#=CL#

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176

LIMS USE: FR - ERIN SAVAGE
LIMS OBJECT ID: 92356244

October 03, 2017

Ms. Erin Savage
Appalachian Voices
171 Grand Blvd.
Boone, NC 28607

RE: Project: McDowell Well Water
Pace Project No.: 92356244
Dear Ms. Savage:
Enclosed are the analytical results for sample(s) received by the laboratory on September 21, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,

Lorri Patton
lorri.patton@pacelabs.com
1(828)254-7176
Project Manager
Enclosures
cc: Mr. Willie Dodson, Appalachian Voices
Mr. Matt Hepler, Appalachian Voices

REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 1 of 14

 #=CP#

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176

CERTIFICATIONS
Project:

McDowell Well Water

Pace Project No.:

92356244

Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712

North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222

REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 2 of 14

 #=SA#

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176

SAMPLE ANALYTE COUNT
Project:

McDowell Well Water

Pace Project No.:

92356244

Lab ID

Sample ID

92356244001
92356244002

Analytes
Reported

Method

Analysts

Laboratory

Frank Roberts

EPA 200.7

SH1

28

PASI-A

Melissa Easterling

EPA 200.7

SH1

28

PASI-A

REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 3 of 14

 #=AR#

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176

ANALYTICAL RESULTS
Project:

McDowell Well Water

Pace Project No.:

92356244

Sample: Frank Roberts
Parameters
200.7 MET ICP
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silicon
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc

Lab ID: 92356244001
Results

Units

Collected: 08/30/17 11:14
Report Limit

Received: 09/21/17 14:02

DF

Prepared

Matrix: Water

Analyzed

CAS No.

Qual

Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
ND
ND
ND
684
ND
ND
ND
54400
ND
ND
ND
7920
ND
14800
163
ND
ND
ND
ND
6970
ND
24300
831
ND
ND
ND
ND
ND

ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L

100
5.0
10.0
5.0
1.0
50.0
1.0
100
5.0
5.0
5.0
50.0
5.0
100
5.0
5.0
5.0
5000
10.0
100
5.0
5000
5.0
10.0
5.0
5.0
5.0
10.0

1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10

10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15
10/03/17 02:15

7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-42-8
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-98-7
7440-02-0
7440-09-7
7782-49-2
7440-21-3
7440-22-4
7440-23-5
7440-24-6
7440-28-0
7440-31-5
7440-32-6
7440-62-2
7440-66-6

M1

M1

REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,

Date: 10/03/2017 04:18 PM

without the written consent of Pace Analytical Services, LLC.

Page 4 of 14

 #=AR#

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176

ANALYTICAL RESULTS
Project:

McDowell Well Water

Pace Project No.:

92356244

Sample: Melissa Easterling
Parameters
200.7 MET ICP
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silicon
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc

Lab ID: 92356244002
Results

Units

Collected: 08/30/17 12:44
Report Limit

Received: 09/21/17 14:02

DF

Prepared

Matrix: Water

Analyzed

CAS No.

Qual

Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
429
ND
10.9
2120
5.0
ND
ND
42600
23.9
5.1
379
127000
20.0
11300
4040
6.5
17.7
ND
ND
20900
ND
8320
1440
ND
ND
6.9
8.1
289

ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L

100
5.0
10.0
5.0
1.0
50.0
1.0
100
5.0
5.0
5.0
250
5.0
100
5.0
5.0
5.0
5000
10.0
500
5.0
5000
5.0
10.0
5.0
5.0
5.0
10.0

1
1
1
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1

10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10
10/01/17 14:10

10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 03:05
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 03:05
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24
10/03/17 02:24

7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-42-8
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-98-7
7440-02-0
7440-09-7
7782-49-2
7440-21-3
7440-22-4
7440-23-5
7440-24-6
7440-28-0
7440-31-5
7440-32-6
7440-62-2
7440-66-6

REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,

Date: 10/03/2017 04:18 PM

without the written consent of Pace Analytical Services, LLC.

