichloroethane 1,2-Dichloroethane 27.7 1,1-Dichloroethene 27.0 "--- cis-I,2-Dichloroethene 33.6 23.9 trans-J ,2-Dichloroethene 1,2-Dichloropropane 26.2 24.5 1,3-Dichloropropane 2,2-Dichloropropane 24.0 ,'---' L,- 10 0.50 0.50 0.50 0.50 1.0 1.0 2.5 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 1.0 0.50 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 1.0 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 25.0 Source: PUFl729-04REl ND 114 10-150 NO 98 70-130 ND 97 70-130 ND 70-130 97 NO 103 70-130 ND 84 62-126 55-136 0.800 71 ND 98 22-150 0.260 97 70-130 0.290 70-130 93 70-130 ND 88 NO 103 56-132 ND 76-131 97 NO 100 70-130 ND 98 67-134 1.81 100 70-130 ND 94 50-135 NO 99 70-130 ND 103 70-130 ND 100 70-130 ND 95 60-135 70-130 ND 106 NO 98 70-130 70-130 ND 97 ND 97 70-130 ND 70-130 94 36-150 NO 148 70-130 2.59 99 ND III 68-143 2.91 96 70-130 70-130 10.2 93 NO 95 70-130 70-130 0.230 104 ND 98 70-130 66-130 NO 96 VI TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in the laboratory. This report sholl not be reproduced, except injull, without writtenpermissionjrom TestAmerica. PUFl729 I ,,--- ( TestAmerica c THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotlon Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454·9303 Project ID: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson c ( Sampled: 06/29/11 Received: 06/29/11 Report Number: PUFl729 ( ( '. ~----------------------------------------------------------------------------------~(. C METHob~iANiQQC:DATA of __ _, , - ( _ C VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) AnaIyte Result Reporting Limit Units Spike Level Source Result %REC ( %REC Limits RPD RPD Limit Data Qualifiers Batch: llG0100 Extracted: 07/06111 C ( ( Matrix Spike Analyzed: 07/06/2011 (l1G0100-MS1) l,l-Dichloropropene 24.4 cis-! ,3-Dichloropropene 26.2 trans-l ,3-Dichloropropene 275 Ethylbenzene 27.1 Source: PUFI729-04REI 25.0 No 98 70-130 25.0 ND 105 70-130 0.50 ugll ugll ugll 25.0 ND 110 71-132 0.50 ugll 25.0 NO 109 70-130 0.50 050 ( C ( Hexachlorobutadiene 21.8 1.0 ugll 25.0 ND 87 66-129 2-Hexanone 32.1 2.5 ugll 25.0 ND 128 18-150 Iodomethane 21.4 2.5 25.0 86 47-141 ( Isopropylbenzene 22.9 050 25.0 NO ND 92 78-137 p-Isopropylto!uene 24.6 050 25.0 ND 98 70-130 ( 25.0 ND 96 74-132 25.0 Methylene Chloride 23.9 1.0 4-Methyl-2-pentanone (MIBK) 32.2 25 ugll ugll ugll ugll ugll 56-145 25.8 050 ugll 25.0 ND ND 129 Methyl-tert-butyl Ether (MTBE) 103 67-138 Naphthalene 24.4 2.5 25.0 ND 97 54-135 n·Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1, 1,I-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total 233 050 25.0 0.390 91 70-130 830 050 25.0 ND 33 51-123 Surrogate: Dibromojluoromethane C ( ( ( 25.0 0.50 ugll ugll ugll ugll 25.0 ND 100 70-130 ( 25.8 050 ugll 25.0 ND 103 69-133 262 050 ugll 25.0 2.37 95 70-130 C M2 ( 26.6 050 ugll 25.0 ND 106 70-130 232 23.4 1.0 25.0 93 70-130 25.0 ND NO 94 66-126 ( ( 25.6 050 25.0 ND 103 76-132 ( 262 0.50 ugll ugll ugll ugll 25.0 ND 105 70-130 1.0 81.4 0.50 ugll 25.0 53.1 