Page 5 of 14

 #=QC#

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176

QUALITY CONTROL DATA
Project:

McDowell Well Water

Pace Project No.:

92356244

QC Batch:

380239

Analysis Method:

EPA 200.7

QC Batch Method:

EPA 200.7

Analysis Description:

200.7 MET

Associated Lab Samples:
METHOD BLANK:

92356244001, 92356244002

2107378

Associated Lab Samples:

Matrix: Water

92356244001, 92356244002

Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silicon
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc

Units

Blank
Result

ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L

LABORATORY CONTROL SAMPLE:
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium

Reporting
Limit
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

100
5.0
10.0
5.0
1.0
50.0
1.0
100
5.0
5.0
5.0
50.0
5.0
100
5.0
5.0
5.0
5000
10.0
100
5.0
5000
5.0
10.0
5.0
5.0
5.0
10.0

Analyzed

Qualifiers

10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21
10/03/17 01:21

2107379
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L

Spike
Conc.
5000
500
500
500
500
500
500
5000

LCS
Result
4870
484
467
492
495
480
485
4880

LCS
% Rec

% Rec
Limits
97
97
93
98
99
96
97
98

Qualifiers

85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,

Date: 10/03/2017 04:18 PM

without the written consent of Pace Analytical Services, LLC.

Page 6 of 14

 #=QC#

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176

QUALITY CONTROL DATA
Project:

McDowell Well Water

Pace Project No.:

92356244

LABORATORY CONTROL SAMPLE:

2107379

Parameter

Spike
Conc.

Units

Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silicon
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc

ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L

MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

Parameter

500
500
500
5000
500
5000
500
500
500
5000
500
2500
250
5000
500
500
500
500
500
500

ug/L
ug/L
ug/L
ug/L
ug/L

Boron
Cadmium

ug/L
ug/L

Calcium
Chromium

ug/L
ug/L

Cobalt
Copper

ug/L
ug/L

Iron
Lead

ug/L
ug/L

Magnesium
Manganese

ug/L
ug/L

58.9J
5.6
5.0U
15.1
0.00005
0U
mg/L
204
0.00050
U mg/L
109000
0.0025
U mg/L
2.5U
0.0097
mg/L
1020
0.0025
U mg/L
53200
37.9

LCS
% Rec

484
487
496
4840
480
4770
485
498
477
4800J
488
2400
242
4820J
493
480
480
480
478
484

2107380

35336652001
Units
Result

Aluminum
Antimony
Arsenic
Barium
Beryllium

LCS
Result

% Rec
Limits
97
97
99
97
96
95
97
100
95
96
98
96
97
96
99
96
96
96
96
97

Qualifiers

85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115

2107381

MS
Spike
Conc.

MSD
Spike
Conc.

MS
Result

MSD
Result

MS
% Rec

MSD
% Rec

% Rec
Limits

RPD

Qual

5000
500
500
500
500

5000
500
500
500
500

4900
484
486
501
493

4780
475
479
488
478

97
96
97
97
99

94
94
95
95
96

70-130
70-130
70-130
70-130
70-130

3
2
1
3
3

500
500

500
500

721
480

702
469

103
96

99
94

70-130
70-130

3
2

5000
500

5000
500

125000
472

121000
461

336
94

256
92

70-130
70-130

3 E,M1
2

500
500

500
500

450
507

441
497

90
99

88
97

70-130
70-130

2
2

5000
500

5000
500

5830
435

5660
426

96
87

93
85

70-130
70-130

3
2

5000
500

5000
500

63300
505

61500
493

202
94

166
91

70-130
70-130

3 M1
2

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,

Date: 10/03/2017 04:18 PM

without the written consent of Pace Analytical Services, LLC.