113 70-130 26.9 050 25.0 0360 106 74-150 25.1 1.0 ugll ugll 25.0 ND 101 70-130 22.1 050 ugll 25.0 0.320 87 70-130 21.8 050 25.0 ND 87 61-138 143 1.0 25.0 ND 0.50 25.0 ND 57 112 50-150 28.0 ugll ugll ugll 48.4 1.5 ugll 50.0 ND 97 70-130 25.1 "gil 25.0 100 70-130 Surrogate: Toluene-d8 28.5 "gil 25.0 114 70-130 Surrogate: 4-Bromojluorobenzene 26] "gil 25.0 107 70-130 ( ( C C C 58-139 ( ( C ( TestAmerica Phoenix ( Carlene McCutcheon Project Manager ( The results pertain only to the samples tested in the laboratory. This report shall/lOt be reproduced, except in/ull, without writtenpennissionjro/11 TestAl1Ierica. PUF1729 ( ( ( r TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Synergy Environmental, LLC Project ID: PO #802.10 June 2011 Sampled: 06/29111 Received: 06/29111 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Report Number: PUF 1729 Attention: Joel Peterson METHOD BLANKlQC DATA VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) Analyte Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: l1GOIOO Extracted: 07/06/11 Matrix Spike Dup Analyzed: 07/06/2011 (IIGOIOO-MSDI) Source: PUFI729-04REI ND 101 10-150 12 Bromomethane 20.3 1.0 2-Butanone (MEK) 25.8 2.5 n-Butylbenzene 24.8 0.50 sec-Butylbenzene 24.0 0.50 tert-Butylbenzene ..--, Carbon disulfide 22.7 0.50 26.2 0.50 Carbon tetrachloride Chlorobenzene 24.7 0.50 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 24.2 0.50 ugll 25.0 ND 97 70-130 3 20 Chloroethane 24.6 1.0 ugll 25.0 ND 99 67-134 20 Chlorofonn 26.9 0.50 25.0 1.81 101 70-130 Chloromethane 23.7 1.0 ugll ugll 0.3 0.3 25.0 ND 95 50-135 2-Chlorotoluene 25.4 0.50 25.0 70-130 3 20 26.2 0.50 25.0 ND ND 102 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane l,l-Dichloroethane 1,2-Dichloroethane l,l-Dichloroethene cis-I,2-Dichloroethene trans-I,2-Dichloroethene 1,2-Dichloropropane l,3-Dichloropropane 2,2-Dichloropropane ugll ugll 105 70-130 20 25.7 0.50 ugll 25.0 ND 103 70-130 I 3 24.5 2.5 25.0 60-135 3 29 0.50 25.0 ND ND 98 26.2 105 70-130 2 20 22.7 0.50 25.0 ND 91 70-130 7 20 24.5 0.50 25.0 ND 98 70-130 I 20 25.0 0.50 25.0 ND 100 70-130 3 20 24.4 0.50 25.0 70-130 4 20 0.50 25.0 ND ND 98 36.9 148 36-150 0.1 27.1 0.50 25.0 2.59 98 70-130 22 20 27.0 0.50 25.0 ND 108 68-143 2 20 26.9 0.50 ugll ugll ugll ugll ugll ugll ugll ugll ugll ugll 25.0 2.91 96 70-130 0.5 20 32.3 0.50 ugll 25.0 10.2 88 70-130 4 20 23.8 0.50 25.0 ND 95 70-130 0.2 20 23.6 0.50 25.0 0.230 93 70-130 II 20 23.9 0.50 25.0 ND 96 70-130 3 20 23.7 1.0 ugll ugll ugll ugll 25.0 ND 95 66-130 ",--, Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane 25.2 24.2 24.7 10 0.50 0.50 24.8 0.50 24.7 0.50 Bromofonn 21.8 1.0 25.0 35 25.0 ND 97 70-130 2 20 25.0 99 70-130 2 20 25.0 ND ND 99 70-130 2 20 25.0 ND 99 70-130 4 20 25.0 ND 87 62-126 4 20 25.0 0.800 78 55-136 9 24 25.0 ND 103 22-150 5 31 25.0 0.260 98 70-130 25.0 0.290 95 70-130 2 20 20 25.0 ND 91 70-130 3 20 25.0 ND 105 56-132 2 20 25.0 ND 99 76-131 I 20 20 20 20 VI 20 TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only 10 the samples lested in the laboratory. 71lis report sha/l/101 be reproduced, except infull, wilhoutwriltenpermissionfrom TestAmerica. PUF1729 TestAmerica C' \" THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project 1D: PO #802.1 0 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson C ( Sampled: 06/29111 Received: 06/29/11 Report Number: PUFI729 ( C c r \ .. Analyte METHOD BLANIATA ( VOLATILE ORGANICS BY GCIMS (EPA 5030B/8260B) C C Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Data Qualifiers Batch: IIGOIOO Extracted: 07/06!11 C ( ( Matrix Spike Dup Analyzed: 07/06/2011 (1!GOIOO-MSDl) Source: PUFI729-04REI ( l,l-Dichloropropene cis-1,3-Dichloropropene trans-I ,3-Dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone Iodomethane Isopropy lbenzene p-Isopropyltoluene 24.2 0.50 ugll 25.0 ND 97 26.2 050 ND 105 70-130 0.1 20 050 25.0 ND 112 71-132 050 25.0 ND 106 70-130 2 2 20 26.6 21.7 1.0 ugll ugll ugll ugll 25.0 28.0 25.0 ND 87 66-129 0.6 21 31.3 2.5 ugll 25.0 ND 125 18-150 3 25 25.0 ND ND 85 47-141 0.6 29 ( 25.0 25,0 94 78-137 2 20 ND 70-130 ( 101 2 20 Methylene Chloride 25.0 ND 94 74-132 ND ND 124 56-145 4 26 104 67-138 0.3 21 C ( 21.3 25 23.4 0.50 25.1 050 23.6 1.0 ugll ugll ugll ugll 4-Methyl-2-pentanone (MIBK) 30.9 25 ugll 25.0 Methyl-tert-butyl Ether (MTBE) Naphthalene n-Propylbenzcne Styrene I, I, 1,2-Tetrachloroethane 1,1 ,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene I, I , I-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride Xylenes, Total 25.9 050 ugll 25.0 Surrogate: Dibromojluoromethane 25.1 SWTogate: Toluene-d8 27.8 Surrogate: 4-Bromojluorobenzene 26.0 70-130 20 C ( 20 ( ( 20 25.7 25 ugll 25.0 ND 103 54-135 5 33 23.8 0.50 ugll 25.0 0.390 94 70-130 2 20 19.6 050 ugll 25.0 ND 78 51-123 81 21 RI ( ( ( ( 24.7 0.50 ugll 25.0 ND 99 70-130 1 20 26.0 050 ugll 25.0 ND 104 69-133 0.9 20 25.6 0.50 2.37 93 70-130 2 20 050 25.0 ND 106 70-130 0.9 20 23.8 1.0 ugll ugll ugll 25.0 26.4 25.0 95 70-130 3 20 23.8 1.0 ugll 25.0 ND ND 95 66-126 2 20 25.4 050 ugll 25.0 ND 102 76-132 0.9 20 ( 25.2 050 ugll 25.0 ND 101 70-130 4 20 75.0 0.50 531 88 70-130 8 20 27.1 25.0 0.360 107 74-150 0.9 20 24.9 1.0 ugll ugll ugll 25.0 0.50 25.0 ND 100 70-130 0.8 20 23.0 0.50 ugll 25.0 0.320 91 70-130 4 20 22.6 050 ugll 25.0 ND 90 61-138 4 33 22.2 1.0 ugll 25.0 ND 89 50-150 43 23 27.8 0.50 25.0 ND 111 58-139 0.7 21 47.7 1.5 ugll ugll C C C C C 50.0 ND 20 ( ugll lIgl1 ugll 95 70-130 25.0 100 70-130 25.0 III 70-130 25.0 104 70-130 RI , (~ c c( c TestAmerica Phoenix Carlene McCutcheon Project Manager The results pertain only to the samples tested in Jhe lahoraJory. This report shall not be reproduced, except infull, without wrillenpermissionjrom TestAmerica. PUFl729 ( ( ( r TestAmerica 4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING r Project!D: PO #802.10 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Report Number: PUFI729' Sampled: 06/29111 Received: 06/29111 ~ , DATA QUALIFIERS AND DEFINITIONS r '~, '-- r '-. r' 'r 'r '-. r L3 The