Page 7 of 14

 #=QC#

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176

QUALITY CONTROL DATA
Project:

McDowell Well Water

Pace Project No.:

92356244

MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

Parameter

35336652001
Units
Result

Molybdenum

ug/L

Nickel

ug/L

Potassium

ug/L

Selenium

ug/L

Silicon
Silver

ug/L
ug/L

Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc

ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L

MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silicon
Silver
Sodium

2107380

0.0037J
mg/L
0.0031J
mg/L
22.0
mg/L
0.0050
U mg/L
5380
0.0025
U mg/L
502000
867
5.0U
2.5U
5.4
2.5U
0.024
mg/L

MSD
Spike
Conc.

ND
ND
ND
684
ND
ND
ND
54400
ND
ND
ND
7920
ND
14800
163
ND
ND
ND
ND
6970
ND
24300

MS
Result

MSD
Result

MS
% Rec

MSD
% Rec

% Rec
Limits

RPD

Qual

500

500

492

482

98

96

70-130

2

500

500

438

431

87

86

70-130

2

5000

5000

29400

28400

148

128

70-130

4 M1

500

500

478

477

96

95

70-130

0

2500
250

2500
250

8400
247

8180
241

121
98

112
96

70-130
70-130

3
2

5000
500
500
500
500
500
500

5000
500
500
500
500
500
500

553000
1450
402
449
486
480
481

537000
1410
400
440
476
468
478

1020
117
80
90
96
96
91

688
108
80
88
94
94
91

70-130
70-130
70-130
70-130
70-130
70-130
70-130

3 E,M1
3
1
2
2
3
1

2107382

92356244001
Units
Result
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L

2107381

MS
Spike
Conc.

2107383

MS
Spike
Conc.
5000
500
500
500
500
500
500
5000
500
500
500
5000
500
5000
500
500
500
5000
500
2500
250
5000

MSD
Spike
Conc.
5000
500
500
500
500
500
500
5000
500
500
500
5000
500
5000
500
500
500
5000
500
2500
250
5000

MS
Result
4580
457
455
1110
463
472
456
56800
455
449
468
12000
442
18600
608
471
438
6460
462
8880
230
27700

MSD
Result

MS
% Rec

4680
466
466
1150
474
481
464
59100
463
457
475
12400
450
19100
620
482
446
6610
474
9220
233
28800

91
91
91
86
93
92
91
46
91
90
94
82
88
77
89
94
88
89
92
76
92
67

MSD
% Rec
93
93
93
94
95
93
93
93
92
91
95
90
90
87
91
96
89
92
95
90
93
89

% Rec
Limits

RPD

70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130

Qual

2
2
2
4
2
2
2
4 M1
2
2
2
4
2
3
2
2
2
2
2
4
2
4 M1

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,

Date: 10/03/2017 04:18 PM

without the written consent of Pace Analytical Services, LLC.

Page 8 of 14

 #=QC#

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176

QUALITY CONTROL DATA
Project:

McDowell Well Water

Pace Project No.:

92356244

MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

Parameter
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc

2107382

92356244001
Units
Result
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L

831
ND
ND
ND
ND
ND

2107383

MS
Spike
Conc.
500
500
500
500
500
500

MSD
Spike
Conc.
500
500
500
500
500
500

MS
Result
1260
438
451
459
456
452

MSD
Result

MS
% Rec

1310
450
462
466
463
461

86
87
90
92
91
90

MSD
% Rec
95
90
92
93
93
92

% Rec
Limits

RPD

70-130
70-130
70-130
70-130
70-130
70-130

Qual

4
3
2
2
2
2

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,

Date: 10/03/2017 04:18 PM

without the written consent of Pace Analytical Services, LLC.

Page 9 of 14

 #=QL#

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176

QUALIFIERS
Project:

McDowell Well Water

Pace Project No.:

92356244

DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A

Pace Analytical Services - Asheville

ANALYTE QUALIFIERS
E

Analyte concentration exceeded the calibration range. The reported result is estimated.

M1

Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.

REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,

Date: 10/03/2017 04:18 PM

without the written consent of Pace Analytical Services, LLC.

Page 10 of 14

 #=CR#

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176

QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:

McDowell Well Water

Pace Project No.:

92356244

Lab ID

Sample ID

QC Batch Method

QC Batch

Analytical Method

Analytical
Batch

92356244001
92356244002

Frank Roberts
Melissa Easterling

EPA 200.7
EPA 200.7

380239
380239

EPA 200.7
EPA 200.7

380381
380381

REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,

Date: 10/03/2017 04:18 PM

without the written consent of Pace Analytical Services, LLC.

Page 11 of 14

  

 

f? Document Name: Document Revised: July 25, 2017
. a Sample Condition Upon Page 1 of 2
1/ Document No.: Issuing Authority:

F-CAR-cs-oaa-Revos Pace Quality or?ce

 

 

 

 

 

Laboratory receiving samples:
Ashevillgg/Edenm Greenwood El Huntersville Raleighlj MechanicsvilleE]

u0#:92356244
a as? Wt? 

 

92355244
Custody Seal Present? Dole/Seals Intact? Elites (a if .1 
Date/Initials Person Examining Con ent 
Packing Material: EIBubble rap [:IBubble Bags one Other BiologicalTissuW

 :Ialue Eng DYes 

Thermometer: [j

IR Gun ID: Type of Ice:

'Iul-I-

 
   

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Correction Factor: Cooler Temp Corrected PC): Temp should be above freezing to 
DSamples out of temp criteria. Samples on ice, cooling process
-- has begun
USDA Regulated Soil water sample)
Did samples origina In a quarantine zone within the United States: CA, NY, or SC {check maps]? Did samples originate from a foreign source (internationally,
EYES DNO including Hawaii and Puerto Rico}? [:IYes 
Comments/Discrepancy:
Chain of Costody Present? DNIA 1.
Samples Arrived within Hold Time? ?irt-f- EINJA 2.
Short Hold Time Analysis {<72 [:IYes 3.
Rush Turn Around Time Requested? DYes 1:]an 4.
Sufficient Volume? [No [:1an 5.
Correct Containers Used? ?gs Dido DNA 6.
-Pace Containers Used? ms Elmo DNKA
Containers Intact? 1]an 7.
Dissolved analysis: Samples Field Filtered? arrow [:1wa
Sample Labels Match .4315 Elm 
-Inciudes Date/Time/ID/Analvsis Matrix: [Pl
Headspace in vm vials Elm 10.
Trip Blank Present? DNO JWA 11.
Trip Blank Custody Seals Present? DYes 
CLIENT Field Data Required? DYes ?ue
Person Contacted: Date/Time:
Comments/Sample Discrepancy:
i-
Project Manager SCURF Review: 1? ll Date: l) 7
7 .
Project Manager SRF Review: ,1 Date: C7 )3 

 

1
Note: Wheneverthere is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office 
Out of hold, incorrect preservative, out of temp, incorrect containers)

Page120f14

Page13of14

 

SamplelD

 

Type of Preservative

 

pH upon receipt

 

Date preservation adjusted

 

Time preservation
adjusted

 

Amount of Preservative
added

 

 

 

 

 

Lot ll

 

pH Adjustment Log for Preserved Samples

12

11

10

ltemtl

 

BEAU-125 mL Plastic Unpreserved (Cl-j

 

BP3U-250 mL Plastic Unpreserved 

 

BPZU-SOO mL Plastic Unpreserved 

 

liter Plastic Unpreserved I

 

mL Plastic H2504 (pH 2} 

 

BP3N-250 mL plastic HN03 (pH 2)

 

BPBZ-ZSO mL Plastic ZN Acetate 8; 

 

BPSC-ZSO mL Plastic {pH 12) 

 

WGFU-Wide-mouthed Glass jar Unpreserved

 

liter Amber Unpreserved (WA) {Cl?j

 

liter Amber {pH 2)

 

AGBU-ZSO mL Amber Unpreserved (Cl-j

 

liter Amber H2504 {pH 2]

 

AGSS-ZSO mL Amber H2504 {pH 2)

 

neaAroeam-zso mL Amber 

 