associated blank spike recovery was above method acceptance limits. M2 Matrix spike recovery was low; the associated blank spike recovery was acceptable. NI RI VI ND RPD See case narrative. The RPDIRSD exceeded the method acceptance limit. cev recovery was above method acceptance limits. This target analyte was not detected in the sample. Analyte NOT DETECTED at or above the reporting limit or MDL, ifMDL is specified. Relative Percent Difference ',. '- '. TestAmerica Phoenix Carlene McCutcheon Project Manager The results perlain ollly 10 the samples tested ill the laboratory. This report shall not be reproduced, excepl in/lIl1, withoutwrittenpermissiolljro/JI Tes/America. PUFl729 TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 4625 East Cotlon Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303 Project ID: PO #802.1 0 June 2011 Synergy Environmental, LLC 10645 N. Tatum Blvd., Suite 200-437 Phoenix, AZ 85028 Attention: Joel Peterson Report Number: PUFI729 Sampled: 06/29/11 Received: 06/29/11 ( ( ( ( ( C ( C ( Certification Summary C C TestAmerica Phoenix Method Matrix NeIac Arizona EPA 8260B Water x x ( ( Nevada and NELAP provide ana/yle specific accreditations. Analyte specific information/or TestAmerica may be obtained by contacting the laboratory or visiting our website at www.testamericainc.com ( ( C ( C ( ( ( ( ( ( ( \ i "( C ( ( ( C C C ( C C C TestAmerica Phoenix C Carlene McCutcheon ( Project Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except in/ul!. withoutwritlen pennissionfrom Tes/America. PUF1729 ( ( ( '( 'I 'I, ' I ,'( '\ 'I 'I '( 'C' ( ' ( 1 ( 1( ,I 'I 1( ; ( 1( TestAmerica ~.. \ ~ ..b. __ ' ~"1 \J\ SUlt>."'" ~'t> . . Project/PO Number: ~_.... --- ) , I ! 'I ,r '1 r , ( - - '"CV '- I Page 1 of ~ Analysis Required ' • \'0, Container # of Type Cant. Special Instructions ~~k I \ Ib!lJILl=--1 w::Q 'IX 'i\ ~~~ 13 l~h~h;I~%1 \.\e.Q, ~ I~~ 13 1~/~rll-lo19)1 \.\-C~ 12 I\J\ ~~\¢, IDvru&~E r- 1( ) r 1r ) ( ) r ) r ! ' ) r " Fax Nu;ter: Sample Description I\N~\ (~! 7~1$'~-21~ . S mpler: I-r?, r ) BIVd.,S~tte . ::l~e~ ) M\,hoenlx- 4625 E. Cotton Center 189, Phoepix,I\l85040 (602) 437-3340 ,FAX (602) 454-9303 /[ hucson -1870 W. Prince Rdad, Suite 59,'TuC5on,1\l8570S '(520) 807-3801 FAX (520) 807-3803 I JLas Vegas - 6000 S Eastern Ave,. Suite SE, Las Vegas/NV 89119 (702) 429-1264 TAL-D01S-550 (10110) , ~){ ~'J I L..\..C.. 1 I CHAIN OF CUSTODY FORM THE LEADER IN ENVIRONMENTAL TESTING Client Name/Address: ,1 ( ) ( ,1 ( 1 ( 1 ( 1 ( 't-J IrUPI1-?~ rx 1~g'}-1316125111\ 1- I " ~/57 "-03 ,_bL ocp rx t:::---. r-- r----t-:. .tI (,1'Z,~h;Tiii 1-'?:>'3 Relinquished By: IRe~ived By: Date/Time: DiteiTf"e: I,Rjived By: Date/Time: Datalnme: I~ve~ 1" '. t"':;"::;711 Note: By relinquishing samples to TestAmerica. client agrees to pay for the services requested .on this chain of custody form and any additional analYses performed on this project. Payment for services is due within 30 days from the date of invoice. Sa'T'ple(s) will be disposed of after 30 days. ;( _9i9L--