DGQH-4O mL VOA HCI 

 

VGBT-4O mL VOA N32SZO3 

 

 

VGQU-40 mL VOA Unp 

 

DGQP-4O mL VOA H3PO4 (NKA)

 

VOAK (6 vials per kin?5035 kit 

 

VIGK (3 vials per kitl-VPH/Gas kit (MIA)

 

SP5T-125 mL Sterile Plastic lab) I

 

SP2T-250 mL Sterile Plastic lab)

 

 

BP3A-250 mL Plastic [9.3417]

 

Cubitainer

 

mL Scintillation vials 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

GN

 

 

 

 



is verified and within the acceptance range for

*Check mark top half of box if pH and/or dechlorination
?Bottom half of box is to list number of bottles

PM: LJP

Due Date:
CLIENT: 93-RPP VOICE

92356244

10/05/17

 

Project ii 

 

aceAna/yti'ca/

-:

 



Sample Condition Upon 
Document No.:

Document Name:

 

Pace Quality Office

 

Document Revised: July 25, 2017
Page 2 of 2
Issuing Authority:

 

 

 

'4 CHAIN-OF-CUSTODY I Analytical Request Document

- - The Chain?of?Custody is 3 LEGAL DOCUMENT. All relevant fields must be completed accurately.
Pace Ana/yt/ca.



    

Pag 14of14

Section A Section Section 
Required Client Information: Required Project lnlormation: Invoice Information;

 

   
   

 

     

 

   

Company:/l Atlention: . .

ReporlTo: . .
a 

       

       

?lei 

 



   

 

      

        

    

Cop).r To:

      

    

REGU LATO RY AGENCY

  
 

-. I 
'1 1.1. 

I?ll 
Address: fl 5
at; 

Milan A ,1?34?5

CompanyNamei./ 





        

 

   

 

Address:

  

NPDES GROUND WATER WATER



 



 

 



     

   
      

    
 

     

      

      
    

 

  
    

 

    

 

 

    

    

 

     

     

    
 

 

 

 

        

    

    

         

    

 

   

      

  

     

   

      

       
 

   

            

        

 

             

      

E'rnail .1 -, Purchase Order No.: Pace Quote UST RCRA OTHER
J. can"; I- t-?b ., Relerencel
Phone: Fax: Projecl Namea, d: Pace Project . .
a ii, 3 .5 -. ?girl r6? Manager: 5th Locatlon
Requested Due Project Number: Pace Pro?le it: 
Requested Analysis Filtered (YIN)

Section Matrix Codes a: 2
Required Client Intormation #3 2 COLLECTED Preservatives 
Drinking Water DW 8 2
Water WT COMPOSITF 3
Waste Water WW T. 
Product 3 ?mm 
SoilfSolid SL 33 [5 5? 
SAMPLE ID 0" 0L :2 {5 .. 
Wipe Sample IDs MUST BE IUE Tissue T8 0 5 I 7K 
Other DATE TIME DATE 00 W: .p I Pace Prolect No"l Lab LD.

   

 

   

   

  

 

  

6

 

 

   

      

 

?t
52?. It 

?x

 

  





 

 

  

 

 

 

 

 

00-40101an

 

 

1U

 

11

 

12

 

    

 

    

    

    

ADDITIONAL IMENTS
l?RELINQUISHED BY AFFILIATION ACCEPTED BY AFFILIATION SAMPLE CONDITIONS

      

          

 

        

new?? A. 

hi 

 

 

  





  

 

 

 

 

 

     

  

     
   

      

 

SAMPLER NAME AND SIGNATURE PRINT Name of SAMPLER: 5/ ., . .- V, 
?33: g;
. 

SIGNATURE of SAMPLER: _,re DATE I9 

., 

   

?Importanl Note: By signin I this form you are accepting Pace?s NET 30 day payment terms and agreemg to late charges of 1.51-Lper month tor any invoices not paid within 30 days. F-ALL-Q-OQUFEVD7. 15-May?2007